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Title: HiSPoD: a program for high-speed polychromatic X-ray diffraction experiments and data analysis on polycrystalline samples

Abstract

Here, a high-speed X-ray diffraction technique was recently developed at the 32-ID-B beamline of the Advanced Photon Source for studying highly dynamic, yet non-repeatable and irreversible, materials processes. In experiments, the microstructure evolution in a single material event is probed by recording a series of diffraction patterns with extremely short exposure time and high frame rate. Owing to the limited flux in a short pulse and the polychromatic nature of the incident X-rays, analysis of the diffraction data is challenging. Here, HiSPoD, a stand-alone Matlab-based software for analyzing the polychromatic X-ray diffraction data from polycrystalline samples, is described. With HiSPoD, researchers are able to perform diffraction peak indexing, extraction of one-dimensional intensity profiles by integrating a two-dimensional diffraction pattern, and, more importantly, quantitative numerical simulations to obtain precise sample structure information.

Authors:
 [1];  [1]
  1. Argonne National Lab. (ANL), Argonne, IL (United States)
Publication Date:
Research Org.:
Argonne National Lab. (ANL), Argonne, IL (United States)
Sponsoring Org.:
USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22)
OSTI Identifier:
1391906
Grant/Contract Number:  
AC02-06CH11357
Resource Type:
Accepted Manuscript
Journal Name:
Journal of Synchrotron Radiation (Online)
Additional Journal Information:
Journal Name: Journal of Synchrotron Radiation (Online); Journal Volume: 23; Journal Issue: 4; Journal ID: ISSN 1600-5775
Publisher:
International Union of Crystallography
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; 46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY; X-ray diffraction; high speed; polychromatic beam; dynamic processes

Citation Formats

Sun, Tao, and Fezzaa, Kamel. HiSPoD: a program for high-speed polychromatic X-ray diffraction experiments and data analysis on polycrystalline samples. United States: N. p., 2016. Web. doi:10.1107/S1600577516005804.
Sun, Tao, & Fezzaa, Kamel. HiSPoD: a program for high-speed polychromatic X-ray diffraction experiments and data analysis on polycrystalline samples. United States. doi:10.1107/S1600577516005804.
Sun, Tao, and Fezzaa, Kamel. Fri . "HiSPoD: a program for high-speed polychromatic X-ray diffraction experiments and data analysis on polycrystalline samples". United States. doi:10.1107/S1600577516005804. https://www.osti.gov/servlets/purl/1391906.
@article{osti_1391906,
title = {HiSPoD: a program for high-speed polychromatic X-ray diffraction experiments and data analysis on polycrystalline samples},
author = {Sun, Tao and Fezzaa, Kamel},
abstractNote = {Here, a high-speed X-ray diffraction technique was recently developed at the 32-ID-B beamline of the Advanced Photon Source for studying highly dynamic, yet non-repeatable and irreversible, materials processes. In experiments, the microstructure evolution in a single material event is probed by recording a series of diffraction patterns with extremely short exposure time and high frame rate. Owing to the limited flux in a short pulse and the polychromatic nature of the incident X-rays, analysis of the diffraction data is challenging. Here, HiSPoD, a stand-alone Matlab-based software for analyzing the polychromatic X-ray diffraction data from polycrystalline samples, is described. With HiSPoD, researchers are able to perform diffraction peak indexing, extraction of one-dimensional intensity profiles by integrating a two-dimensional diffraction pattern, and, more importantly, quantitative numerical simulations to obtain precise sample structure information.},
doi = {10.1107/S1600577516005804},
journal = {Journal of Synchrotron Radiation (Online)},
number = 4,
volume = 23,
place = {United States},
year = {2016},
month = {6}
}

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