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Title: Effect of defects, magnetocrystalline anisotropy, and shape anisotropy on magnetic structure of iron thin films by magnetic force microscopy

Abstract

Microstructures of magnetic materials, including defects and crystallographic orientations, are known to strongly influence magnetic domain structures. Measurement techniques such as magnetic force microscopy (MFM) thus allow study of correlations between microstructural and magnetic properties. The present work probes effects of anisotropy and artificial defects on the evolution of domain structure with applied field. Single crystal iron thin films on MgO substrates were milled by Focused Ion Beam (FIB) to create different magnetically isolated squares and rectangles in [110] crystallographic orientations, having their easy axis 45° from the sample edge. To investigate domain wall response on encountering non-magnetic defects, a 150 nm diameter hole was created in the center of some samples. By simultaneously varying crystal orientation and shape, both magnetocrystalline anisotropy and shape anisotropy, as well as their interaction, could be studied. Shape anisotropy was found to be important primarily for the longer edge of rectangular samples, which exaggerated the FIB edge effects and provided nucleation sites for spike domains in non-easy axis oriented samples. Center holes acted as pinning sites for domain walls until large applied magnetic fields. The present studies are aimed at deepening the understanding of the propagation of different types of domain walls in themore » presence of defects and different crystal orientations.« less

Authors:
 [1];  [2];  [2];  [2]; ORCiD logo [1]
  1. Washington State Univ., Pullman, WA (United States)
  2. Pacific Northwest National Lab. (PNNL), Richland, WA (United States)
Publication Date:
Research Org.:
Pacific Northwest National Laboratory (PNNL), Richland, WA (United States). Environmental Molecular Sciences Laboratory (EMSL)
Sponsoring Org.:
USDOE Office of Nuclear Energy (NE); USDOE Office of Science (SC), Biological and Environmental Research (BER)
OSTI Identifier:
1372997
Report Number(s):
PNNL-SA-123819
Journal ID: ISSN 2158-3226; 49202; NT0104000
Grant/Contract Number:  
AC05-76RL01830
Resource Type:
Accepted Manuscript
Journal Name:
AIP Advances
Additional Journal Information:
Journal Volume: 7; Journal Issue: 5; Journal ID: ISSN 2158-3226
Publisher:
American Institute of Physics (AIP)
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; magnetic structure; iron thin films; magnetic force microscopy; defects; Environmental Molecular Sciences Laboratory

Citation Formats

Xu, Ke, Schreiber, Daniel K., Li, Yulan, Johnson, Bradley R., and McCloy, John. Effect of defects, magnetocrystalline anisotropy, and shape anisotropy on magnetic structure of iron thin films by magnetic force microscopy. United States: N. p., 2017. Web. doi:10.1063/1.4976580.
Xu, Ke, Schreiber, Daniel K., Li, Yulan, Johnson, Bradley R., & McCloy, John. Effect of defects, magnetocrystalline anisotropy, and shape anisotropy on magnetic structure of iron thin films by magnetic force microscopy. United States. https://doi.org/10.1063/1.4976580
Xu, Ke, Schreiber, Daniel K., Li, Yulan, Johnson, Bradley R., and McCloy, John. Fri . "Effect of defects, magnetocrystalline anisotropy, and shape anisotropy on magnetic structure of iron thin films by magnetic force microscopy". United States. https://doi.org/10.1063/1.4976580. https://www.osti.gov/servlets/purl/1372997.
@article{osti_1372997,
title = {Effect of defects, magnetocrystalline anisotropy, and shape anisotropy on magnetic structure of iron thin films by magnetic force microscopy},
author = {Xu, Ke and Schreiber, Daniel K. and Li, Yulan and Johnson, Bradley R. and McCloy, John},
abstractNote = {Microstructures of magnetic materials, including defects and crystallographic orientations, are known to strongly influence magnetic domain structures. Measurement techniques such as magnetic force microscopy (MFM) thus allow study of correlations between microstructural and magnetic properties. The present work probes effects of anisotropy and artificial defects on the evolution of domain structure with applied field. Single crystal iron thin films on MgO substrates were milled by Focused Ion Beam (FIB) to create different magnetically isolated squares and rectangles in [110] crystallographic orientations, having their easy axis 45° from the sample edge. To investigate domain wall response on encountering non-magnetic defects, a 150 nm diameter hole was created in the center of some samples. By simultaneously varying crystal orientation and shape, both magnetocrystalline anisotropy and shape anisotropy, as well as their interaction, could be studied. Shape anisotropy was found to be important primarily for the longer edge of rectangular samples, which exaggerated the FIB edge effects and provided nucleation sites for spike domains in non-easy axis oriented samples. Center holes acted as pinning sites for domain walls until large applied magnetic fields. The present studies are aimed at deepening the understanding of the propagation of different types of domain walls in the presence of defects and different crystal orientations.},
doi = {10.1063/1.4976580},
journal = {AIP Advances},
number = 5,
volume = 7,
place = {United States},
year = {Fri Feb 10 00:00:00 EST 2017},
month = {Fri Feb 10 00:00:00 EST 2017}
}

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Works referenced in this record:

Evaluation of thermal recovery of neutron-irradiated SA508-3 steel using magnetic property measurements
journal, January 1997

  • Park, Duck-Gun; Hong, Hun-Hwa; Kim, In-Sup
  • Journal of Materials Science, Vol. 32, Issue 23, p. 6141-6146
  • DOI: 10.1023/a:1018608321067

Magnetic imaging in the presence of an external field: erasure process of thin film recording medium
journal, January 1995

  • Gomez, R. D.; Mayergoyz, I. D.; Burke, E. R.
  • IEEE Transactions on Magnetics, Vol. 31, Issue 6
  • DOI: 10.1109/20.490377

Structuring of Permalloy by means of Electron-beam Lithography and Focused Ion Beam Milling
journal, September 2007

  • Getlawi, S.; Koblischka, M. R.; Soldera, F.
  • Microscopy and Microanalysis, Vol. 13, Issue S03
  • DOI: 10.1017/s1431927607081792

Hysteresis in single and polycrystalline iron thin films: Major and minor loops, first order reversal curves, and Preisach modeling
journal, December 2015


Micromagnetism and magnetization reversal of micron-scale (110) Fe thin-film magnetic elements
journal, September 1999


TEM Sample Preparation and FIB-Induced Damage
journal, May 2007

  • Mayer, Joachim; Giannuzzi, Lucille A.; Kamino, Takeo
  • MRS Bulletin, Vol. 32, Issue 5
  • DOI: 10.1557/mrs2007.63

Development of high coercivity magnetic force microscopy tips
journal, December 1998


Computational and experimental investigations of magnetic domain structures in patterned magnetic thin films
journal, July 2015


Domain configuration and magnetization switching in arrays of permalloy nanostripes
journal, April 2014

  • Iglesias-Freire, Ó.; Jaafar, M.; Pérez, L.
  • Journal of Magnetism and Magnetic Materials, Vol. 355
  • DOI: 10.1016/j.jmmm.2013.12.012

Direct comparison of domain wall behavior in permalloy nanowires patterned by electron beam lithography and focused ion beam milling
journal, October 2011

  • Basith, M. A.; McVitie, S.; McGrouther, D.
  • Journal of Applied Physics, Vol. 110, Issue 8
  • DOI: 10.1063/1.3642966

Meso-scale magnetic signatures for nuclear reactor steel irradiation embrittlement monitoring
conference, January 2015

  • Suter, J. D.; Ramuhalli, P.; McCloy, J. S.
  • 41ST ANNUAL REVIEW OF PROGRESS IN QUANTITATIVE NONDESTRUCTIVE EVALUATION: Volume 34, AIP Conference Proceedings
  • DOI: 10.1063/1.4914765

Characterization of hydrogen-induced crack initiation in metastable austenitic stainless steels during deformation
journal, September 2010

  • Zhang, L.; An, B.; Fukuyama, S.
  • Journal of Applied Physics, Vol. 108, Issue 6
  • DOI: 10.1063/1.3477321

Works referencing / citing this record:

Staggered magnetic nanowire devices for effective domain-wall pinning in racetrack memory
text, January 2019