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Title: Ultra-low blaze angle gratings for synchrotron and free electron laser applications

Abstract

We have developed a method for the manufacture of x-ray diffraction gratings with arbitrarily small blaze angles. These gratings are made by a process in which a high blaze angle grating made by anisotropic etching of Si (111) is subjected to planarization and reactive ion etching. Differential etching of the planarization medium and silicon ensures reduction of the blaze angle. Repeated application of this process leads to gratings of increasing perfection with an arbitrarily small blaze angle. This opens the way to highly efficient low line density gratings, to damage resistant gratings for ultra-high power applications such as free electron lasers, and for extension of the use of gratings into the hard x-ray energy range for dispersive spectroscopy.

Authors:
; ;
Publication Date:
Research Org.:
Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)
Sponsoring Org.:
USDOE Office of Science (SC), Basic Energy Sciences (BES)
OSTI Identifier:
1463933
Alternate Identifier(s):
OSTI ID: 1480808
Grant/Contract Number:  
AC02-05CH11231
Resource Type:
Published Article
Journal Name:
Optics Express
Additional Journal Information:
Journal Name: Optics Express Journal Volume: 26 Journal Issue: 17; Journal ID: ISSN 1094-4087
Publisher:
Optical Society of America
Country of Publication:
United States
Language:
English
Subject:
47 OTHER INSTRUMENTATION

Citation Formats

Voronov, D. L., Gullikson, E. M., and Padmore, H. A. Ultra-low blaze angle gratings for synchrotron and free electron laser applications. United States: N. p., 2018. Web. doi:10.1364/OE.26.022011.
Voronov, D. L., Gullikson, E. M., & Padmore, H. A. Ultra-low blaze angle gratings for synchrotron and free electron laser applications. United States. https://doi.org/10.1364/OE.26.022011
Voronov, D. L., Gullikson, E. M., and Padmore, H. A. Thu . "Ultra-low blaze angle gratings for synchrotron and free electron laser applications". United States. https://doi.org/10.1364/OE.26.022011.
@article{osti_1463933,
title = {Ultra-low blaze angle gratings for synchrotron and free electron laser applications},
author = {Voronov, D. L. and Gullikson, E. M. and Padmore, H. A.},
abstractNote = {We have developed a method for the manufacture of x-ray diffraction gratings with arbitrarily small blaze angles. These gratings are made by a process in which a high blaze angle grating made by anisotropic etching of Si (111) is subjected to planarization and reactive ion etching. Differential etching of the planarization medium and silicon ensures reduction of the blaze angle. Repeated application of this process leads to gratings of increasing perfection with an arbitrarily small blaze angle. This opens the way to highly efficient low line density gratings, to damage resistant gratings for ultra-high power applications such as free electron lasers, and for extension of the use of gratings into the hard x-ray energy range for dispersive spectroscopy.},
doi = {10.1364/OE.26.022011},
journal = {Optics Express},
number = 17,
volume = 26,
place = {United States},
year = {Thu Aug 09 00:00:00 EDT 2018},
month = {Thu Aug 09 00:00:00 EDT 2018}
}

Journal Article:
Free Publicly Available Full Text
Publisher's Version of Record
https://doi.org/10.1364/OE.26.022011

Citation Metrics:
Cited by: 10 works
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Works referenced in this record:

Gratings for synchrotron and FEL beamlines: a project for the manufacture of ultra-precise gratings at Helmholtz Zentrum Berlin
journal, January 2018


Refraction effects in soft x-ray multilayer blazed gratings
journal, January 2016

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Planarization during spin coating
journal, May 1992

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Investigating the interaction of x-ray free electron laser radiation with grating structure
journal, January 2012

  • Gaudin, Jérôme; Ozkan, Cigdem; Chalupský, Jaromír
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  • DOI: 10.1364/OL.37.003033

X-ray diffraction gratings: Precise control of ultra-low blaze angle via anisotropic wet etching
journal, July 2016

  • Voronov, Dmitriy L.; Lum, Paul; Naulleau, Patrick
  • Applied Physics Letters, Vol. 109, Issue 4
  • DOI: 10.1063/1.4960203

Fabrication and characterization of a new high density Sc/Si multilayer sliced grating
conference, August 2008

  • Voronov, Dmitriy L.; Cambie, Rossana; Gullikson, Eric M.
  • Optical Engineering + Applications, SPIE Proceedings
  • DOI: 10.1117/12.795377

Large area nanoimprint enables ultra-precise x-ray diffraction gratings
journal, January 2017

  • Voronov, D. L.; Gullikson, E. M.; Padmore, H. A.
  • Optics Express, Vol. 25, Issue 19
  • DOI: 10.1364/OE.25.023334

Towards 10 meV resolution: The design of an ultrahigh resolution soft X-ray RIXS spectrometer
journal, November 2016

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  • DOI: 10.1063/1.4964847

Development of coherent scattering and diffractive imaging and the COSMIC facility at the Advanced Light Source
journal, March 2013


Gratings with Blaze Angles Down to 0.1° for Photon Energies up to 10 keV
conference, January 2007

  • Heidemann, K. F.; Nelles, B.; Lenke, R.
  • SYNCHROTRON RADIATION INSTRUMENTATION: Ninth International Conference on Synchrotron Radiation Instrumentation, AIP Conference Proceedings
  • DOI: 10.1063/1.2436104

From Soft to Hard X-ray with a Single Grating Monochromator
conference, January 2007

  • Cocco, D.; Bianco, A.; Kaulich, B.
  • SYNCHROTRON RADIATION INSTRUMENTATION: Ninth International Conference on Synchrotron Radiation Instrumentation, AIP Conference Proceedings
  • DOI: 10.1063/1.2436107

Works referencing / citing this record:

On smart optimization of blazed soft X-ray gratings
journal, June 2019


On smart optimization of blazed soft X-ray gratings
journal, June 2019