Quantitative In Situ Studies of Dynamic Fracture in Brittle Solids Using Dynamic X-ray Phase Contrast Imaging
Abstract
We demonstrate the use of X-ray phase contrast imaging with sub-microsecond temporal resolution to obtain quantitative visualization of dynamic fracture processes in brittle solids. We examine an amorphous solid (fused silica), a ceramic single crystal (single-crystal quartz), and a polycrystalline ceramic (boron carbide), in the form of single-edge notched specimens loaded using a three-point apparatus at nominal strain rates up to ~800 s–1. We observe that the crack tip speed for boron carbide is relatively independent of mode I stress intensity factor rate (K˙I) for these rates of loading, while that of fused silica and single-crystal quartz increases with K˙I. Further, for the amorphous and single crystal cases, we observe the development of a crack tip instability in the form of crack branching as the crack tip speed approaches 45% of the Rayleigh wave speed. This suggests that strain-rate-dependent mechanisms contribute to crack branching. Such mechanisms may, in turn, affect the macroscopic fracture properties of these materials.
- Authors:
-
- Johns Hopkins Univ., Baltimore, MD (United States). Dept. of Materials Science and Engineering and Hopkins Extreme Materials Inst.
- Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)
- Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
- Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS) and Dynamic Compression Sector (DCS)
- Army Research Lab., Adelphi, MD (United States). Weapons and Materials Research Directorate
- Johns Hopkins Univ., Baltimore, MD (United States). Dept. of Materials Science and Engineering
- Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
- Johns Hopkins Univ., Baltimore, MD (United States). Hopkins Extreme Materials Inst. and Dept. of Mechanical Engineering
- Publication Date:
- Research Org.:
- Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Argonne National Lab. (ANL), Argonne, IL (United States); Washington State Univ., Pullman, WA (United States). Inst. of Shock Physics
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES). Scientific User Facilities Division; Defense Threat Reduction Agency (DTRA); US Army Research Laboratory (USARL); USDOE National Nuclear Security Administration (NNSA), Office of Defense Programs (DP)
- Contributing Org.:
- Washington State Univ., Pullman, WA (United States). Inst. for Shock Physics and Dynamic Compression Sector (DCS)
- OSTI Identifier:
- 1473815
- Alternate Identifier(s):
- OSTI ID: 1484023; OSTI ID: 1571759
- Report Number(s):
- LA-UR-18-20842
Journal ID: ISSN 0014-4851
- Grant/Contract Number:
- AC52-06NA25396; HDTRA1-15-1-0056; W911NF-12-2-0022; NA0002442; AC02-06CH11357
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Experimental Mechanics
- Additional Journal Information:
- Journal Volume: 58; Journal Issue: 9; Journal ID: ISSN 0014-4851
- Publisher:
- Springer
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; Phase contrast X-ray imaging · Brittle materials · Dynamic Fracture; X-ray phase contrast imaging; Brittle materials; Dynamic Fracture; crack tip velocity; brittle materials; dynamic Fracture; phase contrast X-ray imaging
Citation Formats
Leong, Andrew F. T., Robinson, Andrew K., Fezzaa, K., Sun, T., Sinclair, N., Casem, D. T., Lambert, P. K., Hustedt, C. J., Daphalapurkar, Nitin P., Ramesh, K. T., and Hufnagel, T. C. Quantitative In Situ Studies of Dynamic Fracture in Brittle Solids Using Dynamic X-ray Phase Contrast Imaging. United States: N. p., 2018.
Web. doi:10.1007/s11340-018-0414-3.
Leong, Andrew F. T., Robinson, Andrew K., Fezzaa, K., Sun, T., Sinclair, N., Casem, D. T., Lambert, P. K., Hustedt, C. J., Daphalapurkar, Nitin P., Ramesh, K. T., & Hufnagel, T. C. Quantitative In Situ Studies of Dynamic Fracture in Brittle Solids Using Dynamic X-ray Phase Contrast Imaging. United States. https://doi.org/10.1007/s11340-018-0414-3
Leong, Andrew F. T., Robinson, Andrew K., Fezzaa, K., Sun, T., Sinclair, N., Casem, D. T., Lambert, P. K., Hustedt, C. J., Daphalapurkar, Nitin P., Ramesh, K. T., and Hufnagel, T. C. Fri .
"Quantitative In Situ Studies of Dynamic Fracture in Brittle Solids Using Dynamic X-ray Phase Contrast Imaging". United States. https://doi.org/10.1007/s11340-018-0414-3. https://www.osti.gov/servlets/purl/1473815.
@article{osti_1473815,
title = {Quantitative In Situ Studies of Dynamic Fracture in Brittle Solids Using Dynamic X-ray Phase Contrast Imaging},
author = {Leong, Andrew F. T. and Robinson, Andrew K. and Fezzaa, K. and Sun, T. and Sinclair, N. and Casem, D. T. and Lambert, P. K. and Hustedt, C. J. and Daphalapurkar, Nitin P. and Ramesh, K. T. and Hufnagel, T. C.},
abstractNote = {We demonstrate the use of X-ray phase contrast imaging with sub-microsecond temporal resolution to obtain quantitative visualization of dynamic fracture processes in brittle solids. We examine an amorphous solid (fused silica), a ceramic single crystal (single-crystal quartz), and a polycrystalline ceramic (boron carbide), in the form of single-edge notched specimens loaded using a three-point apparatus at nominal strain rates up to ~800 s–1. We observe that the crack tip speed for boron carbide is relatively independent of mode I stress intensity factor rate (K˙I) for these rates of loading, while that of fused silica and single-crystal quartz increases with K˙I. Further, for the amorphous and single crystal cases, we observe the development of a crack tip instability in the form of crack branching as the crack tip speed approaches 45% of the Rayleigh wave speed. This suggests that strain-rate-dependent mechanisms contribute to crack branching. Such mechanisms may, in turn, affect the macroscopic fracture properties of these materials.},
doi = {10.1007/s11340-018-0414-3},
journal = {Experimental Mechanics},
number = 9,
volume = 58,
place = {United States},
year = {Fri Sep 07 00:00:00 EDT 2018},
month = {Fri Sep 07 00:00:00 EDT 2018}
}
Web of Science
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