Investigation of periodically driven systems by x-ray absorption spectroscopy using asynchronous data collection mode

Singh, H.; Donetsky, D.; Liu, J.; Attenkofer, K.; Cheng, B.; Trelewicz, J. R.; Lubomirsky, Igor; Stavitski, E.; Frenkel, A. I.

doi:10.1063/1.5000679

Title: Investigation of periodically driven systems by x-ray absorption spectroscopy using asynchronous data collection mode

Journal Article · 18 April 2018 · Review of Scientific Instruments

DOI: https://doi.org/10.1063/1.5000679 · OSTI ID:1460821

^[1]; Donetsky, D. ^[1];

^[1];

^[2]; Cheng, B. ^[1];

^[1]; Lubomirsky, Igor ^[3]; Stavitski, E. ^[2];

^[1]

Stony Brook Univ., Stony Brook, NY (United States)
Brookhaven National Lab. (BNL), Upton, NY (United States)
Weizmann Institute of Science, Rehovot (Israel)

Here, we report the development, testing, and demonstration of a setup for modulation excitation spectroscopy experiments at the Inner Shell Spectroscopy beamline of National Synchrotron Light Source - II. A computer algorithm and dedicated software were developed for asynchronous data processing and analysis. We demonstrate the reconstruction of X-ray absorption spectra for different time points within the modulation pulse using a model system. This setup and the software are intended for a broad range of functional materials which exhibit structural and/or electronic responses to the external stimulation, such as catalysts, energy and battery materials, and electromechanical devices.

View Accepted Manuscript (DOE)

View Accepted Manuscript (Publisher)

Cite

Export

Save

Research Organization:: Brookhaven National Laboratory (BNL), Upton, NY (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: SC0012704; AC02-98CH10886

OSTI ID:: 1460821

Alternate ID(s):: OSTI ID: 1433575

Report Number(s):: BNL-207845-2018-JAAM; TRN: US1901923

Journal Information:: Review of Scientific Instruments, Vol. 89, Issue 4; ISSN 0034-6748

Publisher:: American Institute of Physics (AIP)Copyright Statement

Country of Publication:: United States

Language:: English

Citation Metrics:

Cited by: 6 works

Citation information provided by
Web of Science

References (32)

Sensitivity enhancement and dynamic behavior analysis by modulation excitation spectroscopy: Principle and application in heterogeneous catalysis Urakawa, Atsushi; Bürgi, Thomas; Baiker, Alfons Chemical Engineering Science, Vol. 63, Issue 20 https://doi.org/10.1016/j.ces.2007.06.009	journal	October 2008
In-situ extended X-ray absorption fine structure study of electrostriction in Gd doped ceria Korobko, Roman; Lerner, Alyssa; Li, Yuanyuan Applied Physics Letters, Vol. 106, Issue 4 https://doi.org/10.1063/1.4906857	journal	January 2015
The extraction of signal to noise values in x‐ray absorption spectroscopy Dent, A. J.; Stephenson, P. C.; Greaves, G. N. Review of Scientific Instruments, Vol. 63, Issue 1 https://doi.org/10.1063/1.1142627	journal	January 1992
The ‘universal’ dielectric response Jonscher, A. K. Nature, Vol. 267, Issue 5613 https://doi.org/10.1038/267673a0	journal	June 1977
Synchrotron Techniques for In Situ Catalytic Studies: Capabilities, Challenges, and Opportunities Frenkel, Anatoly I.; Rodriguez, Jose A.; Chen, Jingguang G. ACS Catalysis, Vol. 2, Issue 11 https://doi.org/10.1021/cs3004006	journal	September 2012
Electromechanical properties of electrostrictive CeO ₂ :Gd membranes: Effects of frequency and temperature Ushakov, A. D.; Mishuk, E.; Makagon, E. Applied Physics Letters, Vol. 110, Issue 14 https://doi.org/10.1063/1.4979642	journal	April 2017
Applications of Modulation Excitation Spectroscopy in Heterogeneous Catalysis Müller, Philipp; Hermans, Ive Industrial & Engineering Chemistry Research, Vol. 56, Issue 5 https://doi.org/10.1021/acs.iecr.6b04855	journal	January 2017
Quantitative modulated excitation Fourier transform infrared spectroscopy Baurecht, Dieter; Fringeli, Urs Peter Review of Scientific Instruments, Vol. 72, Issue 10 https://doi.org/10.1063/1.1400152	journal	October 2001
First steps in combining modulation excitation spectroscopy with synchronous dispersive EXAFS/DRIFTS/mass spectrometry for in situ time resolved study of heterogeneous catalysts Ferri, Davide; Kumar, M. Santosh; Wirz, Ronny Physical Chemistry Chemical Physics, Vol. 12, Issue 21 https://doi.org/10.1039/b926886c	journal	January 2010
Electric-field-induced local and mesoscale structural changes in polycrystalline dielectrics and ferroelectrics Usher, Tedi-Marie; Levin, Igor; Daniels, John E. Scientific Reports, Vol. 5, Issue 1 https://doi.org/10.1038/srep14678	journal	October 2015
Emittance and lifetime measurement with damping wigglers Wang, G. M.; Shaftan, T.; Cheng, W. X. Review of Scientific Instruments, Vol. 87, Issue 3 https://doi.org/10.1063/1.4942903	journal	March 2016
A Review on the Structural Studies of Batteries and Host Materials by X-Ray Absorption Spectroscopy Giorgetti, Marco ISRN Materials Science, Vol. 2013 https://doi.org/10.1155/2013/938625	journal	January 2013
Modulation Excitation X-Ray Absorption Spectroscopy to Probe Surface Species on Heterogeneous Catalysts Ferri, Davide; Newton, Mark A.; Nachtegaal, Maarten Topics in Catalysis, Vol. 54, Issue 16-18 https://doi.org/10.1007/s11244-011-9727-5	journal	August 2011
Modeling the Structure and Composition of Nanoparticles by Extended X-Ray Absorption Fine-Structure Spectroscopy Frenkel, Anatoly I.; Yevick, Aaron; Cooper, Chana Annual Review of Analytical Chemistry, Vol. 4, Issue 1 https://doi.org/10.1146/annurev-anchem-061010-113906	journal	July 2011
Modulated excitation extended X-ray absorption fine structure spectroscopy Chiarello, Gian Luca; Ferri, Davide Physical Chemistry Chemical Physics, Vol. 17, Issue 16 https://doi.org/10.1039/c5cp00609k	journal	January 2015
Differential EXAFS analysis using DEXA Ruffoni, M. P. Journal of Synchrotron Radiation, Vol. 16, Issue 4 https://doi.org/10.1107/s0909049509019839	journal	May 2009
Dielectric relaxation in solids Jonscher, Andrew K. Journal of Physics D: Applied Physics, Vol. 32, Issue 14 https://doi.org/10.1088/0022-3727/32/14/201	journal	January 1999
Measurement of femtometre-scale atomic displacements by X-ray absorption spectroscopy Pettifer, Robert F.; Mathon, Olivier; Pascarelli, Sakura Nature, Vol. 435, Issue 7038 https://doi.org/10.1038/nature03516	journal	May 2005
Dynamic in situ observation of rapid size and shape change of supported Pd nanoparticles during CO/NO cycling Newton, Mark A.; Belver-Coldeira, Carolina; Martínez-Arias, Arturo Nature Materials, Vol. 6, Issue 7 https://doi.org/10.1038/nmat1924	journal	May 2007
Kinetic analysis using square-wave stimulation in modulation excitation spectroscopy: Mixing property of a flow-through PM-IRRAS cell Urakawa, Atsushi; Bürgi, Thomas; Baiker, Alfons Chemical Physics, Vol. 324, Issue 2-3 https://doi.org/10.1016/j.chemphys.2005.12.009	journal	May 2006
Geometry of electromechanically active structures in Gadolinium - doped Cerium oxides Li, Yuanyuan; Kraynis, Olga; Kas, Joshua AIP Advances, Vol. 6, Issue 5 https://doi.org/10.1063/1.4952645	journal	May 2016
Quantitative Analysis of Modulated Excitation X-ray Absorption Spectra: Enhanced Precision of EXAFS Fitting König, Christian F. J.; van Bokhoven, Jeroen A.; Schildhauer, Tilman J. The Journal of Physical Chemistry C, Vol. 116, Issue 37 https://doi.org/10.1021/jp306022k	journal	September 2012
Development of light-modulated XAFS spectroscopy Okamoto, Kaoru; Kohdate, Kenji; Nagai, Kensuke Journal of Synchrotron Radiation, Vol. 10, Issue 3 https://doi.org/10.1107/s0909049503004321	journal	April 2003
Methane synthesis and sulfur removal over a Ru catalyst probed in situ with high sensitivity X-ray absorption spectroscopy König, Christian F. J.; Schildhauer, Tilman J.; Nachtegaal, Maarten Journal of Catalysis, Vol. 305 https://doi.org/10.1016/j.jcat.2013.05.002	journal	September 2013
Subsecond and in Situ Chemical Speciation of Pt/Al ₂ O ₃ during Oxidation–Reduction Cycles Monitored by High-Energy Resolution Off-Resonant X-ray Spectroscopy Szlachetko, Jakub; Ferri, Davide; Marchionni, Valentina Journal of the American Chemical Society, Vol. 135, Issue 51 https://doi.org/10.1021/ja410146c	journal	December 2013
Local Structure and Strain-Induced Distortion in Ce0.8Gd0.2O1.9 Kossoy, Anna; Frenkel, Anatoly I.; Wang, Qi Advanced Materials, Vol. 22, Issue 14 https://doi.org/10.1002/adma.200902041	journal	January 2010
Time Resolved Operando X-ray Techniques in Catalysis, a Case Study: CO Oxidation by O2 over Pt Surfaces and Alumina Supported Pt Catalysts Newton, Mark Catalysts, Vol. 7, Issue 12 https://doi.org/10.3390/catal7020058	journal	February 2017
Emerging operando and x-ray pair distribution function methods for energy materials development Chapman, Karena W. MRS Bulletin, Vol. 41, Issue 3 https://doi.org/10.1557/mrs.2016.26	journal	March 2016
Giant Electrostriction in Gd-Doped Ceria Korobko, Roman; Patlolla, Anitha; Kossoy, Anna Advanced Materials, Vol. 24, Issue 43 https://doi.org/10.1002/adma.201202270	journal	August 2012
Dielectric relaxation in solids Henisch, H. K. Materials Research Bulletin, Vol. 19, Issue 1 https://doi.org/10.1016/0025-5408(84)90019-9	journal	January 1984
The universal dielectric response Jonscher, A. K. Annual Conference on Electrical Insulation and Dielectric Phenomena https://doi.org/10.1109/ceidp.1990.201316	conference	January 1990
Dielectric relaxation in solids Calderwood, James Journal of Electrostatics, Vol. 18, Issue 3 https://doi.org/10.1016/0304-3886(86)90028-8	journal	October 1986

Cited By (1)

A review of defect structure and chemistry in ceria and its solid solutions Schmitt, Rafael; Nenning, Andreas; Kraynis, Olga ETH Zurich https://doi.org/10.3929/ethz-b-000396556	text	January 2020