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Title: Solid state microwave synthesis of highly crystalline ordered mesoporous hausmannite Mn 3 O 4 films

Microwave calcination of ordered micelle templated manganese carbonate films leads to highly crystalline, ordered mesoporous manganese oxide, while similar temperatures in a furnace lead to disordered, amorphous manganese oxide.
Authors:
 [1] ;  [2] ; ORCiD logo [3] ; ORCiD logo [1] ; ORCiD logo [2]
  1. Univ. of Akron, OH (United States). Dept. of Polymer Science
  2. Univ. of Akron, OH (United States). Dept. of Polymer Engineering
  3. Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
Publication Date:
Grant/Contract Number:
AC02-06CH11357
Type:
Accepted Manuscript
Journal Name:
CrystEngComm
Additional Journal Information:
Journal Volume: 19; Journal Issue: 30; Journal ID: ISSN 1466-8033
Publisher:
Royal Society of Chemistry
Research Org:
Argonne National Lab. (ANL), Argonne, IL (United States)
Sponsoring Org:
USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22); National Science Foundation (NSF)
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
OSTI Identifier:
1393467