Search Menu
DOE PAGES title logo U.S. Department of Energy
Office of Scientific and Technical Information
Search Scholarly Publications

Title: Clamp cell with in situ pressure monitoring for low-temperature neutron scattering measurements

Abstract

In this study, a clamp pressure cell for neutron scattering experiments at low temperatures and in external magnetic fields under pressure up to 2 GPa has been fabricated and tested. The cell provides optical access to the sample space that allows instantaneous pressure determination during sample loading, cooling and measuring using ruby and/or samarium doped strontium tetraborate fluorescence monitoring. Additionally, a new calibration curve of the pressure-induced shift of the 7D0-5F0 (0-0) line in the fluorescent spectrum of SrB4O7:Sm2+ for moderate pressures, P≤2 GPa, is given.

Authors:
ORCiD logo [1];  [1];  [1]; ORCiD logo [1];  [1]; ORCiD logo [2];  [1];  [1]; ORCiD logo [1]; ORCiD logo [1]
+ Show Author Affiliations
  1. Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Neutron Scattering Division
  2. Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Neutron Technologies Division
Publication Date:
Research Org.:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Sponsoring Org.:
USDOE Office of Science (SC), Basic Energy Sciences (BES)
OSTI Identifier:
1474603
Grant/Contract Number:  
AC05-00OR22725
Resource Type:
Accepted Manuscript
Journal Name:
High Pressure Research
Additional Journal Information:
Journal Volume: 38; Journal Issue: 4; Journal ID: ISSN 0895-7959
Publisher:
Taylor & Francis
Country of Publication:
United States
Language:
English
Subject:
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY; neutron scattering; pressure measurements; clamp cell; fluorescence

Citation Formats

Podlesnyak, Andrey A., Loguillo, Mark, Rucker, Gerald M., Haberl, Bianca, Boehler, Reinhard, Ehlers, Georg, Daemen, Luke L., Armitage, Douglas P., Frontzek, Matthias D., and Lumsden, Mark D. Clamp cell with in situ pressure monitoring for low-temperature neutron scattering measurements. United States: N. p., 2018. Web. doi:10.1080/08957959.2018.1519560.
Copy to clipboard
Podlesnyak, Andrey A., Loguillo, Mark, Rucker, Gerald M., Haberl, Bianca, Boehler, Reinhard, Ehlers, Georg, Daemen, Luke L., Armitage, Douglas P., Frontzek, Matthias D., & Lumsden, Mark D. Clamp cell with in situ pressure monitoring for low-temperature neutron scattering measurements. United States. https://doi.org/10.1080/08957959.2018.1519560
Copy to clipboard
Podlesnyak, Andrey A., Loguillo, Mark, Rucker, Gerald M., Haberl, Bianca, Boehler, Reinhard, Ehlers, Georg, Daemen, Luke L., Armitage, Douglas P., Frontzek, Matthias D., and Lumsden, Mark D. Thu . "Clamp cell with in situ pressure monitoring for low-temperature neutron scattering measurements". United States. https://doi.org/10.1080/08957959.2018.1519560. https://www.osti.gov/servlets/purl/1474603.
Copy to clipboard
@article{osti_1474603,
title = {Clamp cell with in situ pressure monitoring for low-temperature neutron scattering measurements},
author = {Podlesnyak, Andrey A. and Loguillo, Mark and Rucker, Gerald M. and Haberl, Bianca and Boehler, Reinhard and Ehlers, Georg and Daemen, Luke L. and Armitage, Douglas P. and Frontzek, Matthias D. and Lumsden, Mark D.},
abstractNote = {In this study, a clamp pressure cell for neutron scattering experiments at low temperatures and in external magnetic fields under pressure up to 2 GPa has been fabricated and tested. The cell provides optical access to the sample space that allows instantaneous pressure determination during sample loading, cooling and measuring using ruby and/or samarium doped strontium tetraborate fluorescence monitoring. Additionally, a new calibration curve of the pressure-induced shift of the 7D0-5F0 (0-0) line in the fluorescent spectrum of SrB4O7:Sm2+ for moderate pressures, P≤2 GPa, is given.},
doi = {10.1080/08957959.2018.1519560},
journal = {High Pressure Research},
number = 4,
volume = 38,
place = {United States},
year = {Thu Sep 20 00:00:00 EDT 2018},
month = {Thu Sep 20 00:00:00 EDT 2018}
}
Copy to clipboard
Journal Article:
Free Publicly Available Full Text
Publisher's Version of Record
https://doi.org/10.1080/08957959.2018.1519560
Copyright Statement
Other availability
Search WorldCat Search WorldCat to find libraries that may hold this journal
Citation Metrics:
Cited by: 8 works
Citation information provided by
Web of Science

Figures / Tables:

Figure 1 Figure 1: Schematic view and full assembly of the clamp cell used in the current study. (1) Cryostat sample stick; (2) Optical fiber; (3) Locking nut (Al-alloy); (4,11) Pistons (WC). The left piston has a hole for an optical fiber and (5) a diamond anvil; (6) Anti-extrusion rings (Cu); (7,8)more » Sample container (Teflon); (9) Inner sleeve (CuBe or NiCrAl alloy); (10) Main body (Al-alloy); (12) Support spacers (WC). b) Enlarged view of the piston (4).« less
All figures and tables (6 total)
Save / Share:
Export Metadata
Save to My Library
You must Sign In or Create an Account in order to save documents to your library.

Works referenced in this record:

Pressure-induced topological quantum phase transition in Sb 2 Se 3
journal, January 2014

Novel diamond cells for neutron diffraction using multi-carat CVD anvils
journal, August 2017

  • Boehler, R.; Molaison, J. J.; Haberl, B.
  • Review of Scientific Instruments, Vol. 88, Issue 8
  • DOI: 10.1063/1.4997265

Pressure-Induced Spin-State Transition in BiCoO 3
journal, July 2010

  • Oka, Kengo; Azuma, Masaki; Chen, Wei-tin
  • Journal of the American Chemical Society, Vol. 132, Issue 27
  • DOI: 10.1021/ja102987d

On the temperature correction to the ruby pressure scale
journal, May 1991

  • Vos, Willem L.; Schouten, Jan A.
  • Journal of Applied Physics, Vol. 69, Issue 9
  • DOI: 10.1063/1.348903

Optical pressure sensors for high-pressure–high-temperature studies in a diamond anvil cell
journal, December 2007

Pressure-tuned quantum criticality in the antiferromagnetic Kondo semimetal CeNi 2− δ As 2
journal, October 2015

  • Luo, Yongkang; Ronning, F.; Wakeham, N.
  • Proceedings of the National Academy of Sciences, Vol. 112, Issue 44
  • DOI: 10.1073/pnas.1509581112

Sudden reversal in the pressure dependence of Tc in the iron-based superconductor KFe2As2
journal, May 2013

  • Tafti, F. F.; Juneau-Fecteau, A.; Delage, M-È.
  • Nature Physics, Vol. 9, Issue 6
  • DOI: 10.1038/nphys2617

An Optical Fluorescence System for Quantitative Pressure Measurement in the Diamond‐Anvil Cell
journal, January 1973

  • Barnett, J. D.; Block, S.; Piermarini, G. J.
  • Review of Scientific Instruments, Vol. 44, Issue 1
  • DOI: 10.1063/1.1685943

Pressure Measurement Made by the Utilization of Ruby Sharp-Line Luminescence
journal, April 1972

SEQUOIA: A Newly Operating Chopper Spectrometer at the SNS
journal, November 2010

A comparison of four direct geometry time-of-flight spectrometers at the Spallation Neutron Source
journal, April 2014

  • Stone, M. B.; Niedziela, J. L.; Abernathy, D. L.
  • Review of Scientific Instruments, Vol. 85, Issue 4
  • DOI: 10.1063/1.4870050

New diamond cell for single-crystal x-ray diffraction
journal, November 2006

  • Boehler, Reinhard
  • Review of Scientific Instruments, Vol. 77, Issue 11
  • DOI: 10.1063/1.2372734

Ruby under pressure
journal, June 2008

Fabrication and efficiency evaluation of a hybrid NiCrAl pressure cell up to 4GPa
journal, July 2007

  • Fujiwara, Naoki; Matsumoto, Takehiko; Nakazawab, Kazuko-
  • Review of Scientific Instruments, Vol. 78, Issue 7
  • DOI: 10.1063/1.2757129

Neutron diffraction observations of interstitial protons in dense ice
journal, June 2013

  • Guthrie, M.; Boehler, R.; Tulk, C. A.
  • Proceedings of the National Academy of Sciences, Vol. 110, Issue 26
  • DOI: 10.1073/pnas.1309277110

Quantum phase transition under pressure in the heavily hydrogen-doped iron-based superconductor LaFeAsO
journal, October 2017

Freezing of glycerol–water mixtures under pressure
journal, June 2012

Resolution of VISION, a crystal-analyzer spectrometer
journal, June 2009

  • Seeger, Philip A.; Daemen, Luke L.; Larese, John Z.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 604, Issue 3
  • DOI: 10.1016/j.nima.2009.03.204

SrB 4 O 7 :Sm 2+ pressure optical sensor: Investigations in the megabar range
journal, September 1990

  • Leger, J. M.; Chateau, C.; Lacam, A.
  • Journal of Applied Physics, Vol. 68, Issue 5
  • DOI: 10.1063/1.346543

Improved calibration of the SrB4O7:Sm2+ optical pressure gauge: Advantages at very high pressures and high temperatures
journal, April 1997

  • Datchi, F.; LeToullec, R.; Loubeyre, P.
  • Journal of Applied Physics, Vol. 81, Issue 8
  • DOI: 10.1063/1.365025

Reemergent Superconductivity and Avoided Quantum Criticality in Cd-Doped CeIrIn 5 under Pressure
journal, April 2015

Hydrostatic limits in liquids and solids to 100 kbar
journal, December 1973

  • Piermarini, G. J.; Block, S.; Barnett, J. D.
  • Journal of Applied Physics, Vol. 44, Issue 12
  • DOI: 10.1063/1.1662159

Design and operation of the wide angular-range chopper spectrometer ARCS at the Spallation Neutron Source
journal, January 2012

  • Abernathy, D. L.; Stone, M. B.; Loguillo, M. J.
  • Review of Scientific Instruments, Vol. 83, Issue 1
  • DOI: 10.1063/1.3680104

Drastic Pressure Effect on the Extremely Large Magnetoresistance in WTe 2 : Quantum Oscillation Study
journal, July 2015

Charge disproportionation and the pressure-induced insulator–metal transition in cubic perovskite PbCrO 3
journal, January 2015

  • Cheng, Jinguang; Kweon, K. E.; Larregola, S. A.
  • Proceedings of the National Academy of Sciences, Vol. 112, Issue 6
  • DOI: 10.1073/pnas.1424431112

Linewidth and Temperature Shift of the R Lines in Ruby
journal, June 1963

  • McCumber, D. E.; Sturge, M. D.
  • Journal of Applied Physics, Vol. 34, Issue 6
  • DOI: 10.1063/1.1702657

High‐Pressure Equation of State for NaCl, KCl, and CsCl
journal, July 1971

Neutron scattering lengths and cross sections
journal, January 1992

Material properties of Ni Cr Al alloy and design of a 4 GPa class non-magnetic high-pressure cell
journal, October 2002

  • Uwatoko, Yoshiya; Todo, Sakae; Ueda, Kazuhiro
  • Journal of Physics: Condensed Matter, Vol. 14, Issue 44
  • DOI: 10.1088/0953-8984/14/44/469

Recent progress on HYSPEC, and its polarization analysis capabilities
journal, January 2015

Large-volume diamond cells for neutron diffraction above 90 GPa
journal, August 2013

Calibration of the ruby pressure gauge to 800 kbar under quasi-hydrostatic conditions
journal, January 1986

  • Mao, H. K.; Xu, J.; Bell, P. M.
  • Journal of Geophysical Research, Vol. 91, Issue B5, p. 4673-4676
  • DOI: 10.1029/JB091iB05p04673

High‐pressure measurements at moderate temperatures in a diamond anvil cell with a new optical sensor: SrB 4 O 7 :Sm 2 +
journal, July 1989

  • Lacam, A.; Chateau, C.
  • Journal of Applied Physics, Vol. 66, Issue 1
  • DOI: 10.1063/1.343884

Optical calibration of pressure sensors for high pressures and temperatures
journal, May 2005

  • Goncharov, Alexander F.; Zaug, Joseph M.; Crowhurst, Jonathan C.
  • Journal of Applied Physics, Vol. 97, Issue 9
  • DOI: 10.1063/1.1895467

The new cold neutron chopper spectrometer at the Spallation Neutron Source: Design and performance
journal, August 2011

  • Ehlers, G.; Podlesnyak, A. A.; Niedziela, J. L.
  • Review of Scientific Instruments, Vol. 82, Issue 8
  • DOI: 10.1063/1.3626935

The cold neutron chopper spectrometer at the Spallation Neutron Source—A review of the first 8 years of operation
journal, September 2016

  • Ehlers, G.; Podlesnyak, A. A.; Kolesnikov, A. I.
  • Review of Scientific Instruments, Vol. 87, Issue 9
  • DOI: 10.1063/1.4962024

The Wide Angle Neutron Diffractometer squared (WAND2) - Possibilities and future
journal, December 2018

Quantum Phase transition under pressure in a heavily hydrogen-doped iron-based superconductor LaFeAsO
text, January 2017

Resolution of VISION, a crystal-analyzer spectrometer
journal, June 2009

  • Seeger, Philip A.; Daemen, Luke L.; Larese, John Z.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 604, Issue 3
  • DOI: 10.1016/j.nima.2009.03.204

Linewidth and Temperature Shift of the R Lines in Ruby
journal, June 1963

  • McCumber, D. E.; Sturge, M. D.
  • Journal of Applied Physics, Vol. 34, Issue 6
  • DOI: 10.1063/1.1702657

New diamond cell for single-crystal x-ray diffraction
journal, November 2006

  • Boehler, Reinhard
  • Review of Scientific Instruments, Vol. 77, Issue 11
  • DOI: 10.1063/1.2372734

The new cold neutron chopper spectrometer at the Spallation Neutron Source: Design and performance
journal, August 2011

  • Ehlers, G.; Podlesnyak, A. A.; Niedziela, J. L.
  • Review of Scientific Instruments, Vol. 82, Issue 8
  • DOI: 10.1063/1.3626935

Improved calibration of the SrB4O7:Sm2+ optical pressure gauge: Advantages at very high pressures and high temperatures
journal, April 1997

  • Datchi, F.; LeToullec, R.; Loubeyre, P.
  • Journal of Applied Physics, Vol. 81, Issue 8
  • DOI: 10.1063/1.365025

Design and operation of the wide angular-range chopper spectrometer ARCS at the Spallation Neutron Source
journal, January 2012

  • Abernathy, D. L.; Stone, M. B.; Loguillo, M. J.
  • Review of Scientific Instruments, Vol. 83, Issue 1
  • DOI: 10.1063/1.3680104

Hydrostatic limits of 11 pressure transmitting media
journal, March 2009

  • Klotz, S.; Chervin, J-C.; Munsch, P.
  • Journal of Physics D: Applied Physics, Vol. 42, Issue 7, Article No. 075413
  • DOI: 10.1088/0022-3727/42/7/075413

Pressure Measurement Made by the Utilization of Ruby Sharp-Line Luminescence
journal, April 1972

The Cold Neutron Chopper Spectrometer at the Spallation Neutron Source - A Review of the first 8 Years of Operation
text, January 2016

    Sort by:
    [ × clear filter / sort ]

    Works referencing / citing this record:

    Effect of fine-tuning pore structures on the dynamics of confined water
    journal, May 2019

    • Kolesnikov, A. I.; Anovitz, L. M.; Hawthorne, F. C.
    • The Journal of Chemical Physics, Vol. 150, Issue 20
    • DOI: 10.1063/1.5096771

    Metal–organic frameworks under pressure
    journal, November 2019

    • Collings, Ines E.; Goodwin, Andrew L.
    • Journal of Applied Physics, Vol. 126, Issue 18
    • DOI: 10.1063/1.5126911
      Sort by:
      [ × clear filter / sort ]

      Figures / Tables found in this record:

      Figure 1 (p. 3)figure
      Figure 2 (p. 5)figure
      Figure 3 (p. 6)figure
      Figure 4 (p. 6)figure
      Figure 5 (p. 7)figure
      Figure 6 (p. 8)figure
        [ × clear filter / sort ]
        Figures/Tables have been extracted from DOE-funded journal article accepted manuscripts.

        Similar Records in DOE PAGES and OSTI.GOV collections: