Implementation and application of the peak scaling method for temperature measurement in the laser heated diamond anvil cell

Kunz, Martin; Yan, Jinyuan; Cornell, Earl; Domning, Edward E.; Yen, C. Ethan; Doran, Andrew; Beavers, Christine M.; Treger, Aaron; Williams, Quentin; MacDowell, Alastair A.

doi:10.1063/1.5028276

Title: Implementation and application of the peak scaling method for temperature measurement in the laser heated diamond anvil cell

Journal Article · 10 August 2018 · Review of Scientific Instruments

DOI: https://doi.org/10.1063/1.5028276 · OSTI ID:1482539

^[1]; Yan, Jinyuan ^[2];

^[1]; Domning, Edward E. ^[1]; Yen, C. Ethan ^[3];

^[1];

^[2]; Treger, Aaron ^[1]; Williams, Quentin ^[4]; MacDowell, Alastair A. ^[1]

Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States). Advanced Light Source (ALS)
Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States). Advanced Light Source (ALS); Univ. of California, Santa Cruz, CA (United States). Earth and Planetary Sciences Department
Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States). Advanced Light Source (ALS); Berkeley High School, CA (United States); Univ. of California, Berkeley, CA (United States)
Univ. of California, Santa Cruz, CA (United States). Earth and Planetary Sciences Department

In this work, a new design for a double-sided high-pressure diamond anvil cell laser heating set-up is described. The prototype is deployed at beamline 12.2.2 of the Advanced Light Source at Lawrence Berkeley National Lab. Our compact design features shortened mechanical lever arms, which results in more stable imaging optics, and thus more user friendly and more reliable temperature measurements based on pyrometry. A modification of the peak scaling method was implemented for pyrometry, including an iterative method to determine the absolute peak temperature, thus allowing for quasi-real time temperature mapping of the actual hotspot within a laser-heated diamond anvil cell without any assumptions on shape, size, and symmetry of the hotspot and without any assumptions to the relationship between fitted temperature and peak temperature. This is important since we show that the relationship between peak temperature and temperature obtained by fitting the Planck function against the thermal emission spectrum averaged over the entire hotspot is not constant but depends on variable fitting parameters (in particular, the size and position of the fitting window). The accuracy of the method is confirmed through measuring melting points of metal wires at ambient pressure. Having absolute temperature maps in real time allows for more differentiated analyses of laser heating experiments. Finally, we present such an example of the pressure variations within a heated hotspot of AgI at a loaded base pressure of 3.8 GPa.

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Research Organization:: Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22)

Grant/Contract Number:: AC02-05CH11231; AC03-76SF00098

OSTI ID:: 1482539

Journal Information:: Review of Scientific Instruments, Journal Name: Review of Scientific Instruments Journal Issue: 8 Vol. 89; ISSN 0034-6748

Publisher:: American Institute of Physics (AIP)Copyright Statement

Country of Publication:: United States

Language:: English

References (41)

Peak scaling method to measure temperatures in the laser-heated diamond anvil cell and application to the thermal conductivity of MgO: Temperature Measurement in the LHDAC Rainey, E. S. G.; Kavner, A. Journal of Geophysical Research: Solid Earth, Vol. 119, Issue 11 https://doi.org/10.1002/2014jb011267	journal	November 2014
Laser-heated diamond anvil cell experiments at high pressure: Melting curve of nickel up to 700 kbar Lazor, P.; Shen, G.; Saxena, S. K. Physics and Chemistry of Minerals, Vol. 20, Issue 2 https://doi.org/10.1007/bf00207200	journal	July 1993
Thermal conductivity and heat capacity of solid NaCl and NaI under pressure Håkansson, B.; Andersson, P. Journal of Physics and Chemistry of Solids, Vol. 47, Issue 4 https://doi.org/10.1016/0022-3697(86)90025-9	journal	January 1986
The thermal conductivity of silver iodide Goetz, M. C.; Cowen, J. A. Solid State Communications, Vol. 41, Issue 4 https://doi.org/10.1016/0038-1098(82)90377-5	journal	January 1982
Laser-heated diamond anvil cell at the advanced light source beamline 12.2.2 Caldwell, Wendel A.; Kunz, Martin; Celestre, R. S. Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 582, Issue 1 https://doi.org/10.1016/j.nima.2007.08.113	journal	November 2007
Temperature gradients and evaluation of thermoelastic properties in the synchrotron-based laser-heated diamond cell Kavner, Abby; Panero, Wendy R. Physics of the Earth and Planetary Interiors, Vol. 143-144 https://doi.org/10.1016/j.pepi.2003.12.016	journal	June 2004
The effects of chromatic dispersion on temperature measurement in the laser-heated diamond anvil cell Walter, M. Physics of The Earth and Planetary Interiors, Vol. 143-144 https://doi.org/10.1016/s0031-9201(04)00087-1	journal	June 2004
P-V-T equation of state of MgSiO3 perovskite Fiquet, Guillaume; Andrault, Denis; Dewaele, Agnès Physics of the Earth and Planetary Interiors, Vol. 105, Issue 1-2 https://doi.org/10.1016/s0031-9201(97)00077-0	journal	January 1998
The Heat Capacity and Entropy of Silver Iodide and their Interpretation in Terms of Structure Pitzer, Kenneth S. Journal of the American Chemical Society, Vol. 63, Issue 2 https://doi.org/10.1021/ja01847a044	journal	February 1941
High-pressure experiments and the phase diagram of lower mantle and core materials Boehler, R. Reviews of Geophysics, Vol. 38, Issue 2 https://doi.org/10.1029/1998rg000053	journal	May 2000
Quasi-hydrostatic compression of magnesium oxide to 52 GPa: Implications for the pressure-volume-temperature equation of state Speziale, Sergio; Zha, Chang-Sheng; Duffy, Thomas S. Journal of Geophysical Research: Solid Earth, Vol. 106, Issue B1 https://doi.org/10.1029/2000jb900318	journal	January 2001
The high-pressure melting curve of iron: A technical discussion Williams, Quentin; Knittle, Elise; Jeanloz, Raymond Journal of Geophysical Research, Vol. 96, Issue B2 https://doi.org/10.1029/90jb01999	journal	January 1991
Axial temperature gradients in dielectric samples in the laser-heated diamond cell Manga, Michael; Jeanloz, Raymond Geophysical Research Letters, Vol. 23, Issue 14 https://doi.org/10.1029/96gl01602	journal	July 1996
Temperature measurements in the laser-heated diamond cell Heinz, Dion L.; Jeanloz, Raymond High‐Pressure Research in Mineral Physics: A Volume in Honor of Syun‐iti Akimoto https://doi.org/10.1029/GM039p0113	book	January 1987
Thermal pressure in the laser-heated diamond anvil cell Heinz, Dion L. Geophysical Research Letters, Vol. 17, Issue 8 https://doi.org/10.1029/gl017i008p01161	journal	July 1990
A laser heating system that stabilizes and controls the temperature: Diamond anvil cell applications Heinz, Dion L.; Sweeney, Jeffrey S.; Miller, Peter Review of Scientific Instruments, Vol. 62, Issue 6 https://doi.org/10.1063/1.1142434	journal	June 1991
Temperature and pressure distribution in the laser-heated diamond–anvil cell Dewaele, Agnès; Fiquet, Guillaume; Gillet, Philippe Review of Scientific Instruments, Vol. 69, Issue 6 https://doi.org/10.1063/1.1148970	journal	June 1998
The birth and development of laser heating in diamond anvil cells Bassett, William A. Review of Scientific Instruments, Vol. 72, Issue 2 https://doi.org/10.1063/1.1343861	journal	January 2001
Laser heated diamond cell system at the Advanced Photon Source for in situ x-ray measurements at high pressure and temperature Shen, Guoyin; Rivers, Mark L.; Wang, Yanbin Review of Scientific Instruments, Vol. 72, Issue 2 https://doi.org/10.1063/1.1343867	journal	January 2001
Laser heating in the diamond anvil press up to 2000°C sustained and 3000°C pulsed at pressures up to 260 kilobars Ming, Li‐chung; Bassett, William A. Review of Scientific Instruments, Vol. 45, Issue 9 https://doi.org/10.1063/1.1686822	journal	September 1974
Achieving accuracy in spectroradiometric measurements of temperature in the laser-heated diamond anvil cell: Diamond is an optical component Benedetti, Laura Robin; Guignot, Nicolas; Farber, Daniel L. Journal of Applied Physics, Vol. 101, Issue 1 https://doi.org/10.1063/1.2402587	journal	January 2007
Measurement of temperature distributions across laser heated samples by multispectral imaging radiometry Campbell, Andrew J. Review of Scientific Instruments, Vol. 79, Issue 1 https://doi.org/10.1063/1.2827513	journal	January 2008
Precise measurements of radial temperature gradients in the laser-heated diamond anvil cell Kavner, A.; Nugent, C. Review of Scientific Instruments, Vol. 79, Issue 2 https://doi.org/10.1063/1.2841173	journal	January 2008
The great wedge: Quantifying chromatic aberration in imaging spectroscopy systems and application to temperature measurements in the laser-heated diamond anvil cell Benedetti, Laura Robin; Farber, Daniel L.; Kavner, Abby Journal of Applied Physics, Vol. 105, Issue 2 https://doi.org/10.1063/1.3041632	journal	January 2009
Strategy and enhanced temperature determination in a laser heated diamond anvil cell Deemyad, Shanti; Papathanassiou, Anthony N.; Silvera, Isaac F. Journal of Applied Physics, Vol. 105, Issue 9, Article No. 093543 https://doi.org/10.1063/1.3117517	journal	May 2009
Specific volume measurements of Cu, Mo, Pd, and Ag and calibration of the ruby R ₁ fluorescence pressure gauge from 0.06 to 1 Mbar Mao, H. K.; Bell, P. M.; Shaner, J. W. Journal of Applied Physics, Vol. 49, Issue 6 https://doi.org/10.1063/1.325277	journal	June 1978
The equation of state of the gold calibration standard Heinz, Dion L.; Jeanloz, Raymond Journal of Applied Physics, Vol. 55, Issue 4 https://doi.org/10.1063/1.333139	journal	February 1984
The influence of wavelength-dependent absorption and temperature gradients on temperature determination in laser-heated diamond-anvil cells Deng, Jie; Du, Zhixue; Benedetti, Laura Robin Journal of Applied Physics, Vol. 121, Issue 2 https://doi.org/10.1063/1.4973344	journal	January 2017
Emissivity measurements on some metals and oxides using multiwavelength spectral radiometry Dubrovinsky, Leonid; Saxena, Surendra High Temperatures-High Pressures, Vol. 31, Issue 4 https://doi.org/10.1068/htrt146	journal	January 1999
Ferromagnesian postperovskite silicates in the D'' layer of the Earth Mao, W. L.; Shen, G.; Prakapenka, V. B. Proceedings of the National Academy of Sciences, Vol. 101, Issue 45 https://doi.org/10.1073/pnas.0407135101	journal	November 2004
Temperature gradients, wavelength-dependent emissivity, and accuracy of high and very-high temperatures measured in the laser-heated diamond cell Benedetti, Laura Robin; Loubeyre, Paul High Pressure Research, Vol. 24, Issue 4 https://doi.org/10.1080/08957950412331331718	journal	December 2004
DIOPTAS : a program for reduction of two-dimensional X-ray diffraction data and data exploration Prescher, Clemens; Prakapenka, Vitali B. High Pressure Research, Vol. 35, Issue 3 https://doi.org/10.1080/08957959.2015.1059835	journal	May 2015
Melting criteria and imaging spectroradiometry in laser-heated diamond-cell experiments Jeanloz, Raymond; Kavner, Abby Philosophical Transactions of the Royal Society of London. Series A: Mathematical, Physical and Engineering Sciences, Vol. 354, Issue 1711, p. 1279-1305 https://doi.org/10.1098/rsta.1996.0049	journal	June 1996
Temperature measurement and melting determination in the laser-heated diamond-anvil cell Jephcoat, A. P.; Besedin, Stanislav P. Philosophical Transactions of the Royal Society of London. Series A: Mathematical, Physical and Engineering Sciences, Vol. 354, Issue 1711, p. 1333-1360 https://doi.org/10.1098/rsta.1996.0051	journal	June 1996
Constant-stress molecular dynamics: The phase diagram of silver iodide Tallon, J. L. Physical Review B, Vol. 38, Issue 13 https://doi.org/10.1103/physrevb.38.9069	journal	November 1988
Pressure-induced phase transitions in AgCl, AgBr, and AgI Hull, S.; Keen, D. A. Physical Review B, Vol. 59, Issue 2 https://doi.org/10.1103/physrevb.59.750	journal	January 1999
Structural Evidence for a Fast-Ion Transition in the High-Pressure Rocksalt Phase of Silver Iodide Keen, D. A.; Hull, S.; Hayes, W. Physical Review Letters, Vol. 77, Issue 24 https://doi.org/10.1103/physrevlett.77.4914	journal	December 1996
A beamline for high-pressure studies at the Advanced Light Source with a superconducting bending magnet as the source Kunz, Martin; MacDowell, Alastair A.; Caldwell, Wendel A. Journal of Synchrotron Radiation, Vol. 12, Issue 5 https://doi.org/10.1107/s0909049505020959	journal	August 2005
Stability of Fe,Al-bearing bridgmanite in the lower mantle and synthesis of pure Fe-bridgmanite Ismailova, Leyla; Bykova, Elena; Bykov, Maxim Science Advances, Vol. 2, Issue 7 https://doi.org/10.1126/sciadv.1600427	journal	July 2016
EosFit7c and a Fortran module (library) for equation of state calculations Angel, Ross J.; Alvaro, Matteo; Gonzalez-Platas, Javier Zeitschrift für Kristallographie - Crystalline Materials, Vol. 229, Issue 5 https://doi.org/10.1515/zkri-2013-1711	journal	January 2014
Physical contradictions and remedies using simple polythermal equations of state Helffrich, G.; Connolly, J. A. D. American Mineralogist, Vol. 94, Issue 11-12 https://doi.org/10.2138/am.2009.3262	journal	November 2009

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Carbide Formation in Refractory Mo15Nb20Re15Ta30W20 Alloy under a Combined High-Pressure and High-Temperature Condition Zhang, Congyan; Bhandari, Uttam; Zeng, Congyuan Entropy, Vol. 22, Issue 7 https://doi.org/10.3390/e22070718	journal	June 2020
Measurements of thermal conductivity across the B1-B2 phase transition in NaCl McGuire, Christopher; Sawchuk, Krista; Kavner, Abby Journal of Applied Physics, Vol. 124, Issue 11 https://doi.org/10.1063/1.5042407	journal	September 2018

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