Rapid Construction of Fe–Co–Ni Composition-Phase Map by Combinatorial Materials Chip Approach

Xing, Hui; Zhao, Bingbing; Wang, Yujie; Zhang, Xiaoyi; Ren, Yang; Yan, Ningning; Gao, Tieren; Li, Jindong; Zhang, Lanting; Wang, Hong

doi:10.1021/acscombsci.7b00171

Title: Rapid Construction of Fe–Co–Ni Composition-Phase Map by Combinatorial Materials Chip Approach

Journal Article · 30 January 2018 · ACS Combinatorial Science

DOI: https://doi.org/10.1021/acscombsci.7b00171 · OSTI ID:1481174

Xing, Hui ^[1]; Zhao, Bingbing ^[1]; Wang, Yujie ^[1];

^[2]; Ren, Yang ^[2]; Yan, Ningning ^[3];

^[4]; Li, Jindong ^[1];

^[1]; Wang, Hong ^[5]

Shanghai Jiao Tong Univ., Shanghai (China)
Argonne National Lab. (ANL), Argonne, IL (United States)
China Building Academy, Beijing (China)
Univ. of Maryland, College Park, MD (United States)
Shanghai Jiao Tong Univ., Shanghai (China); China Building Academy, Beijing (China)

100 nm thick Fe-Co-Ni materials chips were prepared and isothermally annealed at 500, 600 and 700oC, respectively. Pixel-by-pixel composition and structural mapping was performed by micro-beam X-ray at synchrotron light source. Diffraction images were recorded at a rate of 1 pattern/s. The XRD patterns were automatically processed, phase-identified and categorized by hierarchical clustering algorithm to construct the composition-phase map. Furthermore, the resulting maps are consistent with corresponding isothermal sections reported in the ASM Alloy Phase Diagram DatabaseTM, verifying the effectiveness of the present approach in phase diagram construction.

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Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Organization:: National Key Research and Development Program of China; USDOE Office of Science (SC), Basic Energy Sciences (BES). Scientific User Facilities Division

Grant/Contract Number:: AC02-06CH11357

OSTI ID:: 1481174

Journal Information:: ACS Combinatorial Science, Vol. 20, Issue 3; ISSN 2156-8952

Publisher:: American Chemical Society (ACS)Copyright Statement

Country of Publication:: United States

Language:: English

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