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Title: Micro-beam Laue alignment of multi-reflection Bragg coherent diffraction imaging measurements

Multi-reflection Bragg coherent diffraction imaging has the potential to allow three-dimensional (3D) resolved measurements of the full lattice strain tensor in specific micro-crystals. Until now such measurements were hampered by the need for laborious, time-intensive alignment procedures. Here, in this paper, a different approach is demonstrated, using micro-beam Laue X-ray diffraction to first determine the lattice orientation of the micro-crystal. This information is then used to rapidly align coherent diffraction measurements of three or more reflections from the crystal. Based on these, 3D strain and stress fields in the crystal are successfully determined. This approach is demonstrated on a focused ion beam milled micro-crystal from which six reflections could be measured. Since information from more than three independent reflections is available, the reliability of the phases retrieved from the coherent diffraction data can be assessed. Lastly, our results show that rapid, reliable 3D coherent diffraction measurements of the full lattice strain tensor in specific micro-crystals are now feasible and can be successfully carried out even in heavily distorted samples.
Authors:
 [1] ; ORCiD logo [2] ; ORCiD logo [3] ;  [3] ;  [4] ; ORCiD logo [5] ;  [6]
  1. Univ. of Oxford (United Kingdom). Department of Engineering Science
  2. La Trobe University (Australia). Department of Chemistry and Physics; CSIRO Manufacturing Flagship, Parkville (Australia)
  3. Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
  4. SLAC National Accelerator Lab., Menlo Park, CA (United States). Stanford PULSE Institute
  5. Brookhaven National Lab. (BNL), Upton, NY (United States)
  6. La Trobe University (Australia). Department of Chemistry and Physics
Publication Date:
Report Number(s):
BNL-114072-2017-JA
Journal ID: ISSN 1600-5775; R&D Project: PO011; KC0201060
Grant/Contract Number:
SC0012704; AC02-06CH11357
Type:
Accepted Manuscript
Journal Name:
Journal of Synchrotron Radiation (Online)
Additional Journal Information:
Journal Name: Journal of Synchrotron Radiation (Online); Journal Volume: 24; Journal Issue: 5; Journal ID: ISSN 1600-5775
Publisher:
International Union of Crystallography
Research Org:
Brookhaven National Laboratory (BNL), Upton, NY (United States); Argonne National Lab. (ANL), Argonne, IL (United States)
Sponsoring Org:
USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22); Engineering and Physical Sciences Research Council (EPSRC); European Research Council (ERC); Argonne National Laboratory, Advanced Photon Source
Country of Publication:
United States
Language:
English
Subject:
75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY; 36 MATERIALS SCIENCE; Bragg coherent diffraction imaging; micro-beam Laue diffraction; ion implantation; strain tensor measurement
OSTI Identifier:
1376135
Alternate Identifier(s):
OSTI ID: 1474149

Hofmann, Felix, Phillips, Nicholas W., Harder, Ross J., Liu, Wenjun, Clark, Jesse N., Robinson, Ian K., and Abbey, Brian. Micro-beam Laue alignment of multi-reflection Bragg coherent diffraction imaging measurements. United States: N. p., Web. doi:10.1107/S1600577517009183.
Hofmann, Felix, Phillips, Nicholas W., Harder, Ross J., Liu, Wenjun, Clark, Jesse N., Robinson, Ian K., & Abbey, Brian. Micro-beam Laue alignment of multi-reflection Bragg coherent diffraction imaging measurements. United States. doi:10.1107/S1600577517009183.
Hofmann, Felix, Phillips, Nicholas W., Harder, Ross J., Liu, Wenjun, Clark, Jesse N., Robinson, Ian K., and Abbey, Brian. 2017. "Micro-beam Laue alignment of multi-reflection Bragg coherent diffraction imaging measurements". United States. doi:10.1107/S1600577517009183. https://www.osti.gov/servlets/purl/1376135.
@article{osti_1376135,
title = {Micro-beam Laue alignment of multi-reflection Bragg coherent diffraction imaging measurements},
author = {Hofmann, Felix and Phillips, Nicholas W. and Harder, Ross J. and Liu, Wenjun and Clark, Jesse N. and Robinson, Ian K. and Abbey, Brian},
abstractNote = {Multi-reflection Bragg coherent diffraction imaging has the potential to allow three-dimensional (3D) resolved measurements of the full lattice strain tensor in specific micro-crystals. Until now such measurements were hampered by the need for laborious, time-intensive alignment procedures. Here, in this paper, a different approach is demonstrated, using micro-beam Laue X-ray diffraction to first determine the lattice orientation of the micro-crystal. This information is then used to rapidly align coherent diffraction measurements of three or more reflections from the crystal. Based on these, 3D strain and stress fields in the crystal are successfully determined. This approach is demonstrated on a focused ion beam milled micro-crystal from which six reflections could be measured. Since information from more than three independent reflections is available, the reliability of the phases retrieved from the coherent diffraction data can be assessed. Lastly, our results show that rapid, reliable 3D coherent diffraction measurements of the full lattice strain tensor in specific micro-crystals are now feasible and can be successfully carried out even in heavily distorted samples.},
doi = {10.1107/S1600577517009183},
journal = {Journal of Synchrotron Radiation (Online)},
number = 5,
volume = 24,
place = {United States},
year = {2017},
month = {8}
}