skip to main content

DOE PAGESDOE PAGES

This content will become publicly available on April 30, 2019

Title: Spatially resolved texture and microstructure evolution of additively manufactured and gas gun deformed 304L stainless steel investigated by neutron diffraction and electron backscatter diffraction

In this study, we report the characterization of a 304L stainless steel cylindrical projectile produced by additive manufacturing. The projectile was compressively deformed using a Taylor Anvil Gas Gun, leading to a huge strain gradient along the axis of the deformed cylinder. Spatially resolved neutron diffraction measurements on the HIgh Pressure Preferred Orientation time-of-flight diffractometer (HIPPO) and Spectrometer for Materials Research at Temperature and Stress diffractometer (SMARTS) beamlines at the Los Alamos Neutron Science CEnter (LANSCE) with Rietveld and single-peak analysis were used to quantitatively evaluate the volume fractions of the α, γ, and ε phases as well as residual strain and texture. The texture of the γ phase is consistent with uniaxial compression, while the α texture can be explained by the Kurdjumov–Sachs relationship from the γ texture after deformation. This indicates that the material first deformed in the γ phase and subsequently transformed at larger strains. The ε phase was only found in volumes close to the undeformed material with a texture connected to the γ texture by the Shoji–Nishiyama orientation relationship. This allows us to conclude that the ε phase occurs as an intermediate phase at lower strain, and is superseded by the α phase when strainmore » increases further. We found a proportionality between the root-mean-squared microstrain of the γ phase, dominated by the dislocation density, with the α volume fraction, consistent with strain-induced martensite α formation. In conclusion, knowledge of the sample volume with the ε phase from the neutron diffraction analysis allowed us to identify the ε phase by electron back scatter diffraction analysis, complementing the neutron diffraction analysis with characterization on the grain level.« less
Authors:
 [1] ; ORCiD logo [2] ; ORCiD logo [2] ; ORCiD logo [2] ; ORCiD logo [2] ;  [2] ;  [2] ; ORCiD logo [2]
  1. Los Alamos National Lab. (LANL), Los Alamos, NM (United States); JFE Steel Corporation, Kurashiki (Japan)
  2. Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
Publication Date:
Report Number(s):
LA-UR-17-25178
Journal ID: ISSN 0885-7156; applab
Grant/Contract Number:
AC52-06NA25396
Type:
Accepted Manuscript
Journal Name:
Powder Diffraction
Additional Journal Information:
Conference: Denver X-ray conference, Big sky, MN (United States), 31 Jul - 04 Aug 2017; Journal ID: ISSN 0885-7156
Publisher:
Cambridge University Press
Research Org:
Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
Sponsoring Org:
USDOE National Nuclear Security Administration (NNSA)
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE
OSTI Identifier:
1440473

Takajo, Shigehiro, Brown, Donald William, Clausen, Bjorn, Gray, George Thompson III, Knapp, Cameron M., Martinez, Daniel Tito, Trujillo, Carl Patrick, and Vogel, Sven C.. Spatially resolved texture and microstructure evolution of additively manufactured and gas gun deformed 304L stainless steel investigated by neutron diffraction and electron backscatter diffraction. United States: N. p., Web. doi:10.1017/S0885715618000350.
Takajo, Shigehiro, Brown, Donald William, Clausen, Bjorn, Gray, George Thompson III, Knapp, Cameron M., Martinez, Daniel Tito, Trujillo, Carl Patrick, & Vogel, Sven C.. Spatially resolved texture and microstructure evolution of additively manufactured and gas gun deformed 304L stainless steel investigated by neutron diffraction and electron backscatter diffraction. United States. doi:10.1017/S0885715618000350.
Takajo, Shigehiro, Brown, Donald William, Clausen, Bjorn, Gray, George Thompson III, Knapp, Cameron M., Martinez, Daniel Tito, Trujillo, Carl Patrick, and Vogel, Sven C.. 2018. "Spatially resolved texture and microstructure evolution of additively manufactured and gas gun deformed 304L stainless steel investigated by neutron diffraction and electron backscatter diffraction". United States. doi:10.1017/S0885715618000350.
@article{osti_1440473,
title = {Spatially resolved texture and microstructure evolution of additively manufactured and gas gun deformed 304L stainless steel investigated by neutron diffraction and electron backscatter diffraction},
author = {Takajo, Shigehiro and Brown, Donald William and Clausen, Bjorn and Gray, George Thompson III and Knapp, Cameron M. and Martinez, Daniel Tito and Trujillo, Carl Patrick and Vogel, Sven C.},
abstractNote = {In this study, we report the characterization of a 304L stainless steel cylindrical projectile produced by additive manufacturing. The projectile was compressively deformed using a Taylor Anvil Gas Gun, leading to a huge strain gradient along the axis of the deformed cylinder. Spatially resolved neutron diffraction measurements on the HIgh Pressure Preferred Orientation time-of-flight diffractometer (HIPPO) and Spectrometer for Materials Research at Temperature and Stress diffractometer (SMARTS) beamlines at the Los Alamos Neutron Science CEnter (LANSCE) with Rietveld and single-peak analysis were used to quantitatively evaluate the volume fractions of the α, γ, and ε phases as well as residual strain and texture. The texture of the γ phase is consistent with uniaxial compression, while the α texture can be explained by the Kurdjumov–Sachs relationship from the γ texture after deformation. This indicates that the material first deformed in the γ phase and subsequently transformed at larger strains. The ε phase was only found in volumes close to the undeformed material with a texture connected to the γ texture by the Shoji–Nishiyama orientation relationship. This allows us to conclude that the ε phase occurs as an intermediate phase at lower strain, and is superseded by the α phase when strain increases further. We found a proportionality between the root-mean-squared microstrain of the γ phase, dominated by the dislocation density, with the α volume fraction, consistent with strain-induced martensite α formation. In conclusion, knowledge of the sample volume with the ε phase from the neutron diffraction analysis allowed us to identify the ε phase by electron back scatter diffraction analysis, complementing the neutron diffraction analysis with characterization on the grain level.},
doi = {10.1017/S0885715618000350},
journal = {Powder Diffraction},
number = ,
volume = ,
place = {United States},
year = {2018},
month = {4}
}

Works referenced in this record:

A profile refinement method for nuclear and magnetic structures
journal, June 1969