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Title: Hydrothermal synthesis of silicon oxide clad uranium oxide nanowires

Here, a facile method to synthesize silicon oxide clad uranium oxide nanowires is presented. U 3Si 2, used as a precursor, was oxidized to produce uranium oxide nanocrystallites and amorphous silicon oxide under hydrothermal conditions at 300°C and a pressure of 7.8 × 10 6 Pa. The growth of uranium oxide nanowires was assisted by silicon oxide via assembling the uranium oxide nanocrystallites in an amorphous silicon oxide matrix. The microstructure and composition of silicon oxide clad uranium oxide nanowires were characterized by XRD, SEM, TEM, and EDS. The uranium oxide in the nanowires was determined as UO 2.34 with a fluoride cubic structure.
Authors:
ORCiD logo [1] ; ORCiD logo [1] ; ORCiD logo [1] ; ORCiD logo [1] ; ORCiD logo [1]
  1. Idaho National Lab. (INL), Idaho Falls, ID (United States)
Publication Date:
Report Number(s):
INL/JOU-17-43006
Journal ID: ISSN 0002-7820
Grant/Contract Number:
AC07-05ID14517; FOA‐0000712; FOA-0000712; AC07-051D14517
Type:
Accepted Manuscript
Journal Name:
Journal of the American Ceramic Society
Additional Journal Information:
Journal Volume: 101; Journal Issue: 3; Journal ID: ISSN 0002-7820
Publisher:
American Ceramic Society
Research Org:
Idaho National Lab. (INL), Idaho Falls, ID (United States)
Sponsoring Org:
USDOE Office of Nuclear Energy (NE); Westinghouse Electric Company LLC, Cranberry Township, PA (United States)
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; 77 NANOSCIENCE AND NANOTECHNOLOGY; hydrothermal; nanomaterials; nanowires; oxides; uranium/uranium compounds
OSTI Identifier:
1402684
Alternate Identifier(s):
OSTI ID: 1408185

He, Lingfeng, Harp, Jason M., Wagner, Adrian R., Hoggan, Rita E., and Tolman, Kevin R.. Hydrothermal synthesis of silicon oxide clad uranium oxide nanowires. United States: N. p., Web. doi:10.1111/jace.15295.
He, Lingfeng, Harp, Jason M., Wagner, Adrian R., Hoggan, Rita E., & Tolman, Kevin R.. Hydrothermal synthesis of silicon oxide clad uranium oxide nanowires. United States. doi:10.1111/jace.15295.
He, Lingfeng, Harp, Jason M., Wagner, Adrian R., Hoggan, Rita E., and Tolman, Kevin R.. 2017. "Hydrothermal synthesis of silicon oxide clad uranium oxide nanowires". United States. doi:10.1111/jace.15295. https://www.osti.gov/servlets/purl/1402684.
@article{osti_1402684,
title = {Hydrothermal synthesis of silicon oxide clad uranium oxide nanowires},
author = {He, Lingfeng and Harp, Jason M. and Wagner, Adrian R. and Hoggan, Rita E. and Tolman, Kevin R.},
abstractNote = {Here, a facile method to synthesize silicon oxide clad uranium oxide nanowires is presented. U3Si2, used as a precursor, was oxidized to produce uranium oxide nanocrystallites and amorphous silicon oxide under hydrothermal conditions at 300°C and a pressure of 7.8 × 106 Pa. The growth of uranium oxide nanowires was assisted by silicon oxide via assembling the uranium oxide nanocrystallites in an amorphous silicon oxide matrix. The microstructure and composition of silicon oxide clad uranium oxide nanowires were characterized by XRD, SEM, TEM, and EDS. The uranium oxide in the nanowires was determined as UO2.34 with a fluoride cubic structure.},
doi = {10.1111/jace.15295},
journal = {Journal of the American Ceramic Society},
number = 3,
volume = 101,
place = {United States},
year = {2017},
month = {11}
}

Works referenced in this record:

Growth of nanowires
journal, March 2008
  • Wang, N.; Cai, Y.; Zhang, R. Q.
  • Materials Science and Engineering: R: Reports, Vol. 60, Issue 1-6, p. 1-51
  • DOI: 10.1016/j.mser.2008.01.001