In Situ, Time-Resolved, and Mechanistic Studies of Metal–Organic Framework Nucleation and Growth
Abstract
The vast chemical and structural diversity of metal–organic frameworks (MOFs) opens up the exciting possibility of “crystal engineering” MOFs tailored for particular catalytic or separation applications. Yet the process of reaction discovery, optimization, and scale-up of MOF synthesis remains extremely challenging, presenting significant obstacles to the synthetic realization of many otherwise promising MOF structures. Recently, significant new insights into the fundamental processes governing MOF nucleation and growth, as well as the relationship between reaction parameters and synthetic outcome, have been derived using powerful in situ, time-resolved and/or mechanistic studies of MOF crystallization. This Review provides a summary and associated critical analysis of the results of these and other related “direct” studies of MOF nucleation and growth, with a particular emphasis on the recent advances in instrument technologies that have enabled such studies and on the major hypotheses, theories, and models that have been used to explain MOF formation. We conclude with a summary of the major insights that have been gained from the work summarized in this Review, outlining our own perspective on potential fruitful new directions for investigation.
- Authors:
-
[1]
- Univ. of Wisconsin, Madison, WI (United States). Theoretical Chemistry Inst. and Dept. of Chemistry
- Publication Date:
- Research Org.:
- Univ. of Wisconsin, Madison, WI (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES); National Science Foundation (NSF)
- OSTI Identifier:
- 1433911
- Grant/Contract Number:
- SC0014059; DGE-1256259
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Chemical Reviews
- Additional Journal Information:
- Journal Volume: 118; Journal Issue: 7; Journal ID: ISSN 0009-2665
- Publisher:
- American Chemical Society
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
Citation Formats
Van Vleet, Mary J., Weng, Tingting, Li, Xinyi, and Schmidt, J. R. In Situ, Time-Resolved, and Mechanistic Studies of Metal–Organic Framework Nucleation and Growth. United States: N. p., 2018.
Web. doi:10.1021/acs.chemrev.7b00582.
Van Vleet, Mary J., Weng, Tingting, Li, Xinyi, & Schmidt, J. R. In Situ, Time-Resolved, and Mechanistic Studies of Metal–Organic Framework Nucleation and Growth. United States. https://doi.org/10.1021/acs.chemrev.7b00582
Van Vleet, Mary J., Weng, Tingting, Li, Xinyi, and Schmidt, J. R. Wed .
"In Situ, Time-Resolved, and Mechanistic Studies of Metal–Organic Framework Nucleation and Growth". United States. https://doi.org/10.1021/acs.chemrev.7b00582. https://www.osti.gov/servlets/purl/1433911.
@article{osti_1433911,
title = {In Situ, Time-Resolved, and Mechanistic Studies of Metal–Organic Framework Nucleation and Growth},
author = {Van Vleet, Mary J. and Weng, Tingting and Li, Xinyi and Schmidt, J. R.},
abstractNote = {The vast chemical and structural diversity of metal–organic frameworks (MOFs) opens up the exciting possibility of “crystal engineering” MOFs tailored for particular catalytic or separation applications. Yet the process of reaction discovery, optimization, and scale-up of MOF synthesis remains extremely challenging, presenting significant obstacles to the synthetic realization of many otherwise promising MOF structures. Recently, significant new insights into the fundamental processes governing MOF nucleation and growth, as well as the relationship between reaction parameters and synthetic outcome, have been derived using powerful in situ, time-resolved and/or mechanistic studies of MOF crystallization. This Review provides a summary and associated critical analysis of the results of these and other related “direct” studies of MOF nucleation and growth, with a particular emphasis on the recent advances in instrument technologies that have enabled such studies and on the major hypotheses, theories, and models that have been used to explain MOF formation. We conclude with a summary of the major insights that have been gained from the work summarized in this Review, outlining our own perspective on potential fruitful new directions for investigation.},
doi = {10.1021/acs.chemrev.7b00582},
journal = {Chemical Reviews},
number = 7,
volume = 118,
place = {United States},
year = {Wed Mar 07 00:00:00 EST 2018},
month = {Wed Mar 07 00:00:00 EST 2018}
}
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Self‐Supported Electrocatalysts for Efficient Oxygen Evolution Reaction: Hierarchical CuO x @CoO Nanorods Grown on Cu Foam
journal, March 2020
- Li, Pan; Wang, Jianzhi; Cai, Ning
- ChemCatChem, Vol. 12, Issue 6
Rapid room temperature conversion of hydroxy double salt to MOF-505 for CO 2 capture
journal, January 2019
- Chen, Yongwei; Wu, Houxiao; Xiao, Qiangqiang
- CrystEngComm, Vol. 21, Issue 1
Control of Metal–Organic Framework Crystallization by Metastable Intermediate Pre‐equilibrium Species
journal, December 2018
- Yeung, Hamish H. ‐M.; Sapnik, Adam F.; Massingberd‐Mundy, Felicity
- Angewandte Chemie
Chiral Phosphoric Acids in Metal–Organic Frameworks with Enhanced Acidity and Tunable Catalytic Selectivity
journal, September 2019
- Chen, Xu; Jiang, Hong; Li, Xu
- Angewandte Chemie, Vol. 131, Issue 41
Colloid-assisted growth of metal–organic framework nanoparticles
journal, January 2019
- Nandiyanto, Asep Bayu Dani; He, Xiang; Wang, Wei-Ning
- CrystEngComm, Vol. 21, Issue 14
Two mixed-ligand Cd( ii )–organic frameworks with unique topologies: selective luminescence sensing of TNP and Cu 2+ ions with recyclable performances
journal, January 2019
- Zhang, Jinfang; Jia, Wen; Wu, Junjie
- New Journal of Chemistry, Vol. 43, Issue 40
Nuclear Magnetic Resonance Spectroscopy for In Situ Monitoring of Porous Materials Formation under Hydrothermal Conditions
journal, August 2018
- Haouas, Mohamed
- Materials, Vol. 11, Issue 8
Early stages of phase selection in MOF formation observed in molecular Monte Carlo simulations
journal, January 2019
- Wells, Stephen A.; Cessford, Naomi F.; Seaton, Nigel A.
- RSC Advances, Vol. 9, Issue 25
A flexible metal–organic framework with adaptive pores for high column-capacity gas chromatographic separation
journal, January 2018
- He, Chun-Ting; Ye, Zi-Ming; Xu, Yan-Tong
- Inorganic Chemistry Frontiers, Vol. 5, Issue 11
Ultimate Control over Hydrogen Bond Formation and Reaction Rates for Scalable Synthesis of Highly Crystalline vdW MOF Nanosheets with Large Aspect Ratio
journal, November 2018
- Shen, Yuxia; Shan, Bohan; Cai, Hui
- Advanced Materials, Vol. 30, Issue 52
Chiral Phosphoric Acids in Metal-Organic Frameworks with Enhanced Acidity and Tunable Catalytic Selectivity
journal, September 2019
- Chen, Xu; Jiang, Hong; Li, Xu
- Angewandte Chemie International Edition, Vol. 58, Issue 41
Control of the nucleation and growth processes of metal–organic frameworks using a metal ion-doped polymer substrate for the construction of continuous films
journal, January 2019
- Ohhashi, Takashi; Tsuruoka, Takaaki; Takashima, Yohei
- CrystEngComm, Vol. 21, Issue 33
Tuning the supramolecular isomerism of MOF-74 by controlling the synthesis conditions
journal, January 2019
- Gheorghe, Andreea; Imaz, Inhar; van der Vlugt, Jarl Ivar
- Dalton Transactions, Vol. 48, Issue 27
Control of Metal–Organic Framework Crystallization by Metastable Intermediate Pre‐equilibrium Species
journal, January 2019
- Yeung, Hamish H. ‐M.; Sapnik, Adam F.; Massingberd‐Mundy, Felicity
- Angewandte Chemie International Edition, Vol. 58, Issue 2
Fabrication of zinc-based coordination polymer nanocubes and post-modification through copper decoration
journal, June 2018
- Tran, Ngoc Minh; Mai, Hien Duy; Yoo, Hyojong
- Nano Research, Vol. 11, Issue 11
Structural Transformation in Metal-Organic Frameworks for Reversible Binding of Oxygen
journal, March 2019
- Zeng, Jin-Yue; Wang, Xiao-Shuang; Qi, Yong-Dan
- Angewandte Chemie International Edition, Vol. 58, Issue 17
Hypervalent silicon-based, anionic porous organic polymers with solid microsphere or hollow nanotube morphologies and exceptional capacity for selective adsorption of cationic dyes
journal, January 2019
- Xiong, Gang; Wang, Bin-Bin; You, Li-Xin
- Journal of Materials Chemistry A, Vol. 7, Issue 1
Facet-dependent photocatalytic hydrogen production of metal–organic framework NH 2 -MIL-125(Ti)
journal, January 2019
- Guo, Fan; Guo, Jin-Han; Wang, Peng
- Chemical Science, Vol. 10, Issue 18
Solvent Directed Synthesis of Molecular Cage and Metal Organic Framework of Copper(II) Paddlewheel Cluster
journal, October 2018
- Howlader, Prodip; Mukherjee, Partha Sarathi
- Israel Journal of Chemistry, Vol. 59, Issue 3-4
Molecular chains of coordinated dimolybdenum isonicotinate paddlewheel clusters
journal, January 2019
- Li, Minyuan M.; Claire, F. James; Solomos, Marina A.
- RSC Advances, Vol. 9, Issue 29
Coordination Assemblies of Zn(II) Coordination Polymers: Positional Isomeric Effect and Optical Properties
journal, December 2019
- Liu, Chang-Jie; Zhang, Tong-Tong; Li, Wei-Dong
- Crystals, Vol. 9, Issue 12
Single-crystal-to-single-crystal post-synthetic modifications of three-dimensional LOFs (Ln = Gd, Eu): a way to modulate their luminescence and thermometric properties
journal, January 2020
- De Bellis, Jacopo; Bellucci, Luca; Bottaro, Gregorio
- Dalton Transactions, Vol. 49, Issue 18
Metal−Organic Frameworks for High‐Energy Lithium Batteries with Enhanced Safety: Recent Progress and Future Perspectives
journal, April 2019
- Zhang, Xiahui; Dong, Panpan; Song, Min‐Kyu
- Batteries & Supercaps, Vol. 2, Issue 7
Syntheses, Crystal Structures, and Properties of New Coordination Polymers Incorporating 3,3-Dimethylcyclopropane-1,2-dicarboxylate and 4,4′-Bipyridine Ligands: Syntheses, Crystal Structures, and Properties of New Coordination Polymers Incorporating 3,3-Dimethylcyclopropane-1,2-dicarboxylate and 4,4′-Bipyridin
journal, September 2018
- Shi, Yang; Song, Miao-Miao; Tao, Dong-Liang
- Zeitschrift für anorganische und allgemeine Chemie, Vol. 644, Issue 20
Atomistic structures and dynamics of prenucleation clusters in MOF-2 and MOF-5 syntheses
journal, August 2019
- Xing, Junfei; Schweighauser, Luca; Okada, Satoshi
- Nature Communications, Vol. 10, Issue 1
Highly Transparent, Flexible, and Mechanically Strong Nanopapers of Cellulose Nanofibers @Metal–Organic Frameworks
journal, February 2019
- Zhou, Shengyang; Strømme, Maria; Xu, Chao
- Chemistry – A European Journal, Vol. 25, Issue 14
New Directions in Metal Phosphonate and Phosphinate Chemistry
journal, May 2019
- Shearan, Stephen J. I.; Stock, Norbert; Emmerling, Franziska
- Crystals, Vol. 9, Issue 5
Structural Transformation in Metal–Organic Frameworks for Reversible Binding of Oxygen
journal, March 2019
- Zeng, Jin‐Yue; Wang, Xiao‐Shuang; Qi, Yong‐Dan
- Angewandte Chemie, Vol. 131, Issue 17
Probing the dynamics of Cu nanoparticle growth inside metal-organic frameworks upon electron beam irradiation
journal, September 2020
- Mezenov, Yuri A.; Bruyere, Stéphanie; Kulachenkov, Nikita K.
- Photonics and Nanostructures - Fundamentals and Applications, Vol. 41
Atomistic structures and dynamics of prenucleation clusters in MOF-2 and MOF-5 syntheses
journal, August 2019
- Xing, Junfei; Schweighauser, Luca; Okada, Satoshi
- Nature Communications, Vol. 10, Issue 1
Insights into Functionalization of Metal-Organic Frameworks Using In Situ NMR Spectroscopy
journal, December 2018
- Yuan, Ning; Church, Tamara L.; Brandt, Erik G.
- Scientific Reports, Vol. 8, Issue 1