Organic-Free Synthesis of a Highly Siliceous Faujasite Zeolite with Spatially-Biased Q4(n Al) Si Speciation

Oleksiak, Matthew D.; Muraoka, Koki; Hsieh, Ming-Feng; Conato, Marlon T.; Shimojima, Atsushi; Okubo, Tatsuya; Chaikittisilp, Watcharop; Rimer, Jeffrey D.

doi:10.1002/ange.201702672

Title: Organic-Free Synthesis of a Highly Siliceous Faujasite Zeolite with Spatially-Biased Q⁴(n Al) Si Speciation

Authors:

Oleksiak, Matthew D. ^[1]; Muraoka, Koki ^[2]; Hsieh, Ming-Feng ^[1]; Conato, Marlon T. ^[3]; Shimojima, Atsushi ^[4]; Okubo, Tatsuya ^[2];

^[2];

^[1]

Department of Chemical and Biomolecular Engineering, University of Houston, Houston TX 77204 USA
Department of Chemical System Engineering, The University of Tokyo, Tokyo 113-8656 Japan
Department of Chemical and Biomolecular Engineering, University of Houston, Houston TX 77204 USA, Institute of Chemistry, University of the Philippines, Diliman Quezon City 1101 The Philippines
Department of Applied Chemistry, Waseda University, Tokyo 169-8555 Japan

Publication Date:: 2017-08-25

Sponsoring Org.:: USDOE

OSTI Identifier:: 1376969

Grant/Contract Number:: SC0014468

Resource Type:: Publisher's Accepted Manuscript

Journal Name:: Angewandte Chemie

Additional Journal Information:: Journal Name: Angewandte Chemie; Journal ID: ISSN 0044-8249

Publisher:: German Chemical Society

Country of Publication:: Germany

Language:: English

Citation Formats


                    Oleksiak, Matthew D., Muraoka, Koki, Hsieh, Ming-Feng, Conato, Marlon T., Shimojima, Atsushi, Okubo, Tatsuya, Chaikittisilp, Watcharop, and Rimer, Jeffrey D. Organic-Free Synthesis of a Highly Siliceous Faujasite Zeolite with Spatially-Biased Q4(n Al) Si Speciation.  Germany: N. p., 2017. 
Web.  doi:10.1002/ange.201702672.

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                    Oleksiak, Matthew D., Muraoka, Koki, Hsieh, Ming-Feng, Conato, Marlon T., Shimojima, Atsushi, Okubo, Tatsuya, Chaikittisilp, Watcharop, & Rimer, Jeffrey D. Organic-Free Synthesis of a Highly Siliceous Faujasite Zeolite with Spatially-Biased Q4(n Al) Si Speciation.  Germany.  https://doi.org/10.1002/ange.201702672

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                    Oleksiak, Matthew D., Muraoka, Koki, Hsieh, Ming-Feng, Conato, Marlon T., Shimojima, Atsushi, Okubo, Tatsuya, Chaikittisilp, Watcharop, and Rimer, Jeffrey D. Fri .  
"Organic-Free Synthesis of a Highly Siliceous Faujasite Zeolite with Spatially-Biased Q4(n Al) Si Speciation".  Germany.  https://doi.org/10.1002/ange.201702672.

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@article{osti_1376969,

  title        = {Organic-Free Synthesis of a Highly Siliceous Faujasite Zeolite with Spatially-Biased Q4(n Al) Si Speciation},

  author       = {Oleksiak, Matthew D. and Muraoka, Koki and Hsieh, Ming-Feng and Conato, Marlon T. and Shimojima, Atsushi and Okubo, Tatsuya and Chaikittisilp, Watcharop and Rimer, Jeffrey D.},

  abstractNote = {},

  doi          = {10.1002/ange.201702672},

  journal      = {Angewandte Chemie},

  number       = ,

  volume       = ,

  place        = {Germany},

  year         = {2017},

  month        = {8}

}

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Works referenced in this record:

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Title: Organic-Free Synthesis of a Highly Siliceous Faujasite Zeolite with Spatially-Biased Q4(n Al) Si Speciation

Citation Formats

Nanoscale Control of Homoepitaxial Growth on a Two-Dimensional Zeolite journal, December 2016

Cumene-cracking activity of zeolite catalysts I. Effects of ion exchange and silica-to-alumina mole ratio journal, January 1972

Catalytic Oxidation of Methane into Methanol over Copper-Exchanged Zeolites with Oxygen at Low Temperature journal, April 2016

Capturing Ultrasmall EMT Zeolite from Template-Free Systems journal, December 2011

Alkaline cations directing the transformation of FAU zeolites into five different framework types journal, January 2013

Hierarchical Nanomanufacturing: From Shaped Zeolite Nanoparticles to High-Performance Separation Membranes journal, October 2007

Characterization of the silicon-aluminum distribution in synthetic faujasites by high-resolution solid-state silicon-29 NMR journal, September 1982

Improving effect of Fe additive on the catalytic stability of Mo/HZSM-5 in the methane dehydroaromatization journal, May 2012

Template-Framework Interactions in Tetraethylammonium-Directed Zeolite Synthesis journal, November 2016

CO2 capture by solid adsorbents and their applications: current status and new trends journal, January 2011

Framework stabilization of Si-rich LTA zeolite prepared in organic-free media journal, January 2015

Intracrystalline rearrangement of constitutive water in hydrogen zeolite Y journal, November 1967

Location of Alkali Ions and their Relevance to Crystallization of Low Silica X Zeolite journal, August 2010

Quantitatively Probing the Al Distribution in Zeolites journal, May 2014

Catalysis in a Cage: Condition-Dependent Speciation and Dynamics of Exchanged Cu Cations in SSZ-13 Zeolites journal, April 2016

New Synthetic Crystalline Zeolites journal, May 1956

Properties of organic cations that lead to the structure-direction of high-silica molecular sieves journal, June 1996

Aluminum Siting in Silicon-Rich Zeolite Frameworks: A Combined High-Resolution27Al NMR Spectroscopy and Quantum Mechanics / Molecular Mechanics Study of ZSM-5 journal, September 2007

Crystallization of low-solica faujasite () journal, September 1987

Electron Microscopy Reveals the Nucleation Mechanism of Zeolite Y from Precursor Colloids journal, November 1999

Template-Framework Interactions in Tetraethylammonium-Directed Zeolite Synthesis journal, November 2016

Siting and Distribution of Framework Aluminium Atoms in Silicon-Rich Zeolites and Impact on Catalysis journal, April 2012

Nanoscale Control of Homoepitaxial Growth on a Two-Dimensional Zeolite journal, December 2016

Characterization of Li Cations in Zeolite LiX by Solid-State NMR Spectroscopy and Neutron Diffraction journal, August 1998

Effects of low-temperature gel aging on the synthesis of zeolite Y at different alkalinities journal, June 2002

Improving Stability of Zeolites in Aqueous Phase via Selective Removal of Structural Defects journal, March 2016

High temperature synthesis of high silica zeolite Y with good crystallinity in the presence of N-methylpyridinium iodide journal, January 2013

Synthesis of LSX zeolite in the system: Influence of the ratio journal, March 1995

The Hydrothermal Synthesis of Zeolites: History and Development from the Earliest Days to the Present Time journal, March 2003

Variation of the lattice parameter with aluminum content in synthetic sodium faujasites. Evidence for ordering of the framework ions journal, February 1969

Impact of Zeolites on the Petroleum and Petrochemical Industry journal, May 2009

Synthesis of zeolites in the absence of organic structure-directing agents: factors governing crystal selection and polymorphism journal, January 2014

Inorganic molecular sieves: Preparation, modification and industrial application in catalytic processes journal, July 2011

Aluminum Siting in Silicon-Rich Zeolite Frameworks: A Combined High-Resolution27Al NMR Spectroscopy and Quantum Mechanics / Molecular Mechanics Study of ZSM-5 journal, September 2007

Structure-Directing Behaviors of Tetraethylammonium Cations toward Zeolite Beta Revealed by the Evolution of Aluminosilicate Species Formed during the Crystallization Process journal, November 2015

Factors That Control Zeolite L Crystal Size journal, January 2011

Tailoring Silicalite-1 Crystal Morphology with Molecular Modifiers journal, January 2012

Zeolite and molecular sieve synthesis journal, July 1992

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Chemistry of crystalline aluminosilicates. V. Preparation of aluminum-deficient faujasites journal, July 1968

Effect of framework Si/Al ratio and extra-framework aluminum on the catalytic activity of Y zeolite journal, December 2007

Structure and catalytic properties of the most complex intergrown zeolite ITQ-39 determined by electron crystallography journal, January 2012

Controlling Crystal Polymorphism in Organic-Free Synthesis of Na-Zeolites journal, January 2013

Synthesis, characterization, and catalytic properties of silica-rich faujasite-type zeolite (FAU) and its hexagonal analog (EMT) prepared by using crown-ethers as templates journal, February 1992

Aluminosilicate Species in the Hydrogel Phase Formed during the Aging Process for the Crystallization of FAU Zeolite journal, July 2003

Template-free nanosized faujasite-type zeolites journal, January 2015

The Catalytic Cracking of Cumene journal, January 1982

Translating new materials discoveries in zeolite research to commercial manufacture journal, October 2011

Energy Analysis of Aluminosilicate Zeolites with Comprehensive Ranges of Framework Topologies, Chemical Compositions, and Aluminum Distributions journal, May 2016

A Facile Strategy To Design Zeolite L Crystals with Tunable Morphology and Surface Architecture journal, April 2013

Hierarchische Nanofertigung: von geformten Zeolithnanopartikeln zu hochleistungsfähigen Trennmembranen journal, October 2007

Tailoring Silicalite-1 Crystal Morphology with Molecular Modifiers journal, January 2012

Identification of molybdenum oxide nanostructures on zeolites for natural gas conversion journal, April 2015

A Working Hypothesis for Broadening Framework Types of Zeolites in Seed-Assisted Synthesis without Organic Structure-Directing Agent journal, July 2012

Elektronenmikroskopische Untersuchung der Keimbildung von Zeolith Y in kolloidalen Lösungen journal, November 1999

Combining Pre- and Post-Nucleation Trajectories for the Synthesis of High FAU-Content Faujasite Nanocrystals from Organic-Free Sols journal, June 2016

Prediction of crystallization diagrams for synthesis of zeolites journal, July 1999

A combustion-free methodology for synthesizing zeolites and zeolite-like materials journal, September 2003

Title: Organic-Free Synthesis of a Highly Siliceous Faujasite Zeolite with Spatially-Biased Q⁴(n Al) Si Speciation

Nanoscale Control of Homoepitaxial Growth on a Two-Dimensional Zeolite
journal, December 2016

Cumene-cracking activity of zeolite catalysts I. Effects of ion exchange and silica-to-alumina mole ratio
journal, January 1972

Catalytic Oxidation of Methane into Methanol over Copper-Exchanged Zeolites with Oxygen at Low Temperature
journal, April 2016

Capturing Ultrasmall EMT Zeolite from Template-Free Systems
journal, December 2011

Alkaline cations directing the transformation of FAU zeolites into five different framework types
journal, January 2013

Hierarchical Nanomanufacturing: From Shaped Zeolite Nanoparticles to High-Performance Separation Membranes
journal, October 2007

Characterization of the silicon-aluminum distribution in synthetic faujasites by high-resolution solid-state silicon-29 NMR
journal, September 1982

Improving effect of Fe additive on the catalytic stability of Mo/HZSM-5 in the methane dehydroaromatization
journal, May 2012

Template-Framework Interactions in Tetraethylammonium-Directed Zeolite Synthesis
journal, November 2016

CO2 capture by solid adsorbents and their applications: current status and new trends
journal, January 2011

Framework stabilization of Si-rich LTA zeolite prepared in organic-free media
journal, January 2015

Intracrystalline rearrangement of constitutive water in hydrogen zeolite Y
journal, November 1967

Location of Alkali Ions and their Relevance to Crystallization of Low Silica X Zeolite
journal, August 2010

Quantitatively Probing the Al Distribution in Zeolites
journal, May 2014

Catalysis in a Cage: Condition-Dependent Speciation and Dynamics of Exchanged Cu Cations in SSZ-13 Zeolites
journal, April 2016

New Synthetic Crystalline Zeolites
journal, May 1956

Properties of organic cations that lead to the structure-direction of high-silica molecular sieves
journal, June 1996

Aluminum Siting in Silicon-Rich Zeolite Frameworks: A Combined High-Resolution27Al NMR Spectroscopy and Quantum Mechanics / Molecular Mechanics Study of ZSM-5
journal, September 2007

Crystallization of low-solica faujasite ()
journal, September 1987

Electron Microscopy Reveals the Nucleation Mechanism of Zeolite Y from Precursor Colloids
journal, November 1999

Template-Framework Interactions in Tetraethylammonium-Directed Zeolite Synthesis
journal, November 2016

Siting and Distribution of Framework Aluminium Atoms in Silicon-Rich Zeolites and Impact on Catalysis
journal, April 2012

Nanoscale Control of Homoepitaxial Growth on a Two-Dimensional Zeolite
journal, December 2016

Characterization of Li Cations in Zeolite LiX by Solid-State NMR Spectroscopy and Neutron Diffraction
journal, August 1998

Effects of low-temperature gel aging on the synthesis of zeolite Y at different alkalinities
journal, June 2002

Improving Stability of Zeolites in Aqueous Phase via Selective Removal of Structural Defects
journal, March 2016

High temperature synthesis of high silica zeolite Y with good crystallinity in the presence of N-methylpyridinium iodide
journal, January 2013

Synthesis of LSX zeolite in the system: Influence of the ratio
journal, March 1995

The Hydrothermal Synthesis of Zeolites: History and Development from the Earliest Days to the Present Time
journal, March 2003

Variation of the lattice parameter with aluminum content in synthetic sodium faujasites. Evidence for ordering of the framework ions
journal, February 1969

Impact of Zeolites on the Petroleum and Petrochemical Industry
journal, May 2009

Synthesis of zeolites in the absence of organic structure-directing agents: factors governing crystal selection and polymorphism
journal, January 2014

Inorganic molecular sieves: Preparation, modification and industrial application in catalytic processes
journal, July 2011

Aluminum Siting in Silicon-Rich Zeolite Frameworks: A Combined High-Resolution27Al NMR Spectroscopy and Quantum Mechanics / Molecular Mechanics Study of ZSM-5
journal, September 2007

Structure-Directing Behaviors of Tetraethylammonium Cations toward Zeolite Beta Revealed by the Evolution of Aluminosilicate Species Formed during the Crystallization Process
journal, November 2015

Factors That Control Zeolite L Crystal Size
journal, January 2011

Tailoring Silicalite-1 Crystal Morphology with Molecular Modifiers
journal, January 2012

Zeolite and molecular sieve synthesis
journal, July 1992

Calculation of Madelung potentials for faujasite-type zeolites. I
journal, November 1969

Chemistry of crystalline aluminosilicates. V. Preparation of aluminum-deficient faujasites
journal, July 1968

Effect of framework Si/Al ratio and extra-framework aluminum on the catalytic activity of Y zeolite
journal, December 2007

Structure and catalytic properties of the most complex intergrown zeolite ITQ-39 determined by electron crystallography
journal, January 2012

Controlling Crystal Polymorphism in Organic-Free Synthesis of Na-Zeolites
journal, January 2013

Synthesis, characterization, and catalytic properties of silica-rich faujasite-type zeolite (FAU) and its hexagonal analog (EMT) prepared by using crown-ethers as templates
journal, February 1992

Aluminosilicate Species in the Hydrogel Phase Formed during the Aging Process for the Crystallization of FAU Zeolite
journal, July 2003

Template-free nanosized faujasite-type zeolites
journal, January 2015

The Catalytic Cracking of Cumene
journal, January 1982

Translating new materials discoveries in zeolite research to commercial manufacture
journal, October 2011

Energy Analysis of Aluminosilicate Zeolites with Comprehensive Ranges of Framework Topologies, Chemical Compositions, and Aluminum Distributions
journal, May 2016

A Facile Strategy To Design Zeolite L Crystals with Tunable Morphology and Surface Architecture
journal, April 2013

Hierarchische Nanofertigung: von geformten Zeolithnanopartikeln zu hochleistungsfähigen Trennmembranen
journal, October 2007

Tailoring Silicalite-1 Crystal Morphology with Molecular Modifiers
journal, January 2012

Identification of molybdenum oxide nanostructures on zeolites for natural gas conversion
journal, April 2015

A Working Hypothesis for Broadening Framework Types of Zeolites in Seed-Assisted Synthesis without Organic Structure-Directing Agent
journal, July 2012

Elektronenmikroskopische Untersuchung der Keimbildung von Zeolith Y in kolloidalen Lösungen
journal, November 1999

Combining Pre- and Post-Nucleation Trajectories for the Synthesis of High FAU-Content Faujasite Nanocrystals from Organic-Free Sols
journal, June 2016

Prediction of crystallization diagrams for synthesis of zeolites
journal, July 1999

A combustion-free methodology for synthesizing zeolites and zeolite-like materials
journal, September 2003