A compact membrane-driven diamond anvil cell and cryostat system for nuclear resonant scattering at high pressure and low temperature
Abstract
In order to study the vibrational and thermal dynamic properties of materials using the nuclear resonant inelastic X-ray scattering (NRIXS) and the hyperfine interactions and magnetic properties using the synchrotron Mössbauer spectroscopy (SMS) at simultaneously high pressure (multi-Mbar) and low temperature (T< 10 K), a new miniature panoramic diamond anvil cell (mini-pDAC) as well as a special gas membrane driven mechanism have been developed and implemented at 3ID, Advanced Photon Source. The gas membrane system allows in situ pressure tuning of the mini- pDAC at low temperature. The mini-pDAC fits into a specially designed compact liquid helium flow cryostat system to achieve low temperature, where liquid helium flows through the holder of the mini-pDAC to cool the sample more efficiently. The sample temperature as low as 9 K has been achieved. Through the membrane, the sample pressure as high as 1.4 Mbar has been generated from this mini-pDAC. The instrument has been routinely used at 3ID for NRIXS and SMS studies. In this paper, technical details of the mini-pDAC, membrane engaging mechanism and the cryostat system are described, and some experimental results are discussed.
- Authors:
-
- Argonne National Lab. (ANL), Argonne, IL (United States)
- Argonne National Lab. (ANL), Argonne, IL (United States); Univ. of Illinois at Urbana-Champaign, Urbana, IL (United States)
- Carnegie Institution of Washington, Argonne, IL (United States)
- Chinese Academy of Sciences, Beijing (People's Republic of China)
- The Univ. of Texas at Austin, Austin, TX (United States)
- Publication Date:
- Research Org.:
- Argonne National Laboratory (ANL), Argonne, IL (United States); Energy Frontier Research Centers (EFRC) (United States). Energy Frontier Research in Extreme Environments (EFree)
- Sponsoring Org.:
- National Science Foundation (NSF); National Natural Science Foundation of China (NSFC); Center for High Pressure Science and Technology Advanced Research (HPSTAR); USDOE Office of Science (SC), Basic Energy Sciences (BES)
- OSTI Identifier:
- 1421943
- Alternate Identifier(s):
- OSTI ID: 1413078
- Grant/Contract Number:
- AC02-06CH11357
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Review of Scientific Instruments
- Additional Journal Information:
- Journal Volume: 88; Journal Issue: 12; Journal ID: ISSN 0034-6748
- Publisher:
- American Institute of Physics (AIP)
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY; resonant; scattering
Citation Formats
Zhao, J. Y., Bi, W., Sinogeikin, S., Hu, M. Y., Alp, E. E., Wang, X. C., Jin, C. Q., and Lin, J. F. A compact membrane-driven diamond anvil cell and cryostat system for nuclear resonant scattering at high pressure and low temperature. United States: N. p., 2017.
Web. doi:10.1063/1.4999787.
Zhao, J. Y., Bi, W., Sinogeikin, S., Hu, M. Y., Alp, E. E., Wang, X. C., Jin, C. Q., & Lin, J. F. A compact membrane-driven diamond anvil cell and cryostat system for nuclear resonant scattering at high pressure and low temperature. United States. https://doi.org/10.1063/1.4999787
Zhao, J. Y., Bi, W., Sinogeikin, S., Hu, M. Y., Alp, E. E., Wang, X. C., Jin, C. Q., and Lin, J. F. Wed .
"A compact membrane-driven diamond anvil cell and cryostat system for nuclear resonant scattering at high pressure and low temperature". United States. https://doi.org/10.1063/1.4999787. https://www.osti.gov/servlets/purl/1421943.
@article{osti_1421943,
title = {A compact membrane-driven diamond anvil cell and cryostat system for nuclear resonant scattering at high pressure and low temperature},
author = {Zhao, J. Y. and Bi, W. and Sinogeikin, S. and Hu, M. Y. and Alp, E. E. and Wang, X. C. and Jin, C. Q. and Lin, J. F.},
abstractNote = {In order to study the vibrational and thermal dynamic properties of materials using the nuclear resonant inelastic X-ray scattering (NRIXS) and the hyperfine interactions and magnetic properties using the synchrotron Mössbauer spectroscopy (SMS) at simultaneously high pressure (multi-Mbar) and low temperature (T< 10 K), a new miniature panoramic diamond anvil cell (mini-pDAC) as well as a special gas membrane driven mechanism have been developed and implemented at 3ID, Advanced Photon Source. The gas membrane system allows in situ pressure tuning of the mini- pDAC at low temperature. The mini-pDAC fits into a specially designed compact liquid helium flow cryostat system to achieve low temperature, where liquid helium flows through the holder of the mini-pDAC to cool the sample more efficiently. The sample temperature as low as 9 K has been achieved. Through the membrane, the sample pressure as high as 1.4 Mbar has been generated from this mini-pDAC. The instrument has been routinely used at 3ID for NRIXS and SMS studies. In this paper, technical details of the mini-pDAC, membrane engaging mechanism and the cryostat system are described, and some experimental results are discussed.},
doi = {10.1063/1.4999787},
journal = {Review of Scientific Instruments},
number = 12,
volume = 88,
place = {United States},
year = {Wed Dec 13 00:00:00 EST 2017},
month = {Wed Dec 13 00:00:00 EST 2017}
}
Web of Science
Works referenced in this record:
Nuclear resonant scattering at high pressure and high temperature
journal, December 2004
- Zhao, Jiyong; Sturhahn, Wolfgang; Lin, Jung-fu
- High Pressure Research, Vol. 24, Issue 4
Nuclear Bragg scattering of synchrotron radiation with strong speedup of coherent decay, measured on antiferromagnetic
journal, July 1987
- van Bürck, U.; Mössbauer, R. L.; Gerdau, E.
- Physical Review Letters, Vol. 59, Issue 3
Probing of Pressure-Induced Bonding Transitions in Crystalline and Amorphous Earth Materials: Insights from X-ray Raman Scattering at High Pressure
journal, January 2014
- Lee, S. K.; Eng, P. J.; Mao, H. -k.
- Reviews in Mineralogy and Geochemistry, Vol. 78, Issue 1
High pressure X-ray emission spectroscopy at the advanced photon source
journal, July 2016
- Xiao, Yuming; Chow, Paul; Shen, Guoyin
- High Pressure Research, Vol. 36, Issue 3
The ruby pressure standard to 150GPa
journal, December 2005
- Chijioke, Akobuije D.; Nellis, W. J.; Soldatov, A.
- Journal of Applied Physics, Vol. 98, Issue 11
Nuclear Bragg diffraction of synchrotron radiation in yttrium iron garnet
journal, February 1985
- Gerdau, E.; Rüffer, R.; Winkler, H.
- Physical Review Letters, Vol. 54, Issue 8
Online remote control systems for static and dynamic compression and decompression using diamond anvil cells
journal, July 2015
- Sinogeikin, Stanislav V.; Smith, Jesse S.; Rod, Eric
- Review of Scientific Instruments, Vol. 86, Issue 7
Observation of a pressure-induced As–As hybridization associated with a change in the electronic state of Fe in the tetragonal phase of EuFe 2 As 2
journal, December 2012
- Kobayashi, Hisao; Ikeda, Shugo; Sakaguchi, Yui
- Journal of Physics: Condensed Matter, Vol. 25, Issue 2
New approach to the study of nuclear Bragg scattering of synchrotron radiation
journal, June 1987
- Faigel, G.; Siddons, D. P.; Hastings, J. B.
- Physical Review Letters, Vol. 58, Issue 25
Phonons in Nanocrystalline Fe
journal, August 1997
- Fultz, B.; Ahn, C. C.; Alp, E. E.
- Physical Review Letters, Vol. 79, Issue 5
Phonon Density of States of Iron up to 153 Gigapascals
journal, May 2001
- Mao, H. K.
- Science, Vol. 292, Issue 5518
Time resolved nuclear resonant scattering from nuclei using synchrotron radiation
journal, May 1993
- Alp, E. E.; Mooney, T. M.; Toellner, T.
- Physical Review Letters, Vol. 70, Issue 21
Sound Velocities of Hot Dense Iron: Birch's Law Revisited
journal, June 2005
- Lin, J. -F.
- Science, Vol. 308, Issue 5730
Pressure calibration of diamond anvil Raman gauge to 310GPa
journal, August 2006
- Akahama, Yuichi; Kawamura, Haruki
- Journal of Applied Physics, Vol. 100, Issue 4
Nuclear resonant inelastic X-ray scattering at high pressure and low temperature
journal, April 2015
- Bi, Wenli; Zhao, Jiyong; Lin, Jung-Fu
- Journal of Synchrotron Radiation, Vol. 22, Issue 3
MÖSsbauer Experiments Without Conventional Sources
journal, December 1974
- Ruby, S. L.
- Le Journal de Physique Colloques, Vol. 35, Issue C6
Ruby pressure scale in a low-temperature diamond anvil cell
journal, December 2012
- Yamaoka, Hitoshi; Zekko, Yumiko; Jarrige, Ignace
- Journal of Applied Physics, Vol. 112, Issue 12
Observation of Pure Nuclear Diffraction from a Fe/Cr Antiferromagnetic Multilayer
journal, April 1995
- Toellner, T. S.; Sturhahn, W.; Röhlsberger, R.
- Physical Review Letters, Vol. 74, Issue 17
Melting of compressed iron by monitoring atomic dynamics
journal, January 2013
- Jackson, Jennifer M.; Sturhahn, Wolfgang; Lerche, Michael
- Earth and Planetary Science Letters, Vol. 362
Works referencing / citing this record:
Microscopic phase diagram of LaFeAsO single crystals under pressure
journal, November 2018
- Materne, Philipp; Bi, Wenli; Zhao, Jiyong
- Physical Review B, Vol. 98, Issue 17
Parallel background subtraction in diamond anvil cells for high pressure X-ray data analysis
journal, October 2019
- Cai, Weizhao; Hossain, Mohammad Tomal; Coles, Jared
- High Pressure Research, Vol. 39, Issue 4
High-pressure nuclear inelastic scattering with backscattering monochromatization
text, January 2019
- Sergueev, Ilya; Glazyrin, Konstantin; Herrmann, Markus G.
- Deutsches Elektronen-Synchrotron, DESY, Hamburg
Magnetic phase diagram of -FeH
journal, January 2020
- Ying, Jianjun; Zhao, Jiyong; Bi, Wenli
- Physical Review B, Vol. 101, Issue 2
Microscopic phase diagram of LaFeAsO single crystals under pressure
text, January 2018
- Materne, Philipp; Bi, Wenli; Zhao, Jiyong
- Unpublished
High-pressure nuclear inelastic scattering with backscattering monochromatization
journal, August 2019
- Sergueev, Ilya; Glazyrin, Konstantin; Herrmann, Markus G.
- Journal of Synchrotron Radiation, Vol. 26, Issue 5