Search Menu
DOE PAGES title logo U.S. Department of Energy
Office of Scientific and Technical Information
Search Scholarly Publications

Title: The Change of X‐ray Diffraction Peak Width During in situ Conventional Sintering of Nanoscale Powders

Abstract

Diffraction peaks of nanoscale particles of 3 mol% yttria‐stabilized zirconia become sharper as the powder sinters. The reduction in the peak width is correlated with the increase in density. The sharpening of the peak agrees reasonably well with the remaining free surface area as the sample sinters. Therefore, high curvature of the free surface of the pores is assumed to lead to peak broadening (the grain boundaries that grow at the expense of the free surfaces of the pores do not have this curvature). The change in the grain size during sintering does not make a significant contribution to peak width.

Authors:
 [1];  [2];  [2];  [3];  [3];  [2];
+ Show Author Affiliations
  1. Department of Mechanical Engineering University of Colorado at Boulder Boulder 80309, Northboro Research &, Development Center Saint‐Gobain Innovative Materials Northboro Massachusetts 01532
  2. Department of Mechanical Engineering University of Colorado at Boulder Boulder 80309
  3. Department of Materials Science and Engineering University of Illinois Champaign Urbana Illinois 61801
Publication Date:
Sponsoring Org.:
USDOE
OSTI Identifier:
1401170
Grant/Contract Number:  
DE‐AC02‐06CH11357
Resource Type:
Publisher's Accepted Manuscript
Journal Name:
Journal of the American Ceramic Society
Additional Journal Information:
Journal Name: Journal of the American Ceramic Society Journal Volume: 99 Journal Issue: 3; Journal ID: ISSN 0002-7820
Publisher:
Wiley-Blackwell
Country of Publication:
United States
Language:
English

Citation Formats

Lebrun, Jean‐Marie, Jha, Shikhar K., Naik, Kiran S., Seymour, Kevin C., Kriven, Waltraud M., Raj, Rishi, and Bordia, ed., R. The Change of X‐ray Diffraction Peak Width During in situ Conventional Sintering of Nanoscale Powders. United States: N. p., 2016. Web. doi:10.1111/jace.14112.
Copy to clipboard
Lebrun, Jean‐Marie, Jha, Shikhar K., Naik, Kiran S., Seymour, Kevin C., Kriven, Waltraud M., Raj, Rishi, & Bordia, ed., R. The Change of X‐ray Diffraction Peak Width During in situ Conventional Sintering of Nanoscale Powders. United States. https://doi.org/10.1111/jace.14112
Copy to clipboard
Lebrun, Jean‐Marie, Jha, Shikhar K., Naik, Kiran S., Seymour, Kevin C., Kriven, Waltraud M., Raj, Rishi, and Bordia, ed., R. Fri . "The Change of X‐ray Diffraction Peak Width During in situ Conventional Sintering of Nanoscale Powders". United States. https://doi.org/10.1111/jace.14112.
Copy to clipboard
@article{osti_1401170,
title = {The Change of X‐ray Diffraction Peak Width During in situ Conventional Sintering of Nanoscale Powders},
author = {Lebrun, Jean‐Marie and Jha, Shikhar K. and Naik, Kiran S. and Seymour, Kevin C. and Kriven, Waltraud M. and Raj, Rishi and Bordia, ed., R.},
abstractNote = {Diffraction peaks of nanoscale particles of 3 mol% yttria‐stabilized zirconia become sharper as the powder sinters. The reduction in the peak width is correlated with the increase in density. The sharpening of the peak agrees reasonably well with the remaining free surface area as the sample sinters. Therefore, high curvature of the free surface of the pores is assumed to lead to peak broadening (the grain boundaries that grow at the expense of the free surfaces of the pores do not have this curvature). The change in the grain size during sintering does not make a significant contribution to peak width.},
doi = {10.1111/jace.14112},
journal = {Journal of the American Ceramic Society},
number = 3,
volume = 99,
place = {United States},
year = {Fri Jan 22 00:00:00 EST 2016},
month = {Fri Jan 22 00:00:00 EST 2016}
}
Copy to clipboard
Journal Article:
Free Publicly Available Full Text
Accepted Manuscript (Publisher)
Publisher's Version of Record
https://doi.org/10.1111/jace.14112
Copyright Statement
Other availability
Search WorldCat Search WorldCat to find libraries that may hold this journal
Citation Metrics:
Cited by: 9 works
Citation information provided by
Web of Science
Save / Share:
Export Metadata
Save to My Library
You must Sign In or Create an Account in order to save documents to your library.

Works referenced in this record:

X-ray line broadening from cold-worked iron
journal, March 1955

Young's Modulus, Flexural Strength, and Fracture of Yttria-Stabilized Zirconia versus Temperature
journal, April 1997

Average Grain Size in Polycrystalline Ceramics
journal, August 1969

Quadrupole lamp furnace for high temperature (up to 2050K) synchrotron powder x-ray diffraction studies in air in reflection geometry
journal, September 2006

  • Sarin, P.; Yoon, W.; Jurkschat, K.
  • Review of Scientific Instruments, Vol. 77, Issue 9
  • DOI: 10.1063/1.2349600

X-ray line broadening from filed aluminium and wolfram
journal, January 1953

Powder diffraction
journal, February 1996

The Separation of Cold‐Work Distortion and Particle Size Broadening in X‐Ray Patterns
journal, April 1952

  • Warren, B. E.; Averbach, B. L.
  • Journal of Applied Physics, Vol. 23, Issue 4
  • DOI: 10.1063/1.1702234

The shape of two-dimensional carbon black reflections
journal, May 1966

The Use of the Pseudo-Voigt Function in the Variance Method of X-ray Line-Broadening Analysis
journal, August 1997

Shape effects on crystallite size distributions in synthetic hematites from X-ray line-profile analysis
journal, October 1980

    Sort by:
    [ × clear filter / sort ]

    Similar Records in DOE PAGES and OSTI.GOV collections: