DOE PAGES title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Microscopy Instrumentation and Nanopositioning at NSLS-II: Current Status and Future Directions

Journal Article · · Synchrotron Radiation News

The development of ultra-brilliant synchrotron facilities and recent advances in the fabrication of efficient nano-focusing optics have stimulated rapid development and applications of the focused beams used to elucidate nanoscale phenomena in many areas of science and technology. Various nano-focusing optics, including Kirkpatrick- Baez (KB) and elliptical mirrors, Fresnel zone plates (ZP), compound refractive and kinoform lenses, and multilayer Laue lenses (MLL), are routinely used to achieve nano-focusing. The latest experiments utilizing KB mirrors have demonstrated focal spot size of 13 nm with the ZPs and MLLs being able to focus hard X-rays to 10 nm and below. When the focused beam size is reduced to below 100 nm, there is a need to develop a dedicated system tailored for a specific application, which satisfies stringent mechanical, vibrational, and thermal characteristics to successfully enable nano-scale imaging. Multiple degrees of motion, including their positioning accuracy, resonance frequencies, and amount of heat being dissipated, have to be thoroughly considered in order to efficiently perform nano-focusing experiments.

Research Organization:
Brookhaven National Laboratory (BNL), Upton, NY (United States)
Sponsoring Organization:
USDOE Office of Science (SC), Basic Energy Sciences (BES)
Grant/Contract Number:
SC0012704
OSTI ID:
1483564
Report Number(s):
BNL-209504-2018-JAAM
Journal Information:
Synchrotron Radiation News, Vol. 31, Issue 5; ISSN 0894-0886
Publisher:
Taylor & FrancisCopyright Statement
Country of Publication:
United States
Language:
English

References (29)

Hard x-ray scanning imaging achieved with bonded multilayer Laue lenses journal January 2017
Interlaced zone plate optics for hard X-ray imaging in the 10 nm range journal March 2017
Micro-crystallography comes of age journal October 2012
Measuring Three-Dimensional Strain and Structural Defects in a Single InGaAs Nanowire Using Coherent X-ray Multiangle Bragg Projection Ptychography journal January 2018
Serial crystallography on in vivo grown microcrystals using synchrotron radiation journal February 2014
Multilayer Laue Lens: A Brief History and Current Status journal July 2016
Multimodal hard x-ray imaging with resolution approaching 10 nm for studies in material science journal March 2018
Automated markerless full field hard x-ray microscopic tomography at sub-50 nm 3-dimension spatial resolution journal April 2012
Quantum enhancement of accuracy and precision in optical interferometry journal November 2017
Sample manipulation and data assembly for robust microcrystal synchrotron crystallography journal April 2018
Performance and characterization of the prototype nm-scale spatial resolution scanning multilayer Laue lenses microscope journal March 2013
Design and characterization of a compact nano-positioning system for a portable transmission x-ray microscope journal December 2013
Raster-scanning serial protein crystallography using micro- and nano-focused synchrotron beams journal April 2015
Oxidation of PtNi nanoparticles studied by a scanning X-ray fluorescence microscope with multi-layer Laue lenses journal January 2013
Design and performance of a scanning ptychography microscope journal March 2014
Multimodality hard-x-ray imaging of a chromosome with nanoscale spatial resolution journal February 2016
NSLS-II biomedical beamlines for micro-crystallography, FMX, and for highly automated crystallography, AMX: New opportunities for advanced data collection
  • Fuchs, Martin R.; Bhogadi, Dileep K.; Jakoncic, Jean
  • PROCEEDINGS OF THE 12TH INTERNATIONAL CONFERENCE ON SYNCHROTRON RADIATION INSTRUMENTATION – SRI2015, AIP Conference Proceedings https://doi.org/10.1063/1.4952829
conference January 2016
Pushing the limits: an instrument for hard X-ray imaging below 20 nm journal January 2015
High resolution tip-tilt positioning system for a next generation MLL-based x-ray microscope journal November 2017
Optomechanical Design of a Multilayer Laue Lens Test Bed for 10-nm Focusing of Hard X-rays journal October 2013
Design and performance of an X-ray scanning microscope at the Hard X-ray Nanoprobe beamline of NSLS-II journal October 2017
Protein microcrystallography using synchrotron radiation journal August 2017
Development and characterization of monolithic multilayer Laue lens nanofocusing optics journal June 2016
Sources of inspiration journal January 2014
Efficient concentration of high-energy x-rays for diffraction-limited imaging resolution journal January 2017
High-resolution non-destructive three-dimensional imaging of integrated circuits journal March 2017
Achieving diffraction-limited nanometer-scale X-ray point focus with two crossed multilayer Laue lenses: alignment challenges journal January 2017
Compact prototype apparatus for reducing the circle of confusion down to 40 nm for x-ray nanotomography journal March 2013
Sample manipulation and data assembly for robust microcrystal synchrotron crystallography journal July 2018

Figures / Tables (5)


Similar Records

Related Subjects