DOE PAGES title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Simultaneous 8.2 keV phase-contrast imaging and 24.6 keV X-ray diffraction from shock-compressed matter at the LCLS

Abstract

In this paper, we demonstrate simultaneous phase-contrast imaging (PCI) and X-ray diffraction from shock compressed matter at the Matter in Extreme Conditions endstation, at the Linac Coherent Light Source (LCLS). We utilize the chromaticity from compound refractive X-ray lenses to focus the 24.6 keV 3rd order undulator harmonic of the LCLS to a spot size of 5 μm on target to perform X-ray diffraction. Simultaneous PCI from the 8.2 keV fundamental X-ray beam is used to visualize and measure the transient properties of the shock wave over a 500 μm field of view. Furthermore, we demonstrate the ability to extend the reciprocal space measurements by 5 Å–1, relative to the fundamental X-ray energy, by utilizing X-ray diffraction from the 3rd harmonic of the LCLS.

Authors:
ORCiD logo [1];  [2];  [3];  [4]; ORCiD logo [5];  [2];  [2];  [6];  [7];  [2];  [2]; ORCiD logo [8];  [2];  [2];  [8];  [9];  [10]; ORCiD logo [11]; ORCiD logo [2];  [3] more »;  [2]; ORCiD logo [2]; ORCiD logo [12] « less
  1. SLAC National Accelerator Lab., Menlo Park, CA (United States); Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany)
  2. SLAC National Accelerator Lab., Menlo Park, CA (United States)
  3. Univ. of Oxford, Oxford (United Kingdom)
  4. Diamond Light Source Ltd., Didcot (United Kingdom)
  5. Massachusetts Inst. of Technology (MIT), Cambridge, MA (United States)
  6. European XFEL GmbH, Schenefeld (Germany)
  7. Sorbonne Univ., Paris (France)
  8. Osaka Univ., Osaka (Japan)
  9. Helmholtz-Zentrum Dresden-Rossendorf, Dresden (Germany); Technische Univ. Dresden, Dresden (Germany)
  10. Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany)
  11. STFC, Rutherford Appleton Lab., Didcot (United Kingdom)
  12. SLAC National Accelerator Lab., Menlo Park, CA (United States); European XFEL GmbH, Schenefeld (Germany)
Publication Date:
Research Org.:
SLAC National Accelerator Lab., Menlo Park, CA (United States)
Sponsoring Org.:
USDOE Office of Science (SC), Fusion Energy Sciences (FES)
OSTI Identifier:
1458529
Alternate Identifier(s):
OSTI ID: 1439909
Grant/Contract Number:  
SF00515; 05K13OD2; 12-PDOC-0011; EP/J017256/1; AC02-76SF00515; FWP100182
Resource Type:
Accepted Manuscript
Journal Name:
Applied Physics Letters
Additional Journal Information:
Journal Volume: 112; Journal Issue: 22; Journal ID: ISSN 0003-6951
Publisher:
American Institute of Physics (AIP)
Country of Publication:
United States
Language:
English
Subject:
71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSICS

Citation Formats

Seiboth, F., Fletcher, L. B., McGonegle, D., Anzellini, S., Dresselhaus-Cooper, L. E., Frost, M., Galtier, E., Goede, S., Harmand, M., Lee, H. J., Levitan, A. L., Miyanishi, K., Nagler, B., Nam, I., Ozaki, N., Rodel, M., Schropp, A., Spindloe, C., Sun, P., Wark, J. S., Hastings, J., Glenzer, S. H., and McBride, E. E. Simultaneous 8.2 keV phase-contrast imaging and 24.6 keV X-ray diffraction from shock-compressed matter at the LCLS. United States: N. p., 2018. Web. doi:10.1063/1.5031907.
Seiboth, F., Fletcher, L. B., McGonegle, D., Anzellini, S., Dresselhaus-Cooper, L. E., Frost, M., Galtier, E., Goede, S., Harmand, M., Lee, H. J., Levitan, A. L., Miyanishi, K., Nagler, B., Nam, I., Ozaki, N., Rodel, M., Schropp, A., Spindloe, C., Sun, P., Wark, J. S., Hastings, J., Glenzer, S. H., & McBride, E. E. Simultaneous 8.2 keV phase-contrast imaging and 24.6 keV X-ray diffraction from shock-compressed matter at the LCLS. United States. https://doi.org/10.1063/1.5031907
Seiboth, F., Fletcher, L. B., McGonegle, D., Anzellini, S., Dresselhaus-Cooper, L. E., Frost, M., Galtier, E., Goede, S., Harmand, M., Lee, H. J., Levitan, A. L., Miyanishi, K., Nagler, B., Nam, I., Ozaki, N., Rodel, M., Schropp, A., Spindloe, C., Sun, P., Wark, J. S., Hastings, J., Glenzer, S. H., and McBride, E. E. Mon . "Simultaneous 8.2 keV phase-contrast imaging and 24.6 keV X-ray diffraction from shock-compressed matter at the LCLS". United States. https://doi.org/10.1063/1.5031907. https://www.osti.gov/servlets/purl/1458529.
@article{osti_1458529,
title = {Simultaneous 8.2 keV phase-contrast imaging and 24.6 keV X-ray diffraction from shock-compressed matter at the LCLS},
author = {Seiboth, F. and Fletcher, L. B. and McGonegle, D. and Anzellini, S. and Dresselhaus-Cooper, L. E. and Frost, M. and Galtier, E. and Goede, S. and Harmand, M. and Lee, H. J. and Levitan, A. L. and Miyanishi, K. and Nagler, B. and Nam, I. and Ozaki, N. and Rodel, M. and Schropp, A. and Spindloe, C. and Sun, P. and Wark, J. S. and Hastings, J. and Glenzer, S. H. and McBride, E. E.},
abstractNote = {In this paper, we demonstrate simultaneous phase-contrast imaging (PCI) and X-ray diffraction from shock compressed matter at the Matter in Extreme Conditions endstation, at the Linac Coherent Light Source (LCLS). We utilize the chromaticity from compound refractive X-ray lenses to focus the 24.6 keV 3rd order undulator harmonic of the LCLS to a spot size of 5 μm on target to perform X-ray diffraction. Simultaneous PCI from the 8.2 keV fundamental X-ray beam is used to visualize and measure the transient properties of the shock wave over a 500 μm field of view. Furthermore, we demonstrate the ability to extend the reciprocal space measurements by 5 Å–1, relative to the fundamental X-ray energy, by utilizing X-ray diffraction from the 3rd harmonic of the LCLS.},
doi = {10.1063/1.5031907},
journal = {Applied Physics Letters},
number = 22,
volume = 112,
place = {United States},
year = {Mon May 28 00:00:00 EDT 2018},
month = {Mon May 28 00:00:00 EDT 2018}
}

Journal Article:
Free Publicly Available Full Text
Publisher's Version of Record

Citation Metrics:
Cited by: 16 works
Citation information provided by
Web of Science

Figures / Tables:

FIG. 1 FIG. 1: Experimental setup for simultaneous phase-contrast imaging and X-ray diffraction from shock-compressed matter. The X-ray beam is perpendicular to the optical pump laser used to generate the shock wave in the multi-layer target near the focal place of the 3rd harmonic beam.

Save / Share:

Works referenced in this record:

Development of a broadband reflectivity diagnostic for laser driven shock compression experiments
journal, April 2015

  • Ali, S. J.; Bolme, C. A.; Collins, G. W.
  • Review of Scientific Instruments, Vol. 86, Issue 4
  • DOI: 10.1063/1.4917195

Symmetric Inertial Confinement Fusion Implosions at Ultra-High Laser Energies
journal, January 2010


In situ X-ray diffraction measurement of shock-wave-driven twinning and lattice dynamics
journal, October 2017

  • Wehrenberg, C. E.; McGonegle, D.; Bolme, C.
  • Nature, Vol. 550, Issue 7677
  • DOI: 10.1038/nature24061

Simulational analysis of the local structure in liquid germanium under pressure
journal, August 2002


Formation of diamonds in laser-compressed hydrocarbons at planetary interior conditions
journal, August 2017


The Matter in Extreme Conditions instrument at the Linac Coherent Light Source
journal, April 2015

  • Nagler, Bob; Arnold, Brice; Bouchard, Gary
  • Journal of Synchrotron Radiation, Vol. 22, Issue 3
  • DOI: 10.1107/S1600577515004865

Imaging Shock Waves in Diamond with Both High Temporal and Spatial Resolution at an XFEL
journal, June 2015

  • Schropp, Andreas; Hoppe, Robert; Meier, Vivienne
  • Scientific Reports, Vol. 5, Issue 1
  • DOI: 10.1038/srep11089

Laser interferometer for measuring high velocities of any reflecting surface
journal, November 1972

  • Barker, L. M.; Hollenbach, R. E.
  • Journal of Applied Physics, Vol. 43, Issue 11
  • DOI: 10.1063/1.1660986

Kinoform phase plates for focal plane irradiance profile control
journal, January 1994

  • Dixit, S. N.; Nugent, K. A.; Lawson, J. K.
  • Optics Letters, Vol. 19, Issue 6
  • DOI: 10.1364/OL.19.000417

Imaging by parabolic refractive lenses in the hard X-ray range
journal, November 1999

  • Lengeler, Bruno; Schroer, Christian; Tümmler, Johannes
  • Journal of Synchrotron Radiation, Vol. 6, Issue 6
  • DOI: 10.1107/S0909049599009747

Ultrafast X-Ray Diffraction Studies of the Phase Transitions and Equation of State of Scandium Shock Compressed to 82 GPa
journal, January 2017


Axial yield strengths and phase‐transition stresses for 〈100〉, 〈110〉, and 〈111〉 germanium
journal, November 1972

  • Gust, W. H.; Royce, E. B.
  • Journal of Applied Physics, Vol. 43, Issue 11
  • DOI: 10.1063/1.1660940

Time-resolved diffraction of shock-released SiO2 and diaplectic glass formation
journal, November 2017


Nanosecond formation of diamond and lonsdaleite by shock compression of graphite
journal, March 2016

  • Kraus, D.; Ravasio, A.; Gauthier, M.
  • Nature Communications, Vol. 7, Issue 1
  • DOI: 10.1038/ncomms10970

The phase-contrast imaging instrument at the matter in extreme conditions endstation at LCLS
journal, October 2016

  • Nagler, Bob; Schropp, Andreas; Galtier, Eric C.
  • Review of Scientific Instruments, Vol. 87, Issue 10
  • DOI: 10.1063/1.4963906

Ultrabright X-ray laser scattering for dynamic warm dense matter physics
journal, March 2015


Ultrafast visualization of crystallization and grain growth in shock-compressed SiO2
journal, September 2015

  • Gleason, A. E.; Bolme, C. A.; Lee, H. J.
  • Nature Communications, Vol. 6, Issue 1
  • DOI: 10.1038/ncomms9191

Direct Observation of Melting in Shock-Compressed Bismuth With Femtosecond X-ray Diffraction
journal, August 2015


Physical behavior of germanium under shock wave compression
journal, September 1966

  • Graham, R. A.; Jones, O. E.; Holland, J. R.
  • Journal of Physics and Chemistry of Solids, Vol. 27, Issue 9
  • DOI: 10.1016/0022-3697(66)90147-8

The phase-contrast imaging instrument at the matter in extreme conditions endstation at LCLS
text, January 2016

  • Nagler, Bob; Schropp, Andreas; Galtier, Eric C.
  • Deutsches Elektronen-Synchrotron, DESY, Hamburg
  • DOI: 10.3204/pubdb-2016-05564

Physical behavior of germanium under shock wave compression
journal, May 1966


Erratum: Ultrafast visualization of crystallization and grain growth in shock-compressed SiO2
journal, October 2015

  • Gleason, A. E.; Bolme, C. A.; Lee, H. J.
  • Nature Communications, Vol. 6, Issue 1
  • DOI: 10.1038/ncomms9709

The Phase-Contrast Imaging Instrument at the Matter in Extreme Conditions Endstation at LCLS
text, January 2016


Works referencing / citing this record:

Single-Shot Multi-Frame Imaging of Cylindrical Shock Waves in a Multi-Layered Assembly
journal, March 2019

  • Dresselhaus-Cooper, Leora; Gorfain, Joshua E.; Key, Chris T.
  • Scientific Reports, Vol. 9, Issue 1
  • DOI: 10.1038/s41598-019-40037-3

Visualization of ultrafast melting initiated from radiation-driven defects in solids
journal, May 2019


Figures/Tables have been extracted from DOE-funded journal article accepted manuscripts.