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Title: X-ray Raman scattering: a new in situ probe of molecular structure during nucleation and crystallization from liquid solutions

X-ray Raman scattering (XRS) has been used for in situ probing of solute molecule speciation in solution during cooling crystallization.
Authors:
ORCiD logo [1] ; ORCiD logo [2] ; ORCiD logo [3] ;  [2] ; ORCiD logo [2] ;  [4] ;  [5] ; ORCiD logo [1]
  1. School of Chemical and Process Engineering, University of Leeds, Leeds LS2 9JT, UK, Diamond Light Source Ltd.
  2. Diamond Light Source Ltd., Didcot, UK
  3. Advanced Photon Source, Argonne National Laboratory, Argonne, USA
  4. School of Design, The University of Leeds, Leeds LS2 9JT, UK
  5. School of Chemical and Process Engineering, University of Leeds, Leeds LS2 9JT, UK, Department of Physics
Publication Date:
Grant/Contract Number:
AC02-06CH11357
Type:
Published Article
Journal Name:
CrystEngComm
Additional Journal Information:
Journal Name: CrystEngComm Journal Volume: 20 Journal Issue: 43; Journal ID: ISSN 1466-8033
Publisher:
Royal Society of Chemistry (RSC)
Sponsoring Org:
USDOE
Country of Publication:
United Kingdom
Language:
English
OSTI Identifier:
1474755

Al-Madhagi, Laila H., Chang, Sin-Yuen, Balasubramanian, Mahalingam, Kroner, Anna B., Shotton, Elizabeth J., Willneff, Elizabeth A., Mishra, Bhoopesh, and Schroeder, Sven L. M.. X-ray Raman scattering: a new in situ probe of molecular structure during nucleation and crystallization from liquid solutions. United Kingdom: N. p., Web. doi:10.1039/C8CE00929E.
Al-Madhagi, Laila H., Chang, Sin-Yuen, Balasubramanian, Mahalingam, Kroner, Anna B., Shotton, Elizabeth J., Willneff, Elizabeth A., Mishra, Bhoopesh, & Schroeder, Sven L. M.. X-ray Raman scattering: a new in situ probe of molecular structure during nucleation and crystallization from liquid solutions. United Kingdom. doi:10.1039/C8CE00929E.
Al-Madhagi, Laila H., Chang, Sin-Yuen, Balasubramanian, Mahalingam, Kroner, Anna B., Shotton, Elizabeth J., Willneff, Elizabeth A., Mishra, Bhoopesh, and Schroeder, Sven L. M.. 2018. "X-ray Raman scattering: a new in situ probe of molecular structure during nucleation and crystallization from liquid solutions". United Kingdom. doi:10.1039/C8CE00929E.
@article{osti_1474755,
title = {X-ray Raman scattering: a new in situ probe of molecular structure during nucleation and crystallization from liquid solutions},
author = {Al-Madhagi, Laila H. and Chang, Sin-Yuen and Balasubramanian, Mahalingam and Kroner, Anna B. and Shotton, Elizabeth J. and Willneff, Elizabeth A. and Mishra, Bhoopesh and Schroeder, Sven L. M.},
abstractNote = {X-ray Raman scattering (XRS) has been used for in situ probing of solute molecule speciation in solution during cooling crystallization.},
doi = {10.1039/C8CE00929E},
journal = {CrystEngComm},
number = 43,
volume = 20,
place = {United Kingdom},
year = {2018},
month = {11}
}

Works referenced in this record:

Femtosecond X-ray protein nanocrystallography
journal, February 2011
  • Chapman, Henry N.; Fromme, Petra; Barty, Anton
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  • DOI: 10.1038/nature09750

Enhancement of Protein Crystal Nucleation by Critical Density Fluctuations
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Ab Initio Calculation of Vibrational Absorption and Circular Dichroism Spectra Using Density Functional Force Fields
journal, November 1994
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