Template-Free Synthesis of Hollow-Structured Co3O4 Nanoparticles as High-Performance Anodes for Lithium-Ion Batteries
Abstract
We have developed a template-free procedure to synthesize Co3O4 hollow-structured nanoparticles on a Vulcan XC-72 carbon support. The material was synthesized via an impregnation–reduction method followed by air oxidation. In contrast to spherical particles, the hollow-structured Co3O4 nanoparticles exhibited excellent lithium storage capacity, rate capability, and cycling stability when used as the anode material in lithium-ion batteries. Electrochemical testing showed that the hollow-structured Co3O4 particles delivered a stable reversible capacity of about 880 mAh/g (near the theoretical capacity of 890 mAh/g) at a current density of 50 mA/g after 50 cycles. Lastly, the superior electrochemical performance is attributed to its unique hollow structure, which combines nano- and microscale properties that facilitate electron transfer and enhance structural robustness.
- Authors:
-
- Huazhong Univ. of Science & Technology, Wuhan (China)
- Cornell Univ., Ithaca, NY (United States)
- Publication Date:
- Research Org.:
- Energy Frontier Research Centers (EFRC) (United States). Energy Materials Center at Cornell (EMC2)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES); Natural Science Foundation of China; Program for New Century Excellent Talents in Universities of China; Doctoral Fund of Ministry of Education of China; Fundamental Research Funds for the Central Univ.
- OSTI Identifier:
- 1370462
- Grant/Contract Number:
- SC0001086; FG02-87ER45298; 21306060; NCET-13-0237; 20130142120039; 2013TS136; 2014YQ009
- Resource Type:
- Accepted Manuscript
- Journal Name:
- ACS Nano
- Additional Journal Information:
- Journal Volume: 9; Journal Issue: 2; Related Information: Emc2 partners with Cornell University (lead); Lawrence Berkeley National Laboratory; Journal ID: ISSN 1936-0851
- Publisher:
- American Chemical Society (ACS)
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 25 ENERGY STORAGE; 36 MATERIALS SCIENCE; anode materials; cobalt oxides; electrochemistry; hollowed structure; lithium battery; nanoparticles; electrical properties; electrodes; hollow structures materials
Citation Formats
Wang, Deli, Yu, Yingchao, He, Huan, Wang, Jie, Zhou, Weidong, and Abruña, Hector D. Template-Free Synthesis of Hollow-Structured Co3O4 Nanoparticles as High-Performance Anodes for Lithium-Ion Batteries. United States: N. p., 2015.
Web. doi:10.1021/nn506624g.
Wang, Deli, Yu, Yingchao, He, Huan, Wang, Jie, Zhou, Weidong, & Abruña, Hector D. Template-Free Synthesis of Hollow-Structured Co3O4 Nanoparticles as High-Performance Anodes for Lithium-Ion Batteries. United States. https://doi.org/10.1021/nn506624g
Wang, Deli, Yu, Yingchao, He, Huan, Wang, Jie, Zhou, Weidong, and Abruña, Hector D. Tue .
"Template-Free Synthesis of Hollow-Structured Co3O4 Nanoparticles as High-Performance Anodes for Lithium-Ion Batteries". United States. https://doi.org/10.1021/nn506624g. https://www.osti.gov/servlets/purl/1370462.
@article{osti_1370462,
title = {Template-Free Synthesis of Hollow-Structured Co3O4 Nanoparticles as High-Performance Anodes for Lithium-Ion Batteries},
author = {Wang, Deli and Yu, Yingchao and He, Huan and Wang, Jie and Zhou, Weidong and Abruña, Hector D.},
abstractNote = {We have developed a template-free procedure to synthesize Co3O4 hollow-structured nanoparticles on a Vulcan XC-72 carbon support. The material was synthesized via an impregnation–reduction method followed by air oxidation. In contrast to spherical particles, the hollow-structured Co3O4 nanoparticles exhibited excellent lithium storage capacity, rate capability, and cycling stability when used as the anode material in lithium-ion batteries. Electrochemical testing showed that the hollow-structured Co3O4 particles delivered a stable reversible capacity of about 880 mAh/g (near the theoretical capacity of 890 mAh/g) at a current density of 50 mA/g after 50 cycles. Lastly, the superior electrochemical performance is attributed to its unique hollow structure, which combines nano- and microscale properties that facilitate electron transfer and enhance structural robustness.},
doi = {10.1021/nn506624g},
journal = {ACS Nano},
number = 2,
volume = 9,
place = {United States},
year = {Tue Jan 20 00:00:00 EST 2015},
month = {Tue Jan 20 00:00:00 EST 2015}
}
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