Hard X-ray polarizer to enable simultaneous three-dimensional nanoscale imaging of magnetic structure and lattice strain

Logan, Jonathan; Harder, Ross; Li, Luxi; Haskel, Daniel; Chen, Pice; Winarski, Robert; Fuesz, Peter; Schlagel, Deborah; Vine, David; Benson, Christa; McNulty, Ian

doi:10.1107/S1600577516009632

Title: Hard X-ray polarizer to enable simultaneous three-dimensional nanoscale imaging of magnetic structure and lattice strain

Abstract

Recent progress in the development of dichroic Bragg coherent diffractive imaging, a new technique for simultaneous three-dimensional imaging of strain and magnetization at the nanoscale, is reported. This progress includes the installation of a diamond X-ray phase retarder at beamline 34-ID-C of the Advanced Photon Source. The performance of the phase retarder for tuning X-ray polarization is demonstrated with temperature-dependent X-ray magnetic circular dichroism measurements on a gadolinium foil in transmission and on a Gd₅Si₂Ge₂crystal in diffraction geometry with a partially coherent, focused X-ray beam. Feasibility tests for dichroic Bragg coherent diffractive imaging are presented. These tests include (1) using conventional Bragg coherent diffractive imaging to determine whether the phase retarder introduces aberrations using a nonmagnetic gold nanocrystal as a control sample, and (2) collecting coherent diffraction patterns of a magnetic Gd₅Si₂Ge₂nanocrystal with left- and right-circularly polarized X-rays. Future applications of dichroic Bragg coherent diffractive imaging for the correlation of strain and lattice defects with magnetic ordering and inhomogeneities are considered.

Authors:

Logan, Jonathan ^[1]; Harder, Ross ^[1]; Li, Luxi ^[1]; Haskel, Daniel ^[1]; Chen, Pice ^[2]; Winarski, Robert ^[1]; Fuesz, Peter ^[1]; Schlagel, Deborah ^[3]; Vine, David ^[4]; Benson, Christa ^[1]; McNulty, Ian ^[1]

Argonne National Lab. (ANL), Argonne, IL (United States)
Northwestern Univ., Evanston, IL (United States)
Ames Lab., Ames, IA (United States)
Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)

Publication Date:: Fri Jan 01 00:00:00 EST 2016

Research Org.:: Ames Lab., Ames, IA (United States); Argonne National Lab. (ANL), Argonne, IL (United States); Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)

Sponsoring Org.:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

OSTI Identifier:: 1337684

Alternate Identifier(s):: OSTI ID: 1339299; OSTI ID: 1378749

Report Number(s):: IS-J-9094
Journal ID: ISSN 1600-5775; JSYRES; PII: S1600577516009632

Grant/Contract Number:: AC02-07CH11358; AC02-06CH11357; AC02-05CH11231

Resource Type:: Accepted Manuscript

Journal Name:: Journal of Synchrotron Radiation (Online)

Additional Journal Information:: Journal Name: Journal of Synchrotron Radiation (Online); Journal Volume: 23; Journal Issue: 5; Journal ID: ISSN 1600-5775

Publisher:: International Union of Crystallography

Country of Publication:: United States

Language:: English

Subject:: 46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY; Bragg coherent diffractive imaging; XMCD; nanomagnetism; strain; 75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY; 73 NUCLEAR PHYSICS AND RADIATION PHYSICS

Citation Formats


                    Logan, Jonathan, Harder, Ross, Li, Luxi, Haskel, Daniel, Chen, Pice, Winarski, Robert, Fuesz, Peter, Schlagel, Deborah, Vine, David, Benson, Christa, and McNulty, Ian. Hard X-ray polarizer to enable simultaneous three-dimensional nanoscale imaging of magnetic structure and lattice strain.  United States: N. p., 2016. 
Web.  doi:10.1107/S1600577516009632.

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                    Logan, Jonathan, Harder, Ross, Li, Luxi, Haskel, Daniel, Chen, Pice, Winarski, Robert, Fuesz, Peter, Schlagel, Deborah, Vine, David, Benson, Christa, & McNulty, Ian. Hard X-ray polarizer to enable simultaneous three-dimensional nanoscale imaging of magnetic structure and lattice strain.  United States.  https://doi.org/10.1107/S1600577516009632

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                    Logan, Jonathan, Harder, Ross, Li, Luxi, Haskel, Daniel, Chen, Pice, Winarski, Robert, Fuesz, Peter, Schlagel, Deborah, Vine, David, Benson, Christa, and McNulty, Ian. Fri .  
"Hard X-ray polarizer to enable simultaneous three-dimensional nanoscale imaging of magnetic structure and lattice strain".  United States.  https://doi.org/10.1107/S1600577516009632.  https://www.osti.gov/servlets/purl/1337684.

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@article{osti_1337684,

  title        = {Hard X-ray polarizer to enable simultaneous three-dimensional nanoscale imaging of magnetic structure and lattice strain},

  author       = {Logan, Jonathan and Harder, Ross and Li, Luxi and Haskel, Daniel and Chen, Pice and Winarski, Robert and Fuesz, Peter and Schlagel, Deborah and Vine, David and Benson, Christa and McNulty, Ian},

  abstractNote = {Recent progress in the development of dichroic Bragg coherent diffractive imaging, a new technique for simultaneous three-dimensional imaging of strain and magnetization at the nanoscale, is reported. This progress includes the installation of a diamond X-ray phase retarder at beamline 34-ID-C of the Advanced Photon Source. The performance of the phase retarder for tuning X-ray polarization is demonstrated with temperature-dependent X-ray magnetic circular dichroism measurements on a gadolinium foil in transmission and on a Gd5Si2Ge2crystal in diffraction geometry with a partially coherent, focused X-ray beam. Feasibility tests for dichroic Bragg coherent diffractive imaging are presented. These tests include (1) using conventional Bragg coherent diffractive imaging to determine whether the phase retarder introduces aberrations using a nonmagnetic gold nanocrystal as a control sample, and (2) collecting coherent diffraction patterns of a magnetic Gd5Si2Ge2nanocrystal with left- and right-circularly polarized X-rays. Future applications of dichroic Bragg coherent diffractive imaging for the correlation of strain and lattice defects with magnetic ordering and inhomogeneities are considered.},

  doi          = {10.1107/S1600577516009632},

  journal      = {Journal of Synchrotron Radiation (Online)},

  number       = 5,

  volume       = 23,

  place        = {United States},

  year         = {Fri Jan 01 00:00:00 EST 2016},

  month        = {Fri Jan 01 00:00:00 EST 2016}

}

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Title: Hard X-ray polarizer to enable simultaneous three-dimensional nanoscale imaging of magnetic structure and lattice strain

Abstract

Citation Formats

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A hard X-ray nanoprobe beamline for nanoscale microscopy journal, September 2012

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