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Title: Characterization of a quadrant diamond transmission X-ray detector including a precise determination of the mean electron–hole pair creation energy

Abstract

Precise monitoring of the incoming photon flux is crucial for many experiments using synchrotron radiation. For photon energies above a few keV, thin semiconductor photodiodes can be operated in transmission for this purpose. Diamond is a particularly attractive material as a result of its low absorption. The responsivity of a state-of-the art diamond quadrant transmission detector has been determined, with relative uncertainties below 1% by direct calibration against an electrical substitution radiometer. From these data and the measured transmittance, the thickness of the involved layers as well as the mean electron–hole pair creation energy were determined, the latter with an unprecedented relative uncertainty of 1%. Lastly, the linearity and X-ray scattering properties of the device are also described.

Authors:
ORCiD logo [1];  [2];  [2]; ORCiD logo [2]
+ Show Author Affiliations
  1. Brookhaven National Lab. (BNL), Upton, NY (United States). National Synchrotron Light Source II (NSLS-II)
  2. Physikalisch-Technische Bundesanstalt (PTB), Berlin (Germany)
Publication Date:
Research Org.:
Brookhaven National Lab. (BNL), Upton, NY (United States)
Sponsoring Org.:
USDOE Office of Science (SC), Basic Energy Sciences (BES)
OSTI Identifier:
1433988
Report Number(s):
BNL-203530-2018-JAAM
Journal ID: ISSN 1600-5775; JSYRES; TRN: US1802668
Grant/Contract Number:  
SC0012704
Resource Type:
Accepted Manuscript
Journal Name:
Journal of Synchrotron Radiation (Online)
Additional Journal Information:
Journal Name: Journal of Synchrotron Radiation (Online); Journal Volume: 25; Journal Issue: 2; Journal ID: ISSN 1600-5775
Publisher:
International Union of Crystallography
Country of Publication:
United States
Language:
English
Subject:
47 OTHER INSTRUMENTATION; X-ray; detectors; diamond; calibration; scattering; quadrant diamond transmission X-ray detector

Citation Formats

Keister, Jeffrey W., Cibik, Levent, Schreiber, Swenja, and Krumrey, Michael. Characterization of a quadrant diamond transmission X-ray detector including a precise determination of the mean electron–hole pair creation energy. United States: N. p., 2018. Web. doi:10.1107/S1600577517017659.
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Keister, Jeffrey W., Cibik, Levent, Schreiber, Swenja, & Krumrey, Michael. Characterization of a quadrant diamond transmission X-ray detector including a precise determination of the mean electron–hole pair creation energy. United States. https://doi.org/10.1107/S1600577517017659
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Keister, Jeffrey W., Cibik, Levent, Schreiber, Swenja, and Krumrey, Michael. Tue . "Characterization of a quadrant diamond transmission X-ray detector including a precise determination of the mean electron–hole pair creation energy". United States. https://doi.org/10.1107/S1600577517017659. https://www.osti.gov/servlets/purl/1433988.
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@article{osti_1433988,
title = {Characterization of a quadrant diamond transmission X-ray detector including a precise determination of the mean electron–hole pair creation energy},
author = {Keister, Jeffrey W. and Cibik, Levent and Schreiber, Swenja and Krumrey, Michael},
abstractNote = {Precise monitoring of the incoming photon flux is crucial for many experiments using synchrotron radiation. For photon energies above a few keV, thin semiconductor photodiodes can be operated in transmission for this purpose. Diamond is a particularly attractive material as a result of its low absorption. The responsivity of a state-of-the art diamond quadrant transmission detector has been determined, with relative uncertainties below 1% by direct calibration against an electrical substitution radiometer. From these data and the measured transmittance, the thickness of the involved layers as well as the mean electron–hole pair creation energy were determined, the latter with an unprecedented relative uncertainty of 1%. Lastly, the linearity and X-ray scattering properties of the device are also described.},
doi = {10.1107/S1600577517017659},
journal = {Journal of Synchrotron Radiation (Online)},
number = 2,
volume = 25,
place = {United States},
year = {Tue Feb 20 00:00:00 EST 2018},
month = {Tue Feb 20 00:00:00 EST 2018}
}
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Journal Article:
Free Publicly Available Full Text
Publisher's Version of Record
https://doi.org/10.1107/S1600577517017659
Copyright Statement
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Citation Metrics:
Cited by: 4 works
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Figures / Tables:

Figure 1 Figure 1: Photon cross sections for platinum (electrical surface contacts) and carbon (diamond sensor) from the literature (Berger et al., 2010; Hubbell & Seltzer, 2004). The Pt M absorption edges above 2 keV are clearly visible.
All figures and tables (7 total)
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Works referenced in this record:

A quarter-century of metrology using synchrotron radiation by PTB in Berlin
journal, July 2009

  • Beckhoff, Burkhard; Gottwald, Alexander; Klein, Roman
  • physica status solidi (b), Vol. 246, Issue 7
  • DOI: 10.1002/pssb.200945162

Thin Transmission Photodiodes as Monitor Detectors in the X-ray Range
conference, January 2007

  • Krumrey, Michael; Gerlach, Martin; Hoffmann, Michael
  • SYNCHROTRON RADIATION INSTRUMENTATION: Ninth International Conference on Synchrotron Radiation Instrumentation, AIP Conference Proceedings
  • DOI: 10.1063/1.2436266

10μm thin transmissive photodiode produced by ALBA Synchrotron and IMB-CNM-CSIC
journal, March 2015

Towards traceable size determination of extracellular vesicles
journal, January 2014

  • Varga, Zoltán; Yuana, Yuana; Grootemaat, Anita E.
  • Journal of Extracellular Vesicles, Vol. 3, Issue 1
  • DOI: 10.3402/jev.v3.23298

Single crystal diamond photodiode for soft X-ray radiometry
journal, July 2009

  • Keister, Jeffrey W.; Smedley, John
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 606, Issue 3
  • DOI: 10.1016/j.nima.2009.04.044

Review of photon interaction cross section data in the medical and biological context
journal, January 1999

Ultra-thin optical grade scCVD diamond as X-ray beam position monitor
journal, October 2014

  • Desjardins, Kewin; Pomorski, Michal; Morse, John
  • Journal of Synchrotron Radiation, Vol. 21, Issue 6
  • DOI: 10.1107/s1600577514016191

ASAXS study of CaF 2 nanoparticles embedded in a silicate glass matrix
journal, January 2014

  • Hoell, Armin; Varga, Zoltan; Raghuwanshi, Vikram Singh
  • Journal of Applied Crystallography, Vol. 47, Issue 1
  • DOI: 10.1107/s1600576713030100

High-accuracy X-ray detector calibration based on cryogenic radiometry
conference, January 2010

  • Krumrey, M.; Cibik, L.; Müller, P.
  • SRI 2009, 10TH INTERNATIONAL CONFERENCE ON RADIATION INSTRUMENTATION, AIP Conference Proceedings
  • DOI: 10.1063/1.3463341

Development of diamond-based X-ray detection for high-flux beamline diagnostics
journal, September 2010

Preparation and Characteristics of Natural Diamond Nuclear Radiation Detectors
journal, January 1975

  • Kozlov, S. F.; Stuck, R.; Hage-Ali, M.
  • IEEE Transactions on Nuclear Science, Vol. 22, Issue 1
  • DOI: 10.1109/tns.1975.4327634

High-accuracy detector calibration at the PTB four-crystal monochromator beamline
journal, July 2001

  • Krumrey, M.; Ulm, G.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 467-468
  • DOI: 10.1016/s0168-9002(01)00598-8

Cryogenic radiometry in the hard x-ray range
journal, October 2008

Diamond detectors for hadron physics research
journal, May 2010

Annealing dependence of diamond-metal Schottky barrier heights probed by hard x-ray photoelectron spectroscopy
journal, May 2012

  • Gaowei, M.; Muller, E. M.; Rumaiz, A. K.
  • Applied Physics Letters, Vol. 100, Issue 20
  • DOI: 10.1063/1.4718028

Diamond sensors and polycapillary lenses for X-ray absorption spectroscopy
journal, October 2013

  • Ravel, B.; Attenkofer, K.; Bohon, J.
  • Review of Scientific Instruments, Vol. 84, Issue 10
  • DOI: 10.1063/1.4824350

Carbon edge response of diamond devices
journal, March 2014

  • Muller, Erik M.; Gaowei, Mengjia; Ben-Zvi, Ilan
  • Applied Physics Letters, Vol. 104, Issue 9
  • DOI: 10.1063/1.4868135

Chemical vapor deposition diamond based multilayered radiation detector: Physical analysis of detection properties
journal, January 2010

  • Almaviva, S.; Marinelli, Marco; Milani, E.
  • Journal of Applied Physics, Vol. 107, Issue 1
  • DOI: 10.1063/1.3275501

Charge Collection and Propagation in Diamond X-Ray Detectors
journal, August 2010

  • Keister, Jeffrey W.; Smedley, John; Dimitrov, Dimitre
  • IEEE Transactions on Nuclear Science, Vol. 57, Issue 4
  • DOI: 10.1109/tns.2010.2052288

Traceable size determination of PMMA nanoparticles based on Small Angle X-ray Scattering (SAXS)
journal, October 2010

Electrical properties and performances of natural diamond nuclear radiation detectors
journal, March 1979

Zum Mechanismus des lichtelektrischen Prim�rstromes in isolierenden Kristallen
journal, March 1932

Transmission-mode diamond white-beam position monitor at NSLS
journal, March 2012

  • Muller, Erik M.; Smedley, John; Bohon, Jen
  • Journal of Synchrotron Radiation, Vol. 19, Issue 3
  • DOI: 10.1107/S0909049512005043
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