skip to main content
DOE PAGES title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Bragg coherent diffractive imaging of ferromagnetic nickel nanoparticles

Abstract

We synthesized Ni nanoparticles with an atmospheric-thermal chemical vapor deposition method and investigated their lattice distortions and defects using Bragg coherent diffractive imaging. Because the strain can alter the magnetic properties of ferromagnetic materials, it is important to study the lattice distortion and structural imperfection. As a result of the Bragg coherent diffractive imaging, we found that the Ni nanocubes have a deformation-free zone in the middle. In addition, the defects such as dislocation and twin domain defects were detected in other Ni nanoparticles based on the Bragg diffraction images and patterns. The imaging of nanoparticles can contribute to a better understanding of their growth mechanisms and improve the design and synthesis of nanoparticles.

Authors:
ORCiD logo [1];  [2];  [3];  [2];  [2];  [2]
  1. Argonne National Lab. (ANL), Argonne, IL (United States); Univ. of California, San Diego, CA (United States)
  2. Univ. of California, San Diego, CA (United States)
  3. Argonne National Lab. (ANL), Argonne, IL (United States)
Publication Date:
Research Org.:
Argonne National Lab. (ANL), Argonne, IL (United States)
Sponsoring Org.:
USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22)
OSTI Identifier:
1474148
Alternate Identifier(s):
OSTI ID: 1438953
Grant/Contract Number:  
AC02-06CH11357; SC0001805
Resource Type:
Accepted Manuscript
Journal Name:
Journal of Applied Physics
Additional Journal Information:
Journal Volume: 123; Journal Issue: 20; Journal ID: ISSN 0021-8979
Publisher:
American Institute of Physics (AIP)
Country of Publication:
United States
Language:
English
Subject:
74 ATOMIC AND MOLECULAR PHYSICS

Citation Formats

Kim, J. W., Manna, S., Harder, R., Wingert, J., Fullerton, E. E., and Shpyrko, O. G. Bragg coherent diffractive imaging of ferromagnetic nickel nanoparticles. United States: N. p., 2018. Web. doi:10.1063/1.5022328.
Kim, J. W., Manna, S., Harder, R., Wingert, J., Fullerton, E. E., & Shpyrko, O. G. Bragg coherent diffractive imaging of ferromagnetic nickel nanoparticles. United States. doi:10.1063/1.5022328.
Kim, J. W., Manna, S., Harder, R., Wingert, J., Fullerton, E. E., and Shpyrko, O. G. Thu . "Bragg coherent diffractive imaging of ferromagnetic nickel nanoparticles". United States. doi:10.1063/1.5022328. https://www.osti.gov/servlets/purl/1474148.
@article{osti_1474148,
title = {Bragg coherent diffractive imaging of ferromagnetic nickel nanoparticles},
author = {Kim, J. W. and Manna, S. and Harder, R. and Wingert, J. and Fullerton, E. E. and Shpyrko, O. G.},
abstractNote = {We synthesized Ni nanoparticles with an atmospheric-thermal chemical vapor deposition method and investigated their lattice distortions and defects using Bragg coherent diffractive imaging. Because the strain can alter the magnetic properties of ferromagnetic materials, it is important to study the lattice distortion and structural imperfection. As a result of the Bragg coherent diffractive imaging, we found that the Ni nanocubes have a deformation-free zone in the middle. In addition, the defects such as dislocation and twin domain defects were detected in other Ni nanoparticles based on the Bragg diffraction images and patterns. The imaging of nanoparticles can contribute to a better understanding of their growth mechanisms and improve the design and synthesis of nanoparticles.},
doi = {10.1063/1.5022328},
journal = {Journal of Applied Physics},
number = 20,
volume = 123,
place = {United States},
year = {2018},
month = {5}
}

Journal Article:
Free Publicly Available Full Text
Publisher's Version of Record

Save / Share:

Works referenced in this record:

Bragg x-ray ptychography of a silicon crystal: Visualization of the dislocation strain field and the production of a vortex beam
journal, March 2013


The emergence of spin electronics in data storage
journal, November 2007

  • Chappert, Claude; Fert, Albert; Van Dau, Frédéric Nguyen
  • Nature Materials, Vol. 6, Issue 11
  • DOI: 10.1038/nmat2024

Three-dimensional imaging of dislocation dynamics during the hydriding phase transformation
journal, January 2017

  • Ulvestad, A.; Welland, M. J.; Cha, W.
  • Nature Materials, Vol. 16, Issue 5
  • DOI: 10.1038/nmat4842

Coherent X-ray diffraction imaging of strain at the nanoscale
journal, April 2009

  • Robinson, Ian; Harder, Ross
  • Nature Materials, Vol. 8, Issue 4
  • DOI: 10.1038/nmat2400

Nanofabricated and self-assembled magnetic structures as data storage media
journal, June 2005


Topological defect dynamics in operando battery nanoparticles
journal, June 2015


Phase transition in nanostructured LaMnO3
journal, May 2009


High- Q resonant modes in a photonic crystal heterostructure nanocavity and applicability to a Raman silicon laser
journal, December 2013


Strain-induced change in local structure and its effect on the ferromagnetic properties of La0.5Sr0.5CoO3 thin films
journal, November 2008

  • Xie, C. K.; Budnick, J. I.; Hines, W. A.
  • Applied Physics Letters, Vol. 93, Issue 18
  • DOI: 10.1063/1.3011031

Measurement of the displacement field of dislocations to 0.03 Å by electron microscopy
journal, May 2003

  • Hÿtch, Martin J.; Putaux, Jean-Luc; Pénisson, Jean-Michel
  • Nature, Vol. 423, Issue 6937
  • DOI: 10.1038/nature01638

A Micellar Approach to Magnetic Ultrahigh-Density Data-Storage Media: Extending the Limits of Current Colloidal Methods
journal, February 2007


Coherent diffraction imaging of nanoscale strain evolution in a single crystal under high pressure
journal, April 2013

  • Yang, Wenge; Huang, Xiaojing; Harder, Ross
  • Nature Communications, Vol. 4, Issue 1
  • DOI: 10.1038/ncomms2661

Accurate, rapid identification of dislocation lines in coherent diffractive imaging via a min-max optimization formulation
journal, January 2018

  • Ulvestad, A.; Menickelly, M.; Wild, S. M.
  • AIP Advances, Vol. 8, Issue 1
  • DOI: 10.1063/1.5017596

3D lattice distortions and defect structures in ion-implanted nano-crystals
journal, April 2017

  • Hofmann, Felix; Tarleton, Edmund; Harder, Ross J.
  • Scientific Reports, Vol. 7, Issue 1
  • DOI: 10.1038/srep45993

Three-dimensional mapping of a deformation field inside a nanocrystal
journal, July 2006

  • Pfeifer, Mark A.; Williams, Garth J.; Vartanyants, Ivan A.
  • Nature, Vol. 442, Issue 7098
  • DOI: 10.1038/nature04867

Analysis of strain and stacking faults in single nanowires using Bragg coherent diffraction imaging
journal, March 2010


In Situ 3D Imaging of Catalysis Induced Strain in Gold Nanoparticles
journal, July 2016

  • Ulvestad, Andrew; Sasikumar, Kiran; Kim, Jong Woo
  • The Journal of Physical Chemistry Letters, Vol. 7, Issue 15
  • DOI: 10.1021/acs.jpclett.6b01038

Curvature-induced and thermal strain in polyhedral gold nanocrystals
journal, October 2014

  • Kim, J. W.; Manna, S.; Dietze, S. H.
  • Applied Physics Letters, Vol. 105, Issue 17
  • DOI: 10.1063/1.4900866

Characterization of strain and its effects on ferromagnetic nickel nanocubes
journal, December 2017

  • Manna, Sohini; Kim, Jong Woo; Lubarda, Marko V.
  • AIP Advances, Vol. 7, Issue 12
  • DOI: 10.1063/1.5004577

Coherent X-ray diffraction investigation of twinned microcrystals
journal, October 2010

  • Aranda, Miguel A. G.; Berenguer, Felisa; Bean, Richard J.
  • Journal of Synchrotron Radiation, Vol. 17, Issue 6
  • DOI: 10.1107/S0909049510039774

Facet development during platinum nanocube growth
journal, August 2014


Strain controlled orbital state and magnetization in insulating LaMnO 3+δ films
journal, May 2015

  • Zhang, A. M.; Cheng, S. L.; Lin, J. G.
  • Journal of Applied Physics, Vol. 117, Issue 17
  • DOI: 10.1063/1.4919226

Patterned media: a viable route to 50 Gbit/in/sup 2/ and up for magnetic recording?
journal, January 1997

  • White, R. L.; Newt, R. M. H.; Pease, R. F. W.
  • IEEE Transactions on Magnetics, Vol. 33, Issue 1
  • DOI: 10.1109/20.560144

Three-dimensional imaging of dislocation propagation during crystal growth and dissolution
journal, June 2015

  • Clark, Jesse N.; Ihli, Johannes; Schenk, Anna S.
  • Nature Materials, Vol. 14, Issue 8
  • DOI: 10.1038/nmat4320

Transmission Electron Microscopy of Shape-Controlled Nanocrystals and Their Assemblies
journal, February 2000

  • Wang, Z. L.
  • The Journal of Physical Chemistry B, Vol. 104, Issue 6
  • DOI: 10.1021/jp993593c

3D Bragg coherent diffractive imaging of five-fold multiply twinned gold nanoparticle
journal, January 2017

  • Kim, Jong Woo; Ulvestad, Andrew; Manna, Sohini
  • Nanoscale, Vol. 9, Issue 35
  • DOI: 10.1039/C7NR05028C

3D Imaging of Twin Domain Defects in Gold Nanoparticles
journal, May 2015


Deformation Twinning of a Silver Nanocrystal under High Pressure
journal, October 2015