Microscopy Instrumentation and Nanopositioning at NSLS-II: Current Status and Future Directions
Abstract
The development of ultra-brilliant synchrotron facilities and recent advances in the fabrication of efficient nano-focusing optics have stimulated rapid development and applications of the focused beams used to elucidate nanoscale phenomena in many areas of science and technology. Various nano-focusing optics, including Kirkpatrick- Baez (KB) and elliptical mirrors, Fresnel zone plates (ZP), compound refractive and kinoform lenses, and multilayer Laue lenses (MLL), are routinely used to achieve nano-focusing. The latest experiments utilizing KB mirrors have demonstrated focal spot size of 13 nm with the ZPs and MLLs being able to focus hard X-rays to 10 nm and below. When the focused beam size is reduced to below 100 nm, there is a need to develop a dedicated system tailored for a specific application, which satisfies stringent mechanical, vibrational, and thermal characteristics to successfully enable nano-scale imaging. Multiple degrees of motion, including their positioning accuracy, resonance frequencies, and amount of heat being dissipated, have to be thoroughly considered in order to efficiently perform nano-focusing experiments.
- Authors:
-
- Brookhaven National Lab. (BNL), Upton, NY (United States)
- Publication Date:
- Research Org.:
- Brookhaven National Lab. (BNL), Upton, NY (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES)
- OSTI Identifier:
- 1483564
- Report Number(s):
- BNL-209504-2018-JAAM
Journal ID: ISSN 0894-0886
- Grant/Contract Number:
- SC0012704
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Synchrotron Radiation News
- Additional Journal Information:
- Journal Volume: 31; Journal Issue: 5; Journal ID: ISSN 0894-0886
- Publisher:
- Taylor & Francis
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 47 OTHER INSTRUMENTATION
Citation Formats
Nazaretski, E., Xu, W., Yan, H., Huang, X., Coburn, D. S., Ge, M., Lee, W. -K., Gao, Y., Xu, W., Fuchs, M. R., and Chu, Y. S. Microscopy Instrumentation and Nanopositioning at NSLS-II: Current Status and Future Directions. United States: N. p., 2018.
Web. doi:10.1080/08940886.2018.1506233.
Nazaretski, E., Xu, W., Yan, H., Huang, X., Coburn, D. S., Ge, M., Lee, W. -K., Gao, Y., Xu, W., Fuchs, M. R., & Chu, Y. S. Microscopy Instrumentation and Nanopositioning at NSLS-II: Current Status and Future Directions. United States. https://doi.org/10.1080/08940886.2018.1506233
Nazaretski, E., Xu, W., Yan, H., Huang, X., Coburn, D. S., Ge, M., Lee, W. -K., Gao, Y., Xu, W., Fuchs, M. R., and Chu, Y. S. Tue .
"Microscopy Instrumentation and Nanopositioning at NSLS-II: Current Status and Future Directions". United States. https://doi.org/10.1080/08940886.2018.1506233. https://www.osti.gov/servlets/purl/1483564.
@article{osti_1483564,
title = {Microscopy Instrumentation and Nanopositioning at NSLS-II: Current Status and Future Directions},
author = {Nazaretski, E. and Xu, W. and Yan, H. and Huang, X. and Coburn, D. S. and Ge, M. and Lee, W. -K. and Gao, Y. and Xu, W. and Fuchs, M. R. and Chu, Y. S.},
abstractNote = {The development of ultra-brilliant synchrotron facilities and recent advances in the fabrication of efficient nano-focusing optics have stimulated rapid development and applications of the focused beams used to elucidate nanoscale phenomena in many areas of science and technology. Various nano-focusing optics, including Kirkpatrick- Baez (KB) and elliptical mirrors, Fresnel zone plates (ZP), compound refractive and kinoform lenses, and multilayer Laue lenses (MLL), are routinely used to achieve nano-focusing. The latest experiments utilizing KB mirrors have demonstrated focal spot size of 13 nm with the ZPs and MLLs being able to focus hard X-rays to 10 nm and below. When the focused beam size is reduced to below 100 nm, there is a need to develop a dedicated system tailored for a specific application, which satisfies stringent mechanical, vibrational, and thermal characteristics to successfully enable nano-scale imaging. Multiple degrees of motion, including their positioning accuracy, resonance frequencies, and amount of heat being dissipated, have to be thoroughly considered in order to efficiently perform nano-focusing experiments.},
doi = {10.1080/08940886.2018.1506233},
journal = {Synchrotron Radiation News},
number = 5,
volume = 31,
place = {United States},
year = {2018},
month = {9}
}
Figures / Tables:

Works referenced in this record:
Hard x-ray scanning imaging achieved with bonded multilayer Laue lenses
journal, January 2017
- Huang, Xiaojing; Xu, Weihe; Nazaretski, Evgeny
- Optics Express, Vol. 25, Issue 8
Interlaced zone plate optics for hard X-ray imaging in the 10 nm range
journal, March 2017
- Mohacsi, Istvan; Vartiainen, Ismo; Rösner, Benedikt
- Scientific Reports, Vol. 7, Issue 1
Micro-crystallography comes of age
journal, October 2012
- Smith, Janet L.; Fischetti, Robert F.; Yamamoto, Masaki
- Current Opinion in Structural Biology, Vol. 22, Issue 5
Measuring Three-Dimensional Strain and Structural Defects in a Single InGaAs Nanowire Using Coherent X-ray Multiangle Bragg Projection Ptychography
journal, January 2018
- Hill, Megan O.; Calvo-Almazan, Irene; Allain, Marc
- Nano Letters, Vol. 18, Issue 2
Serial crystallography on in vivo grown microcrystals using synchrotron radiation
journal, February 2014
- Gati, Cornelius; Bourenkov, Gleb; Klinge, Marco
- IUCrJ, Vol. 1, Issue 2
Multilayer Laue Lens: A Brief History and Current Status
journal, July 2016
- Conley, Ray; Bouet, Nathalie; Chu, Yong S.
- Synchrotron Radiation News, Vol. 29, Issue 4
Multimodal hard x-ray imaging with resolution approaching 10 nm for studies in material science
journal, March 2018
- Yan, Hanfei; Bouet, Nathalie; Zhou, Juan
- Nano Futures, Vol. 2, Issue 1
Automated markerless full field hard x-ray microscopic tomography at sub-50 nm 3-dimension spatial resolution
journal, April 2012
- Wang, Jun; Karen Chen, Yu-chen; Yuan, Qingxi
- Applied Physics Letters, Vol. 100, Issue 14
Quantum enhancement of accuracy and precision in optical interferometry
journal, November 2017
- Kaiser, Florian; Vergyris, Panagiotis; Aktas, Djeylan
- Light: Science & Applications, Vol. 7, Issue 3
Sample manipulation and data assembly for robust microcrystal synchrotron crystallography
journal, April 2018
- Guo, Gongrui; Fuchs, Martin R.; Shi, Wuxian
- IUCrJ, Vol. 5, Issue 3
Performance and characterization of the prototype nm-scale spatial resolution scanning multilayer Laue lenses microscope
journal, March 2013
- Nazaretski, E.; Kim, Jungdae; Yan, H.
- Review of Scientific Instruments, Vol. 84, Issue 3
Design and characterization of a compact nano-positioning system for a portable transmission x-ray microscope
journal, December 2013
- Hwu, En-Te; Nazaretski, Evgeny; Chu, Yong S.
- Review of Scientific Instruments, Vol. 84, Issue 12
Raster-scanning serial protein crystallography using micro- and nano-focused synchrotron beams
journal, April 2015
- Coquelle, Nicolas; Brewster, Aaron S.; Kapp, Ulrike
- Acta Crystallographica Section D Biological Crystallography, Vol. 71, Issue 5
Oxidation of PtNi nanoparticles studied by a scanning X-ray fluorescence microscope with multi-layer Laue lenses
journal, January 2013
- Kang, Hyon Chol; Yan, Hanfei; Chu, Yong S.
- Nanoscale, Vol. 5, Issue 16
Design and performance of a scanning ptychography microscope
journal, March 2014
- Nazaretski, E.; Huang, X.; Yan, H.
- Review of Scientific Instruments, Vol. 85, Issue 3
Multimodality hard-x-ray imaging of a chromosome with nanoscale spatial resolution
journal, February 2016
- Yan, Hanfei; Nazaretski, Evgeny; Lauer, Kenneth
- Scientific Reports, Vol. 6, Issue 1
NSLS-II biomedical beamlines for micro-crystallography, FMX, and for highly automated crystallography, AMX: New opportunities for advanced data collection
conference, January 2016
- Fuchs, Martin R.; Bhogadi, Dileep K.; Jakoncic, Jean
- PROCEEDINGS OF THE 12TH INTERNATIONAL CONFERENCE ON SYNCHROTRON RADIATION INSTRUMENTATION – SRI2015, AIP Conference Proceedings
High resolution tip-tilt positioning system for a next generation MLL-based x-ray microscope
journal, November 2017
- Xu, Weihe; Schlossberger, Noah; Xu, Wei
- Measurement Science and Technology, Vol. 28, Issue 12
Optomechanical Design of a Multilayer Laue Lens Test Bed for 10-nm Focusing of Hard X-rays
journal, October 2013
- Shu, Deming; Nazaretski, Evgeny; Kim, Jungdae
- Journal of Physics: Conference Series, Vol. 463
Protein microcrystallography using synchrotron radiation
journal, August 2017
- Yamamoto, Masaki; Hirata, Kunio; Yamashita, Keitaro
- IUCrJ, Vol. 4, Issue 5
Development and characterization of monolithic multilayer Laue lens nanofocusing optics
journal, June 2016
- Nazaretski, E.; Xu, W.; Bouet, N.
- Applied Physics Letters, Vol. 108, Issue 26
Sources of inspiration
journal, January 2014
- McSweeney, Sean; Fromme, Petra
- Nature, Vol. 505, Issue 7485
Efficient concentration of high-energy x-rays for diffraction-limited imaging resolution
journal, January 2017
- Cesar da Silva, Julio; Pacureanu, Alexandra; Yang, Yang
- Optica, Vol. 4, Issue 5
High-resolution non-destructive three-dimensional imaging of integrated circuits
journal, March 2017
- Holler, Mirko; Guizar-Sicairos, Manuel; Tsai, Esther H. R.
- Nature, Vol. 543, Issue 7645
Achieving diffraction-limited nanometer-scale X-ray point focus with two crossed multilayer Laue lenses: alignment challenges
journal, January 2017
- Yan, Hanfei; Huang, Xiaojing; Bouet, Nathalie
- Optics Express, Vol. 25, Issue 21
Compact prototype apparatus for reducing the circle of confusion down to 40 nm for x-ray nanotomography
journal, March 2013
- Kim, Jungdae; Lauer, K.; Yan, H.
- Review of Scientific Instruments, Vol. 84, Issue 3
Sample manipulation and data assembly for robust microcrystal synchrotron crystallography
journal, July 2018
- Liu, Qun; Guo, Gongrui; Fuchs, Martin R.
- Acta Crystallographica Section A Foundations and Advances, Vol. 74, Issue a1
Figures / Tables found in this record: