Single Crystal Growth of URu2Si2 by the Modified Bridgman Technique

Gallagher, Andrew; Nelson, William L.; Chen, Kuan Wen; Besara, Tiglet; Siegrist, Theo; Baumbach, Ryan E.

doi:10.3390/cryst6100128

Title: Single Crystal Growth of URu₂Si₂ by the Modified Bridgman Technique

Abstract

We describe a modified Bridgman growth technique to produce single crystals of the strongly correlated electron material URu₂Si₂ and its nonmagnetic analogue ThRu₂Si₂. Bulk thermodynamic and electrical transport measurements show that the properties of crystals produced in this way are comparable to those previously synthesized using the Czochralski or conventional molten metal flux growth techniques. For the specimens reported here, we find residual resistivity ratios RRR = ρ_300K / ρ₀ as large as 116 and 187 for URu₂Si₂ and ThRu₂Si₂, respectively.

Authors:

Gallagher, Andrew ^[1]; Nelson, William L. ^[1]; Chen, Kuan Wen ^[1]; Besara, Tiglet ^[1]; Siegrist, Theo ^[1]; Baumbach, Ryan E. ^[1]

Florida State Univ., Tallahassee, FL (United States). National High Magnetic Field Lab. (MagLab)

Publication Date:: Sun Oct 02 00:00:00 EDT 2016

Research Org.:: Florida State Univ., Tallahassee, FL (United States). National High Magnetic Field Lab. (MagLab)

Sponsoring Org.:: USDOE; National Science Foundation (NSF); State of Florida (United States)

OSTI Identifier:: 1395955

Grant/Contract Number:: DMR-0084173

Resource Type:: Accepted Manuscript

Journal Name:: Crystals

Additional Journal Information:: Journal Volume: 6; Journal Issue: 10; Journal ID: ISSN 2073-4352

Publisher:: MDPI

Country of Publication:: United States

Language:: English

Subject:: 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY; URu2Si2; hidden order; single crystal; molten metal flux; Bridgman

Citation Formats


                    Gallagher, Andrew, Nelson, William L., Chen, Kuan Wen, Besara, Tiglet, Siegrist, Theo, and Baumbach, Ryan E. Single Crystal Growth of URu2Si2 by the Modified Bridgman Technique.  United States: N. p., 2016. 
Web.  doi:10.3390/cryst6100128.

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                    Gallagher, Andrew, Nelson, William L., Chen, Kuan Wen, Besara, Tiglet, Siegrist, Theo, & Baumbach, Ryan E. Single Crystal Growth of URu2Si2 by the Modified Bridgman Technique.  United States.  https://doi.org/10.3390/cryst6100128

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                    Gallagher, Andrew, Nelson, William L., Chen, Kuan Wen, Besara, Tiglet, Siegrist, Theo, and Baumbach, Ryan E. Sun .  
"Single Crystal Growth of URu2Si2 by the Modified Bridgman Technique".  United States.  https://doi.org/10.3390/cryst6100128.  https://www.osti.gov/servlets/purl/1395955.

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@article{osti_1395955,

  title        = {Single Crystal Growth of URu2Si2 by the Modified Bridgman Technique},

  author       = {Gallagher, Andrew and Nelson, William L. and Chen, Kuan Wen and Besara, Tiglet and Siegrist, Theo and Baumbach, Ryan E.},

  abstractNote = {We describe a modified Bridgman growth technique to produce single crystals of the strongly correlated electron material URu2Si2 and its nonmagnetic analogue ThRu2Si2. Bulk thermodynamic and electrical transport measurements show that the properties of crystals produced in this way are comparable to those previously synthesized using the Czochralski or conventional molten metal flux growth techniques. For the specimens reported here, we find residual resistivity ratios RRR = ρ300K / ρ0 as large as 116 and 187 for URu2Si2 and ThRu2Si2, respectively.},

  doi          = {10.3390/cryst6100128},

  journal      = {Crystals},

  number       = 10,

  volume       = 6,

  place        = {United States},

  year         = {Sun Oct 02 00:00:00 EDT 2016},

  month        = {Sun Oct 02 00:00:00 EDT 2016}

}

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Works referenced in this record:

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Works referencing / citing this record:

Flow Instabilities of Coupled Rotation and Thermal-Solutal Capillary Convection of Binary Mixture in Czochralski Configuration
journal, January 2019

Wu, Chunmei; Yuan, Bo; Li, Yourong
Crystals, Vol. 9, Issue 2
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Similar Records

Title: Single Crystal Growth of URu2Si2 by the Modified Bridgman Technique

Abstract

Citation Formats

Sequential Spin Polarization of the Fermi Surface Pockets in URu 2 Si 2 and Its Implications for the Hidden Order journal, April 2011

The de Haas–van Alphen effect in URu 2 Si 2 under pressure journal, July 2003

Chemical pressure tuning of URu 2 Si 2 via isoelectronic substitution of Ru with Fe journal, February 2015

Hybridization-driven orthorhombic lattice instability in URu 2 Si 2 journal, November 2013

Partially gapped Fermi surface in the heavy-electron superconductor URu 2 Si 2 journal, January 1986

Magnetic and Electronic Properties of URu 2 Si 2 Revealed by Comparison with Nonmagnetic References ThRu 2 Si 2 and LaRu 2 Si 2 journal, June 2015

Crystal growth and characterization of MT2Si2 ternary intermetallics (M = U, RE and T = 3d, 4d, 5d transition metals) journal, December 1986

Unfolding the physics of URu2Si2 through silicon to phosphorus substitution journal, February 2016

Anisotropic electrical resistivity of the magnetic heavy-fermion superconductor URu 2 Si 2 journal, May 1986

Hybridization model for the magnetic-ordering behavior of uranium- and cerium-based 1:2:2 intermetallic compounds journal, October 1993

Neutron Scattering Study on Competition between Hidden Order and Antiferromagnetism in U(Ru 1- x Rh x ) 2 Si 2 ( x ≤0.05) journal, March 2004

Details of Sample Dependence and Transport Properties of URu 2 Si 2 journal, November 2011

Superconductivity and magnetic order in a strongly interacting fermi-system: URu2Si2 journal, June 1986

High purity specimens of URu 2 Si 2 produced by a molten metal flux technique journal, April 2014

Effect of transition-metal substitutions on competing electronic transitions in the heavy-electron compound URu 2 Si 2 journal, February 1990

Super Clean Sample of URu 2 Si 2 journal, January 2008

Similarity of the Fermi Surface in the Hidden Order State and in the Antiferromagnetic State of URu 2 Si 2 journal, November 2010

Evidence for broken time-reversal symmetry in the superconducting phase of URu 2 Si 2 journal, April 2015

Enhancement of the hidden order/large moment antiferromagnetic transition temperature in the URu 2− x Os x Si 2 system journal, April 2014

Colloquium : Hidden order, superconductivity, and magnetism: The unsolved case of URu 2 Si 2 journal, November 2011

Purification of Uranium Metal using the Solid State Electrotransport Method under Ultrahigh Vacuum journal, June 1998

Fermi Surface of ThRu 2 Si 2 as a Reference to the Strongly Correlated Isostructural Metals Investigated by Quantum Oscillations journal, October 2016

Hidden order behaviour in URu 2 Si 2 (A critical review of the status of hidden order in 2014) journal, May 2014

The suppression of hidden order and the onset of ferromagnetism in URu 2 Si 2 via Re substitution journal, March 2010

Chirality density wave of the "hidden order" phase in URu2Si2 journal, February 2015

Twofold enhancement of the hidden-order/large-moment antiferromagnetic phase boundary in the URu 2 − x Fe x Si 2 system journal, December 2011

Evidence for a nematic component to the hidden-order parameter in URu2Si2 from differential elastoresistance measurements journal, March 2015

Direct observation of lattice symmetry breaking at the hidden-order transition in URu2Si2 journal, June 2014

The suppression of hidden order and onset of ferromagnetism in URu2Si2 via Re substitution text, January 2010

Details of Sample Dependence and Transport Properties of URu2Si2 text, January 2011

Hidden Order Behaviour in URu2Si2 (A Critical Review of the Status of Hidden Order in 2014) text, January 2014

Evidence for a nematic component to the Hidden Order parameter in URu2Si2 from differential elastoresistance measurements text, January 2014

Direct observation of lattice symmetry breaking at the hidden-order transition in URu2Si2 text, January 2014

Chirality density wave of the 'hidden order' phase in URu$_2$Si$_2$ text, January 2014

Flow Instabilities of Coupled Rotation and Thermal-Solutal Capillary Convection of Binary Mixture in Czochralski Configuration journal, January 2019

Title: Single Crystal Growth of URu₂Si₂ by the Modified Bridgman Technique

Sequential Spin Polarization of the Fermi Surface Pockets in ${URu}_{2} {Si}_{2}$ and Its Implications for the Hidden Order
journal, April 2011

The de Haas–van Alphen effect in URu ₂ Si ₂ under pressure
journal, July 2003

Chemical pressure tuning of ${URu}_{2} {Si}_{2}$ via isoelectronic substitution of Ru with Fe
journal, February 2015

Hybridization-driven orthorhombic lattice instability in URu $_{2}$ Si $_{2}$
journal, November 2013

Partially gapped Fermi surface in the heavy-electron superconductor ${URu}_{2}$ ${Si}_{2}$
journal, January 1986

Magnetic and Electronic Properties of URu ₂ Si ₂ Revealed by Comparison with Nonmagnetic References ThRu ₂ Si ₂ and LaRu ₂ Si ₂
journal, June 2015

Crystal growth and characterization of MT2Si2 ternary intermetallics (M = U, RE and T = 3d, 4d, 5d transition metals)
journal, December 1986

Unfolding the physics of URu2Si2 through silicon to phosphorus substitution
journal, February 2016

Anisotropic electrical resistivity of the magnetic heavy-fermion superconductor ${URu}_{2}$ ${Si}_{2}$
journal, May 1986

Hybridization model for the magnetic-ordering behavior of uranium- and cerium-based 1:2:2 intermetallic compounds
journal, October 1993

Neutron Scattering Study on Competition between Hidden Order and Antiferromagnetism in U(Ru _{1- x} Rh _x ) ₂ Si ₂ ( x ≤0.05)
journal, March 2004

Details of Sample Dependence and Transport Properties of URu ₂ Si ₂
journal, November 2011

Superconductivity and magnetic order in a strongly interacting fermi-system: URu2Si2
journal, June 1986

High purity specimens of URu ₂ Si ₂ produced by a molten metal flux technique
journal, April 2014

Effect of transition-metal substitutions on competing electronic transitions in the heavy-electron compound ${URu}_{2}$ ${Si}_{2}$
journal, February 1990

Super Clean Sample of URu ₂ Si ₂
journal, January 2008

Similarity of the Fermi Surface in the Hidden Order State and in the Antiferromagnetic State of ${URu}_{2} {Si}_{2}$
journal, November 2010

Evidence for broken time-reversal symmetry in the superconducting phase of ${URu}_{2} {Si}_{2}$
journal, April 2015

Enhancement of the hidden order/large moment antiferromagnetic transition temperature in the URu _{2− x} Os _x Si ₂ system
journal, April 2014

Colloquium : Hidden order, superconductivity, and magnetism: The unsolved case of ${URu}_{2} {Si}_{2}$
journal, November 2011

Purification of Uranium Metal using the Solid State Electrotransport Method under Ultrahigh Vacuum
journal, June 1998

Fermi Surface of ThRu ₂ Si ₂ as a Reference to the Strongly Correlated Isostructural Metals Investigated by Quantum Oscillations
journal, October 2016

Hidden order behaviour in URu ₂ Si ₂ (A critical review of the status of hidden order in 2014)
journal, May 2014

The suppression of hidden order and the onset of ferromagnetism in URu ₂ Si ₂ via Re substitution
journal, March 2010

Chirality density wave of the "hidden order" phase in URu2Si2
journal, February 2015

Twofold enhancement of the hidden-order/large-moment antiferromagnetic phase boundary in the URu $_{2 - x}$ Fe $_{x}$ Si $_{2}$ system
journal, December 2011

Evidence for a nematic component to the hidden-order parameter in URu2Si2 from differential elastoresistance measurements
journal, March 2015

Direct observation of lattice symmetry breaking at the hidden-order transition in URu2Si2
journal, June 2014

The suppression of hidden order and onset of ferromagnetism in URu2Si2 via Re substitution
text, January 2010

Details of Sample Dependence and Transport Properties of URu2Si2
text, January 2011

Hidden Order Behaviour in URu2Si2 (A Critical Review of the Status of Hidden Order in 2014)
text, January 2014

Evidence for a nematic component to the Hidden Order parameter in URu2Si2 from differential elastoresistance measurements
text, January 2014

Direct observation of lattice symmetry breaking at the hidden-order transition in URu2Si2
text, January 2014

Chirality density wave of the 'hidden order' phase in URu$_2$Si$_2$
text, January 2014

Flow Instabilities of Coupled Rotation and Thermal-Solutal Capillary Convection of Binary Mixture in Czochralski Configuration
journal, January 2019