Solvent-Mediated Crystallization of CH3NH3SnI3 Films for Heterojunction Depleted Perovskite Solar Cells
Abstract
Organo-lead halide perovskite solar cells have gained enormous significance and have now achieved power conversion efficiencies of ~20%. However, the potential toxicity of lead in these systems raises environmental concerns for widespread deployment. In this work we investigate solvent effects on the crystallization of the lead-free methylammonium tin triiodide (CH3NH3SnI3) perovskite films in a solution growth process. Highly uniform, pinhole-free perovskite films are obtained from a dimethyl sulfoxide (DMSO) solution via a transitional SnI2·3DMSO intermediate phase. This high-quality perovskite film enables the realization of heterojunction depleted solar cells based on mesoporous TiO2 layer but in the absence of any hole-transporting material with an unprecedented photocurrent up to 21 mA cm–2. Charge extraction and transient photovoltage decay measurements reveal high carrier densities in the CH3NH3SnI3 perovskite device which are one order of magnitude larger than CH3NH3PbI3-based devices but with comparable recombination lifetimes in both devices. The relatively high background dark carrier density of the Sn-based perovskite is responsible for the lower photovoltaic efficiency in comparison to the Pb-based analogues. These results provide important progress toward achieving improved perovskite morphology control in realizing solution-processed highly efficient lead-free perovskite solar cells.
- Authors:
-
- Energy Frontier Research Centers (EFRC) (United States). Argonne-Northwestern Solar Energy Research Center (ANSER); Northwestern Univ., Evanston, IL (United States)
- Publication Date:
- Research Org.:
- Energy Frontier Research Centers (EFRC) (United States). Argonne-Northwestern Solar Energy Research Center (ANSER)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES); National Science Foundation (NSF); State of Illinois
- OSTI Identifier:
- 1386526
- Grant/Contract Number:
- SC0001059
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Journal of the American Chemical Society
- Additional Journal Information:
- Journal Volume: 137; Journal Issue: 35; Related Information: ANSER partners with Northwestern University (lead); Argonne National Laboratory; University of Chicago; University of Illinois, Urbana-Champaign; Yale University; Journal ID: ISSN 0002-7863
- Publisher:
- American Chemical Society (ACS)
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY; catalysis (homogeneous); catalysis (heterogeneous); solar (photovoltaic); solar (fuels); photosynthesis (natural and artificial); bio-inspired; hydrogen and fuel cells; electrodes - solar; defects; charge transport; spin dynamics; membrane; materials and chemistry by design; optics; synthesis (novel materials); synthesis (self-assembly); crystallization; layers; solvents; solar cells; perovskites
Citation Formats
Hao, Feng, Stoumpos, Constantinos C., Guo, Peijun, Zhou, Nanjia, Marks, Tobin J., Chang, Robert P. H., and Kanatzidis, Mercouri G. Solvent-Mediated Crystallization of CH3NH3SnI3 Films for Heterojunction Depleted Perovskite Solar Cells. United States: N. p., 2015.
Web. doi:10.1021/jacs.5b06658.
Hao, Feng, Stoumpos, Constantinos C., Guo, Peijun, Zhou, Nanjia, Marks, Tobin J., Chang, Robert P. H., & Kanatzidis, Mercouri G. Solvent-Mediated Crystallization of CH3NH3SnI3 Films for Heterojunction Depleted Perovskite Solar Cells. United States. https://doi.org/10.1021/jacs.5b06658
Hao, Feng, Stoumpos, Constantinos C., Guo, Peijun, Zhou, Nanjia, Marks, Tobin J., Chang, Robert P. H., and Kanatzidis, Mercouri G. Thu .
"Solvent-Mediated Crystallization of CH3NH3SnI3 Films for Heterojunction Depleted Perovskite Solar Cells". United States. https://doi.org/10.1021/jacs.5b06658. https://www.osti.gov/servlets/purl/1386526.
@article{osti_1386526,
title = {Solvent-Mediated Crystallization of CH3NH3SnI3 Films for Heterojunction Depleted Perovskite Solar Cells},
author = {Hao, Feng and Stoumpos, Constantinos C. and Guo, Peijun and Zhou, Nanjia and Marks, Tobin J. and Chang, Robert P. H. and Kanatzidis, Mercouri G.},
abstractNote = {Organo-lead halide perovskite solar cells have gained enormous significance and have now achieved power conversion efficiencies of ~20%. However, the potential toxicity of lead in these systems raises environmental concerns for widespread deployment. In this work we investigate solvent effects on the crystallization of the lead-free methylammonium tin triiodide (CH3NH3SnI3) perovskite films in a solution growth process. Highly uniform, pinhole-free perovskite films are obtained from a dimethyl sulfoxide (DMSO) solution via a transitional SnI2·3DMSO intermediate phase. This high-quality perovskite film enables the realization of heterojunction depleted solar cells based on mesoporous TiO2 layer but in the absence of any hole-transporting material with an unprecedented photocurrent up to 21 mA cm–2. Charge extraction and transient photovoltage decay measurements reveal high carrier densities in the CH3NH3SnI3 perovskite device which are one order of magnitude larger than CH3NH3PbI3-based devices but with comparable recombination lifetimes in both devices. The relatively high background dark carrier density of the Sn-based perovskite is responsible for the lower photovoltaic efficiency in comparison to the Pb-based analogues. These results provide important progress toward achieving improved perovskite morphology control in realizing solution-processed highly efficient lead-free perovskite solar cells.},
doi = {10.1021/jacs.5b06658},
journal = {Journal of the American Chemical Society},
number = 35,
volume = 137,
place = {United States},
year = {Thu Aug 27 00:00:00 EDT 2015},
month = {Thu Aug 27 00:00:00 EDT 2015}
}
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Figures / Tables:
Table 1: Physical Properties of the Polar Solvents Used in the Perovskite Film Deposition
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Suppressing Charge Recombination and Ultraviolet Light Degradation of Perovskite Solar Cells Using Silicon Oxide Passivation
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Formation of Stable Tin Perovskites Co-crystallized with Three Halides for Carbon-Based Mesoscopic Lead-Free Perovskite Solar Cells
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Room Temperature Phase Transition in Methylammonium Lead Iodide Perovskite Thin Films Induced by Hydrohalic Acid Additives
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A micron-scale laminar MAPbBr 3 single crystal for an efficient and stable perovskite solar cell
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Crystallization, Properties, and Challenges of Low-Bandgap Sn-Pb Binary Perovskites
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Multichannel Interdiffusion Driven FASnI 3 Film Formation Using Aqueous Hybrid Salt/Polymer Solutions toward Flexible Lead-Free Perovskite Solar Cells
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Selection of an anti-solvent for efficient and stable cesium-containing triple cation planar perovskite solar cells
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Highly Efficient Perovskite Solar Cells with Substantial Reduction of Lead Content
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Lead-free hybrid perovskites for photovoltaics
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Highly efficient tin perovskite solar cells achieved in a wide oxygen concentration range
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Interfacial defect passivation in CH3NH3PbI3 perovskite solar cells using modifying of hole transport layer
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Hydrazinium-assisted stabilisation of methylammonium tin iodide for lead-free perovskite solar cells
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Improved film morphology of (CH3NH3)3Bi2I9 via cation displacement approach for lead-free perovskite solar cells
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Evolution of Pb-Free and Partially Pb-Substituted Perovskite Absorbers for Efficient Perovskite Solar Cells
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Robust Tin-Based Perovskite Solar Cells with Hybrid Organic Cations to Attain Efficiency Approaching 10%
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Band alignment of Pb–Sn mixed triple cation perovskites for inverted solar cells with negligible hysteresis
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Lead-Free Inverted Planar Formamidinium Tin Triiodide Perovskite Solar Cells Achieving Power Conversion Efficiencies up to 6.22%
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Enhanced stability and efficiency in hole-transport-layer-free CsSnI3 perovskite photovoltaics
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Understanding Film Formation Morphology and Orientation in High Member 2D Ruddlesden-Popper Perovskites for High-Efficiency Solar Cells
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Large-Grain Tin-Rich Perovskite Films for Efficient Solar Cells via Metal Alloying Technique
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Flexible Perowskit‐Solarzellen: Herstellung und Anwendungen
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Highly Efficient Light Emitting Diodes Based on In Situ Fabricated FAPbI 3 Nanocrystals: Solvent Effects of On‐Chip Crystallization
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High-Performance Photodetectors Based on Organometal Halide Perovskite Nanonets
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Zero-dimensional hybrid iodobismuthate derivatives: from structure study to photovoltaic application
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Interface Engineering in Tin Perovskite Solar Cells
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Reversible Band Gap Narrowing of Sn-Based Hybrid Perovskite Single Crystal with Excellent Phase Stability
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Dependence of material properties and photovoltaic performance of triple cation tin perovskites on the iodide to bromide ratio
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Narrow band gap and high mobility of lead-free perovskite single crystal Sn-doped MA 3 Sb 2 I 9
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Lead‐Free Tin‐Based Perovskite Solar Cells: Strategies Toward High Performance
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Bifacial Contact Junction Engineering for High‐Performance Perovskite Solar Cells with Efficiency Exceeding 21%
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Addressing Toxicity of Lead: Progress and Applications of Low-Toxic Metal Halide Perovskites and Their Derivatives
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Pb‐Reduced CsPb 0.9 Zn 0.1 I 2 Br Thin Films for Efficient Perovskite Solar Cells
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Light-induced effects on crystal size and photo-stability of colloidal CsPbBr 3 perovskite nanocrystals
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Searching for stability at lower dimensions: current trends and future prospects of layered perovskite solar cells
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Ideal Bandgap Organic-Inorganic Hybrid Perovskite Solar Cells
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Formation of Hybrid Perovskite Tin Iodide Single Crystals by Top-Seeded Solution Growth
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High coverage solution-processed planar perovskite solar cell grown based on the Stranski–Krastanov mechanism at low temperature and short time
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Highly Efficient Perovskite-Perovskite Tandem Solar Cells Reaching 80% of the Theoretical Limit in Photovoltage
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Assessing the suitability of copper thiocyanate as a hole-transport layer in inverted CsSnI3 perovskite photovoltaics
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Synergy Effect of Both 2,2,2-Trifluoroethylamine Hydrochloride and SnF 2 for Highly Stable FASnI 3−x Cl x Perovskite Solar Cells
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Management of Crystallization Kinetics for Efficient and Stable Low-Dimensional Ruddlesden-Popper (LDRP) Lead-Free Perovskite Solar Cells
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Present Status and Research Prospects of Tin‐based Perovskite Solar Cells
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Enhanced Structural Stability and Photo Responsiveness of CH 3 NH 3 SnI 3 Perovskite via Pressure-Induced Amorphization and Recrystallization
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Stable Low-Bandgap Pb-Sn Binary Perovskites for Tandem Solar Cells
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Lead-Free Hybrid Perovskite Absorbers for Viable Application: Can We Eat the Cake and Have It too?
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Heterogeneous Supersaturation in Mixed Perovskites
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Tin Halide Perovskites: Progress and Challenges
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Lead‐Free Solar Cells based on Tin Halide Perovskite Films with High Coverage and Improved Aggregation
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Potential Substitutes for Replacement of Lead in Perovskite Solar Cells: A Review
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Trihydrazine Dihydriodide‐Assisted Fabrication of Efficient Formamidinium Tin Iodide Perovskite Solar Cells
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Emerging alkali metal ion (Li + , Na + , K + and Rb + ) doped perovskite films for efficient solar cells: recent advances and prospects
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Enhanced stability of the optical responses from all-inorganic perovskite nanocrystals embedded in a synthetic opal matrix
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Pathways toward high-performance perovskite solar cells: review of recent advances in organo-metal halide perovskites for photovoltaic applications
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Causes and Solutions of Recombination in Perovskite Solar Cells
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Formation of Stable Tin Perovskites Co-crystallized with Three Halides for Carbon-Based Mesoscopic Lead-Free Perovskite Solar Cells
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Reversible Band Gap Narrowing of Sn-Based Hybrid Perovskite Single Crystal with Excellent Phase Stability
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A Cation-Exchange Approach for the Fabrication of Efficient Methylammonium Tin Iodide Perovskite Solar Cells
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Formation of Hybrid Perovskite Tin Iodide Single Crystals by Top-Seeded Solution Growth
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Mixed-Organic-Cation Tin Iodide for Lead-Free Perovskite Solar Cells with an Efficiency of 8.12%
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Lead-Free Hybrid Perovskite Absorbers for Viable Application: Can We Eat the Cake and Have It too?
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Recent Advances in Flexible Perovskite Solar Cells: Fabrication and Applications
journal, February 2019
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Potential Substitutes for Replacement of Lead in Perovskite Solar Cells: A Review
journal, July 2019
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Recent Advances in Synthesis and Properties of Hybrid Halide Perovskites for Photovoltaics
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Highly Efficient Perovskite Solar Cells with Substantial Reduction of Lead Content
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Perovskite solar cells: must lead be replaced – and can it be done?
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Enhanced photovoltaic performance and stability with a new type of hollow 3D perovskite {en}FASnI 3
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Lead-free hybrid perovskites for photovoltaics
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