Bragg coherent diffractive imaging of ferromagnetic nickel nanoparticles
Abstract
We synthesized Ni nanoparticles with an atmospheric-thermal chemical vapor deposition method and investigated their lattice distortions and defects using Bragg coherent diffractive imaging. Because the strain can alter the magnetic properties of ferromagnetic materials, it is important to study the lattice distortion and structural imperfection. As a result of the Bragg coherent diffractive imaging, we found that the Ni nanocubes have a deformation-free zone in the middle. In addition, the defects such as dislocation and twin domain defects were detected in other Ni nanoparticles based on the Bragg diffraction images and patterns. The imaging of nanoparticles can contribute to a better understanding of their growth mechanisms and improve the design and synthesis of nanoparticles.
- Authors:
-
[1];
- Argonne National Lab. (ANL), Argonne, IL (United States); Univ. of California, San Diego, CA (United States)
- Univ. of California, San Diego, CA (United States)
- Argonne National Lab. (ANL), Argonne, IL (United States)
- Publication Date:
- Research Org.:
- Argonne National Lab. (ANL), Argonne, IL (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES)
- OSTI Identifier:
- 1474148
- Alternate Identifier(s):
- OSTI ID: 1438953
- Grant/Contract Number:
- AC02-06CH11357; SC0001805
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Journal of Applied Physics
- Additional Journal Information:
- Journal Volume: 123; Journal Issue: 20; Journal ID: ISSN 0021-8979
- Publisher:
- American Institute of Physics (AIP)
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 74 ATOMIC AND MOLECULAR PHYSICS
Citation Formats
Kim, J. W., Manna, S., Harder, R., Wingert, J., Fullerton, E. E., and Shpyrko, O. G. Bragg coherent diffractive imaging of ferromagnetic nickel nanoparticles. United States: N. p., 2018.
Web. doi:10.1063/1.5022328.
Kim, J. W., Manna, S., Harder, R., Wingert, J., Fullerton, E. E., & Shpyrko, O. G. Bragg coherent diffractive imaging of ferromagnetic nickel nanoparticles. United States. https://doi.org/10.1063/1.5022328
Kim, J. W., Manna, S., Harder, R., Wingert, J., Fullerton, E. E., and Shpyrko, O. G. Thu .
"Bragg coherent diffractive imaging of ferromagnetic nickel nanoparticles". United States. https://doi.org/10.1063/1.5022328. https://www.osti.gov/servlets/purl/1474148.
@article{osti_1474148,
title = {Bragg coherent diffractive imaging of ferromagnetic nickel nanoparticles},
author = {Kim, J. W. and Manna, S. and Harder, R. and Wingert, J. and Fullerton, E. E. and Shpyrko, O. G.},
abstractNote = {We synthesized Ni nanoparticles with an atmospheric-thermal chemical vapor deposition method and investigated their lattice distortions and defects using Bragg coherent diffractive imaging. Because the strain can alter the magnetic properties of ferromagnetic materials, it is important to study the lattice distortion and structural imperfection. As a result of the Bragg coherent diffractive imaging, we found that the Ni nanocubes have a deformation-free zone in the middle. In addition, the defects such as dislocation and twin domain defects were detected in other Ni nanoparticles based on the Bragg diffraction images and patterns. The imaging of nanoparticles can contribute to a better understanding of their growth mechanisms and improve the design and synthesis of nanoparticles.},
doi = {10.1063/1.5022328},
journal = {Journal of Applied Physics},
number = 20,
volume = 123,
place = {United States},
year = {Thu May 24 00:00:00 EDT 2018},
month = {Thu May 24 00:00:00 EDT 2018}
}
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Figures / Tables:
Figure 1: (a) Schematic of experimental setup with SEM image of Nickel nanocube. (b) 3D isosurface of the diffraction intensity. (c) 3D rendering of reconstructed Ni nanocube in which the color represents the phase. (d) Three cross-sections of reconstructed nanocube parallel to the substrate.
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