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Title: A compact membrane-driven diamond anvil cell and cryostat system for nuclear resonant scattering at high pressure and low temperature

In order to study the vibrational and thermal dynamic properties of materials using the nuclear resonant inelastic X-ray scattering (NRIXS) and the hyperfine interactions and magnetic properties using the synchrotron Mössbauer spectroscopy (SMS) at simultaneously high pressure (multi-Mbar) and low temperature (T< 10 K), a new miniature panoramic diamond anvil cell (mini-pDAC) as well as a special gas membrane driven mechanism have been developed and implemented at 3ID, Advanced Photon Source. The gas membrane system allows in situ pressure tuning of the mini- pDAC at low temperature. The mini-pDAC fits into a specially designed compact liquid helium flow cryostat system to achieve low temperature, where liquid helium flows through the holder of the mini-pDAC to cool the sample more efficiently. The sample temperature as low as 9 K has been achieved. Through the membrane, the sample pressure as high as 1.4 Mbar has been generated from this mini-pDAC. The instrument has been routinely used at 3ID for NRIXS and SMS studies. In this paper, technical details of the mini-pDAC, membrane engaging mechanism and the cryostat system are described, and some experimental results are discussed.
Authors:
 [1] ;  [2] ;  [3] ; ORCiD logo [1] ;  [1] ;  [4] ;  [4] ;  [5]
  1. Argonne National Lab. (ANL), Argonne, IL (United States)
  2. Argonne National Lab. (ANL), Argonne, IL (United States); Univ. of Illinois at Urbana-Champaign, Urbana, IL (United States)
  3. Carnegie Institution of Washington, Argonne, IL (United States)
  4. Chinese Academy of Sciences, Beijing (People's Republic of China)
  5. The Univ. of Texas at Austin, Austin, TX (United States)
Publication Date:
Grant/Contract Number:
AC02-06CH11357
Type:
Accepted Manuscript
Journal Name:
Review of Scientific Instruments
Additional Journal Information:
Journal Volume: 88; Journal Issue: 12; Journal ID: ISSN 0034-6748
Publisher:
American Institute of Physics (AIP)
Research Org:
Argonne National Lab. (ANL), Argonne, IL (United States)
Sponsoring Org:
National Science Foundation (NSF); National Natural Science Foundation of China (NNSFC); USDOE Office of Science (SC), Energy Frontier Research Center; Center for High Pressure Science and Technology Advanced Research (HPSTAR); USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22)
Country of Publication:
United States
Language:
English
Subject:
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY; resonant; scattering
OSTI Identifier:
1421943
Alternate Identifier(s):
OSTI ID: 1413078

Zhao, J. Y., Bi, W., Sinogeikin, S., Hu, M. Y., Alp, E. E., Wang, X. C., Jin, C. Q., and Lin, J. F.. A compact membrane-driven diamond anvil cell and cryostat system for nuclear resonant scattering at high pressure and low temperature. United States: N. p., Web. doi:10.1063/1.4999787.
Zhao, J. Y., Bi, W., Sinogeikin, S., Hu, M. Y., Alp, E. E., Wang, X. C., Jin, C. Q., & Lin, J. F.. A compact membrane-driven diamond anvil cell and cryostat system for nuclear resonant scattering at high pressure and low temperature. United States. doi:10.1063/1.4999787.
Zhao, J. Y., Bi, W., Sinogeikin, S., Hu, M. Y., Alp, E. E., Wang, X. C., Jin, C. Q., and Lin, J. F.. 2017. "A compact membrane-driven diamond anvil cell and cryostat system for nuclear resonant scattering at high pressure and low temperature". United States. doi:10.1063/1.4999787.
@article{osti_1421943,
title = {A compact membrane-driven diamond anvil cell and cryostat system for nuclear resonant scattering at high pressure and low temperature},
author = {Zhao, J. Y. and Bi, W. and Sinogeikin, S. and Hu, M. Y. and Alp, E. E. and Wang, X. C. and Jin, C. Q. and Lin, J. F.},
abstractNote = {In order to study the vibrational and thermal dynamic properties of materials using the nuclear resonant inelastic X-ray scattering (NRIXS) and the hyperfine interactions and magnetic properties using the synchrotron Mössbauer spectroscopy (SMS) at simultaneously high pressure (multi-Mbar) and low temperature (T< 10 K), a new miniature panoramic diamond anvil cell (mini-pDAC) as well as a special gas membrane driven mechanism have been developed and implemented at 3ID, Advanced Photon Source. The gas membrane system allows in situ pressure tuning of the mini- pDAC at low temperature. The mini-pDAC fits into a specially designed compact liquid helium flow cryostat system to achieve low temperature, where liquid helium flows through the holder of the mini-pDAC to cool the sample more efficiently. The sample temperature as low as 9 K has been achieved. Through the membrane, the sample pressure as high as 1.4 Mbar has been generated from this mini-pDAC. The instrument has been routinely used at 3ID for NRIXS and SMS studies. In this paper, technical details of the mini-pDAC, membrane engaging mechanism and the cryostat system are described, and some experimental results are discussed.},
doi = {10.1063/1.4999787},
journal = {Review of Scientific Instruments},
number = 12,
volume = 88,
place = {United States},
year = {2017},
month = {12}
}