Pressure-mediated structural transitions in bulk EuTiO3

Bessas, D.; Glazyrin, K.; Ellis, D. S.; Kantor, I.; Merkel, D. G.; Cerantola, V.; Potapkin, V.; van Smaalen, S.; Baron, A. Q.  R.; Hermann, R. P.

doi:10.1103/PhysRevB.98.054105

Title: Pressure-mediated structural transitions in bulk ${EuTiO}_{3}$

Abstract

The high pressure structural phase diagram of EuTiO₃ is revisited by means of single crystal x-ray diffraction at pressures below 30GPa. We report a transition at about 3GPa with a surprisingly small lattice distortion. At 23GPa we have detected a yet unknown transition into a new orthorhombic phase (space group Ibam). Combining our observations on structures obtained on single crystals and polycrystalline samples with complementary methods, such as electrical resistivity and nuclear forward scattering of synchrotron radiation measured on polycrystalline samples, we address issues relevant to chemistry and disorder.

Authors:

Bessas, D. ^[1]; Glazyrin, K. ^[2]; Ellis, D. S. ^[3]; Kantor, I. ^[4]; Merkel, D. G. ^[4]; Cerantola, V. ^[4]; Potapkin, V. ^[5]; van Smaalen, S. ^[6]; Baron, A. Q. R. ^[3]; Hermann, R. P. ^[7]

Delft Univ. of Technology (Netherlands)
Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany)
RIKEN, Hyogo (Japan)
European Synchrotron Radiation Facility (ESRF), Grenoble (France)
Univ. Munster (Germany)
Univ. of Bayreuth (Germany)
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

Publication Date:: 2018-08-09

Research Org.:: Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1470847

Alternate Identifier(s):: OSTI ID: 1463757

Grant/Contract Number:: AC05-00OR22725

Resource Type:: Accepted Manuscript

Journal Name:: Physical Review B

Additional Journal Information:: Journal Volume: 98; Journal Issue: 5; Journal ID: ISSN 2469-9950

Publisher:: American Physical Society (APS)

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE

Citation Formats


                    Bessas, D., Glazyrin, K., Ellis, D. S., Kantor, I., Merkel, D. G., Cerantola, V., Potapkin, V., van Smaalen, S., Baron, A. Q.  R., and Hermann, R. P. Pressure-mediated structural transitions in bulk EuTiO3.  United States: N. p., 2018. 
Web.  doi:10.1103/PhysRevB.98.054105.

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                    Bessas, D., Glazyrin, K., Ellis, D. S., Kantor, I., Merkel, D. G., Cerantola, V., Potapkin, V., van Smaalen, S., Baron, A. Q.  R., & Hermann, R. P. Pressure-mediated structural transitions in bulk EuTiO3.  United States.  https://doi.org/10.1103/PhysRevB.98.054105

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                    Bessas, D., Glazyrin, K., Ellis, D. S., Kantor, I., Merkel, D. G., Cerantola, V., Potapkin, V., van Smaalen, S., Baron, A. Q.  R., and Hermann, R. P. Thu .  
"Pressure-mediated structural transitions in bulk EuTiO3".  United States.  https://doi.org/10.1103/PhysRevB.98.054105.  https://www.osti.gov/servlets/purl/1470847.

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@article{osti_1470847,

  title        = {Pressure-mediated structural transitions in bulk EuTiO3},

  author       = {Bessas, D. and Glazyrin, K. and Ellis, D. S. and Kantor, I. and Merkel, D. G. and Cerantola, V. and Potapkin, V. and van Smaalen, S. and Baron, A. Q.  R. and Hermann, R. P.},

  abstractNote = {The high pressure structural phase diagram of EuTiO3 is revisited by means of single crystal x-ray diffraction at pressures below 30GPa. We report a transition at about 3GPa with a surprisingly small lattice distortion. At 23GPa we have detected a yet unknown transition into a new orthorhombic phase (space group Ibam). Combining our observations on structures obtained on single crystals and polycrystalline samples with complementary methods, such as electrical resistivity and nuclear forward scattering of synchrotron radiation measured on polycrystalline samples, we address issues relevant to chemistry and disorder.},

  doi          = {10.1103/PhysRevB.98.054105},

  journal      = {Physical Review B},

  number       = 5,

  volume       = 98,

  place        = {United States},

  year         = {2018},

  month        = {8}

}

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Works referenced in this record:

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Works referencing / citing this record:

Multicaloric effect in multiferroic EuTiO3 thin films
journal, February 2020

Zhao, Yi-Quan; Cao, Hai-Xia
Journal of Materials Science, Vol. 55, Issue 14
DOI: 10.1007/s10853-020-04407-x

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Similar Records

Title: Pressure-mediated structural transitions in bulk EuTiO 3

Abstract

Citation Formats

Universality aspects of the metal-nonmetal transition in condensed media journal, March 1978

Structural and magnetic phase transitions in EuTi 1 − x Nb x O 3 journal, July 2015

Pressure-temperature phase diagram of multiferroic EuTiO 3 journal, August 2015

High pressure antiferrodistortive phase transition in mixed crystals of EuTiO 3 and SrTiO 3 journal, June 2016

Nuclear resonance scattering of synchrotron radiation at the 21.5 keV resonance of 151 Eu journal, September 1996

X‐Ray Diffractometry of Low‐Temperature Phase Transformations in Strontium Titanate journal, July 1964

Reversible control of magnetic interactions by electric field in a single-phase material journal, January 2013

Effect of an Eu3+ impurity on the antiferrodistortion and ferroelectric instabilities in an EuTiO3 bulk crystal and thin films journal, January 2015

Elastic and anelastic relaxations associated with phase transitions in EuTiO 3 journal, August 2014

Lattice instabilities in bulk EuTiO 3 journal, October 2013

An Antiferro-to-Ferromagnetic Transition in EuTiO 3– x H x Induced by Hydride Substitution journal, January 2015

Structural instability of EuTiO 3 from X-ray powder diffraction journal, November 2012

Reentrant Valence Transition in EuO at High Pressures: Beyond the Bond-Valence Model journal, July 2012

Nonlinear pressure dependence of T N in almost multiferroic EuTiO 3 journal, August 2013

Pressure-temperature phase diagram of SrTiO 3 up to 53 GPa journal, February 2010

Antiferrodistortive phase transition in EuTiO 3 journal, August 2012

Rare earth titanates with a perovskite structure journal, January 1953

Magnetoelastic relaxations in EuTiO 3 journal, March 2015

Hydrostatic limits of 11 pressure transmitting media journal, March 2009

X-ray study of the structural distortion in EuTiO3 journal, June 2014

Structure and thermoelectric properties of EuTi(O,N) 3 ± δ journal, July 2013

Emergent Superstructural Dynamic Order due to Competing Antiferroelectric and Antiferrodistortive Instabilities in Bulk EuTiO 3 journal, January 2013

DIOPTAS : a program for reduction of two-dimensional X-ray diffraction data and data exploration journal, May 2015

Studies of the antiferrodistortive transition in EuTiO 3 journal, November 2014

Hyperfine Splitting and Room-Temperature Ferromagnetism of Ni at Multimegabar Pressure journal, October 2013

Relation between structural instabilities in EuTiO 3 and SrTiO 3 journal, June 2011

Nuclear forward scattering by the 68.7 keV state of 73 Ge in CaGeO 3 and GeO 2 journal, October 2013

Role of intrinsic disorder in the structural phase transition of magnetoelectric EuTiO 3 journal, May 2012

Magnetic Properties of Some Divalent Europium Compounds journal, April 1963

Influence of the Oxygen Content on the Electronic Transport Properties of Sr x Eu 1– x TiO 3-δ journal, April 2014

Two-dimensional detector software: From real detector to idealised image or two-theta scan journal, January 1996

Nonlinear behavior of thin film SrTiO3 capacitors at microwave frequencies journal, September 1998

Phonon softening and dispersion in EuTiO 3 journal, December 2012

Nonlinear pressure dependence ofTNin almost multiferroic EuTiO3 text, January 2013

Reversible Control of Magnetic Interactions by Electric Field in a Single Phase Material text, January 2012

Nonlinear pressure dependence of T_N in almost multiferroic EuTiO_3 text, January 2013

Lattice instabilities in bulk EuTiO3 text, January 2013

Multicaloric effect in multiferroic EuTiO3 thin films journal, February 2020

Title: Pressure-mediated structural transitions in bulk ${EuTiO}_{3}$

Universality aspects of the metal-nonmetal transition in condensed media
journal, March 1978

Structural and magnetic phase transitions in ${EuTi}_{1 - x} {Nb}_{x} O_{3}$
journal, July 2015

Pressure-temperature phase diagram of multiferroic ${EuTiO}_{3}$
journal, August 2015

High pressure antiferrodistortive phase transition in mixed crystals of EuTiO ₃ and SrTiO ₃
journal, June 2016

Nuclear resonance scattering of synchrotron radiation at the 21.5 keV resonance of ¹⁵¹ Eu
journal, September 1996

X‐Ray Diffractometry of Low‐Temperature Phase Transformations in Strontium Titanate
journal, July 1964

Reversible control of magnetic interactions by electric field in a single-phase material
journal, January 2013

Effect of an Eu3+ impurity on the antiferrodistortion and ferroelectric instabilities in an EuTiO3 bulk crystal and thin films
journal, January 2015

Elastic and anelastic relaxations associated with phase transitions in ${EuTiO}_{3}$
journal, August 2014

Lattice instabilities in bulk EuTiO $_{3}$
journal, October 2013

An Antiferro-to-Ferromagnetic Transition in EuTiO _{3– x} H _x Induced by Hydride Substitution
journal, January 2015

Structural instability of EuTiO ₃ from X-ray powder diffraction
journal, November 2012

Reentrant Valence Transition in EuO at High Pressures: Beyond the Bond-Valence Model
journal, July 2012

Nonlinear pressure dependence of T _N in almost multiferroic EuTiO ₃
journal, August 2013

Pressure-temperature phase diagram of ${SrTiO}_{3}$ up to 53 GPa
journal, February 2010

Antiferrodistortive phase transition in EuTiO $_{3}$
journal, August 2012

Rare earth titanates with a perovskite structure
journal, January 1953

Magnetoelastic relaxations in EuTiO ₃
journal, March 2015

Hydrostatic limits of 11 pressure transmitting media
journal, March 2009

X-ray study of the structural distortion in EuTiO3
journal, June 2014

Structure and thermoelectric properties of EuTi(O,N) _3 ± _δ
journal, July 2013

Emergent Superstructural Dynamic Order due to Competing Antiferroelectric and Antiferrodistortive Instabilities in Bulk ${EuTiO}_{3}$
journal, January 2013

DIOPTAS : a program for reduction of two-dimensional X-ray diffraction data and data exploration
journal, May 2015

Studies of the antiferrodistortive transition in EuTiO ₃
journal, November 2014

Hyperfine Splitting and Room-Temperature Ferromagnetism of Ni at Multimegabar Pressure
journal, October 2013

Relation between structural instabilities in EuTiO $_{3}$ and SrTiO $_{3}$
journal, June 2011

Nuclear forward scattering by the 68.7 keV state of ⁷³ Ge in CaGeO ₃ and GeO ₂
journal, October 2013

Role of intrinsic disorder in the structural phase transition of magnetoelectric EuTiO $_{3}$
journal, May 2012

Magnetic Properties of Some Divalent Europium Compounds
journal, April 1963

Influence of the Oxygen Content on the Electronic Transport Properties of Sr _x Eu _{1– x} TiO _3-δ
journal, April 2014

Two-dimensional detector software: From real detector to idealised image or two-theta scan
journal, January 1996

Nonlinear behavior of thin film SrTiO3 capacitors at microwave frequencies
journal, September 1998

Phonon softening and dispersion in EuTiO $_{3}$
journal, December 2012

Nonlinear pressure dependence ofTNin almost multiferroic EuTiO3
text, January 2013

Reversible Control of Magnetic Interactions by Electric Field in a Single Phase Material
text, January 2012

Nonlinear pressure dependence of T_N in almost multiferroic EuTiO_3
text, January 2013

Lattice instabilities in bulk EuTiO3
text, January 2013

Multicaloric effect in multiferroic EuTiO3 thin films
journal, February 2020