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Title: Low-power broadband solid-state MAS NMR of 14 N

Authors:
 [1];  [2];  [3];  [2];  [1]
  1. Department of Chemistry, University of Cambridge, Lensfield Road, Cambridge CB2 1EW, United Kingdom
  2. Centre de RMN à Très Hauts Champs, Institut des Sciences Analytiques (CNRS, ENS Lyon, UCB Lyon 1), Université de Lyon, 69100 Villeurbanne, France
  3. Bruker BioSpin GmbH, D 76287 Rheinstetten, Germany
Publication Date:
Sponsoring Org.:
USDOE
OSTI Identifier:
1361885
Grant/Contract Number:  
AC02-05CH11231
Resource Type:
Publisher's Accepted Manuscript
Journal Name:
Journal of Chemical Physics
Additional Journal Information:
Journal Name: Journal of Chemical Physics Journal Volume: 146 Journal Issue: 19; Journal ID: ISSN 0021-9606
Publisher:
American Institute of Physics
Country of Publication:
United States
Language:
English

Citation Formats

Pell, Andrew J., Sanders, Kevin J., Wegner, Sebastian, Pintacuda, Guido, and Grey, Clare P. Low-power broadband solid-state MAS NMR of 14 N. United States: N. p., 2017. Web. doi:10.1063/1.4983220.
Pell, Andrew J., Sanders, Kevin J., Wegner, Sebastian, Pintacuda, Guido, & Grey, Clare P. Low-power broadband solid-state MAS NMR of 14 N. United States. doi:10.1063/1.4983220.
Pell, Andrew J., Sanders, Kevin J., Wegner, Sebastian, Pintacuda, Guido, and Grey, Clare P. Sun . "Low-power broadband solid-state MAS NMR of 14 N". United States. doi:10.1063/1.4983220.
@article{osti_1361885,
title = {Low-power broadband solid-state MAS NMR of 14 N},
author = {Pell, Andrew J. and Sanders, Kevin J. and Wegner, Sebastian and Pintacuda, Guido and Grey, Clare P.},
abstractNote = {},
doi = {10.1063/1.4983220},
journal = {Journal of Chemical Physics},
number = 19,
volume = 146,
place = {United States},
year = {2017},
month = {5}
}

Journal Article:
Free Publicly Available Full Text
Publisher's Version of Record
DOI: 10.1063/1.4983220

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Cited by: 2 works
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Works referenced in this record:

Investigations of a nonrandom numerical method for multidimensional integration
journal, October 1973

  • Cheng, Vera B.; Suzukawa, Henry H.; Wolfsberg, Max
  • The Journal of Chemical Physics, Vol. 59, Issue 8
  • DOI: 10.1063/1.1680590

Rotational echo 14 N/ 13 C/ 1 H triple resonance solid‐state nuclear magnetic resonance: A probe of 13 C– 14 N internuclear distances
journal, May 1993

  • Grey, Clare P.; Veeman, Wiebren S.; Vega, Alexander J.
  • The Journal of Chemical Physics, Vol. 98, Issue 10
  • DOI: 10.1063/1.464579

13C/14N heteronuclear multiple-quantum correlation with rotary resonance and REDOR dipolar recoupling
journal, January 2007


Theoretical aspects of higher‐order truncations in solid‐state nuclear magnetic resonance
journal, December 1992

  • Goldman, M.; Grandinetti, P. J.; Llor, A.
  • The Journal of Chemical Physics, Vol. 97, Issue 12
  • DOI: 10.1063/1.463321

NMR in rotating solids
journal, April 1979

  • Maricq, M. Matti; Waugh, J. S.
  • The Journal of Chemical Physics, Vol. 70, Issue 7
  • DOI: 10.1063/1.437915

Broadband excitation and indirect detection of nitrogen-14 in rotating solids using Delays Alternating with Nutation (DANTE)
journal, September 2011

  • Vitzthum, Veronika; Caporini, Marc A.; Ulzega, Simone
  • Journal of Magnetic Resonance, Vol. 212, Issue 1
  • DOI: 10.1016/j.jmr.2011.06.013

The application of tensor operators in the analysis of EPR and ENDOR spectra
journal, September 1972

  • Buckmaster, H. A.; Chatterjee, R.; Shing, Y. H.
  • Physica Status Solidi (a), Vol. 13, Issue 1
  • DOI: 10.1002/pssa.2210130102

Generalized Perturbation Theory in Operator Form
journal, July 1963


Structural information from quadrupolar nuclei in solid state NMR
journal, January 2006

  • Ashbrook, Sharon E.; Duer, Melinda J.
  • Concepts in Magnetic Resonance Part A, Vol. 28A, Issue 3
  • DOI: 10.1002/cmr.a.20053

Frequency-stepped acquisition in nuclear magnetic resonance spectroscopy under magic angle spinning
journal, March 2013

  • Pell, Andrew J.; Clément, Raphaële J.; Grey, Clare P.
  • The Journal of Chemical Physics, Vol. 138, Issue 11
  • DOI: 10.1063/1.4795001

Proton-Selective 17 O− 1 H Distance Measurements in Fast Magic-Angle-Spinning Solid-State NMR Spectroscopy for the Determination of Hydrogen Bond Lengths
journal, November 2006

  • Brinkmann, Andreas; Kentgens, Arno P. M.
  • Journal of the American Chemical Society, Vol. 128, Issue 46
  • DOI: 10.1021/ja065415k

14 N overtone NMR spectra under magic angle spinning: Experiments and numerically exact simulations
journal, February 2013

  • O’Dell, Luke A.; Brinkmann, Andreas
  • The Journal of Chemical Physics, Vol. 138, Issue 6
  • DOI: 10.1063/1.4775592

Nitrogen-14 NMR Spectroscopy Using Residual Dipolar Splittings in Solids
journal, June 2006

  • Cavadini, Simone; Lupulescu, Adonis; Antonijevic, Sasa
  • Journal of the American Chemical Society, Vol. 128, Issue 24
  • DOI: 10.1021/ja0618898

Evidence for Dynamics on a 100 ns Time Scale from Single- and Double-Quantum Nitrogen-14 NMR in Solid Peptides
journal, August 2008

  • Cavadini, Simone; Abraham, Anuji; Ulzega, Simone
  • Journal of the American Chemical Society, Vol. 130, Issue 33
  • DOI: 10.1021/ja802603q

Adiabatic Pulses for Wideband Inversion and Broadband Decoupling
journal, August 1995

  • Kupce, E.; Freeman, R.
  • Journal of Magnetic Resonance, Series A, Vol. 115, Issue 2
  • DOI: 10.1006/jmra.1995.1179

14N magic angle spinning overtone NMR spectra
journal, September 2011


Sensitivity enhancement of solid-state NMR spectra of half-integer spin quadrupolar nuclei: Double- or single-frequency sweeps? Insights from the hyperbolic secant experiment
journal, January 2008

  • Nakashima, Thomas T.; Wasylishen, Roderick E.; Siegel, Renée
  • Chemical Physics Letters, Vol. 450, Issue 4-6
  • DOI: 10.1016/j.cplett.2007.11.032

Solid-state14N MAS NMR of ammonium ions as a spy to structural insights for ammonium salts
journal, January 2006

  • Jakobsen, Hans J.; Hove, Anders R.; Hazell, Rita G.
  • Magnetic Resonance in Chemistry, Vol. 44, Issue 3
  • DOI: 10.1002/mrc.1772

Indirect Detection of Nitrogen-14 in Solid-State NMR Spectroscopy
journal, June 2007

  • Cavadini, Simone; Antonijevic, Sasa; Lupulescu, Adonis
  • ChemPhysChem, Vol. 8, Issue 9
  • DOI: 10.1002/cphc.200700049

Fast Broadband Inversion by Adiabatic Pulses
journal, July 1998

  • Hwang, Tsang-Lin; van Zijl, Peter C. M.; Garwood, Michael
  • Journal of Magnetic Resonance, Vol. 133, Issue 1
  • DOI: 10.1006/jmre.1998.1441

Rotary resonance echo double resonance for measuring heteronuclear dipolar coupling under MAS
journal, December 2006


Symmetry pathways in solid-state NMR
journal, August 2011

  • Grandinetti, Philip J.; Ash, Jason T.; Trease, Nicole M.
  • Progress in Nuclear Magnetic Resonance Spectroscopy, Vol. 59, Issue 2
  • DOI: 10.1016/j.pnmrs.2010.11.003

Sensitivity enhancement of NMR spectra of half-integer spin quadrupolar nuclei in solids using hyperbolic secant pulses
journal, January 2007

  • Siegel, Renée; Nakashima, Thomas T.; Wasylishen, Roderick E.
  • Journal of Magnetic Resonance, Vol. 184, Issue 1
  • DOI: 10.1016/j.jmr.2006.09.007

Spectral editing in solid-state MAS NMR of quadrupolar nuclei using selective satellite inversion
journal, April 2007


Excitation Sculpting in High-Resolution Nuclear Magnetic Resonance Spectroscopy: Application to Selective NOE Experiments
journal, April 1995

  • Stott, Katherine; Stonehouse, Jonathan; Keeler, James
  • Journal of the American Chemical Society, Vol. 117, Issue 14
  • DOI: 10.1021/ja00119a048

Acquisition of ultra-wideline NMR spectra from quadrupolar nuclei by frequency stepped WURST–QCPMG
journal, January 2009


Isotropic NMR Spectra of Half-Integer Quadrupolar Nuclei Using Satellite Transitions and Magic-Angle Spinning
journal, April 2000

  • Gan, Zhehong
  • Journal of the American Chemical Society, Vol. 122, Issue 13
  • DOI: 10.1021/ja9939791

2H double-quantum MAS NMR spectroscopy as a probe of dynamics on the microsecond timescale in solids
journal, June 2006


Floquet theory in solid-state nuclear magnetic resonance
journal, November 2010

  • Leskes, Michal; Madhu, P. K.; Vega, Shimon
  • Progress in Nuclear Magnetic Resonance Spectroscopy, Vol. 57, Issue 4
  • DOI: 10.1016/j.pnmrs.2010.06.002

Solid-state nuclear magnetic resonance spectra of dipolar-coupled multi-spin systems under fast magic angle spinning
journal, January 1999

  • Filip, Claudiu; Hafner, Siegfried; Schnell, Ingo
  • The Journal of Chemical Physics, Vol. 110, Issue 1
  • DOI: 10.1063/1.478135

The Return of the Frequency Sweep: Designing Adiabatic Pulses for Contemporary NMR
journal, December 2001

  • Garwood, Michael; DelaBarre, Lance
  • Journal of Magnetic Resonance, Vol. 153, Issue 2
  • DOI: 10.1006/jmre.2001.2340

Fictitious spin 1/2 operator formalism for multiple quantum NMR
journal, June 1978

  • Vega, Shimon
  • The Journal of Chemical Physics, Vol. 68, Issue 12
  • DOI: 10.1063/1.435679

Theory and applications of supercycled symmetry-based recoupling sequences in solid-state nuclear magnetic resonance
journal, June 2006

  • Kristiansen, Per Eugen; Carravetta, Marina; van Beek, Jacco D.
  • The Journal of Chemical Physics, Vol. 124, Issue 23
  • DOI: 10.1063/1.2205857

Pulse sequence symmetries in the nuclear magnetic resonance of spinning solids: Application to heteronuclear decoupling
journal, July 1999

  • Edén, Mattias; Levitt, Malcolm H.
  • The Journal of Chemical Physics, Vol. 111, Issue 4
  • DOI: 10.1063/1.479410

Good lattice points, discrepancy, and numerical integration
journal, December 1966

  • Zaremba, S. K.
  • Annali di Matematica Pura ed Applicata, Series 4, Vol. 73, Issue 1
  • DOI: 10.1007/bf02415091

Water Suppression That Works. Excitation Sculpting Using Arbitrary Wave-Forms and Pulsed-Field Gradients
journal, February 1995

  • Hwang, T. L.; Shaka, A. J.
  • Journal of Magnetic Resonance, Series A, Vol. 112, Issue 2
  • DOI: 10.1006/jmra.1995.1047

Broadband solid-state MAS NMR of paramagnetic systems
journal, February 2015


Selective pulse experiments in high-resolution solid state NMR
journal, October 1983


Proton-detected nitrogen-14 NMR by recoupling of heteronuclear dipolar interactions using symmetry-based sequences
journal, September 2007


Fast and Simple Acquisition of Solid-State 14 N NMR Spectra with Signal Enhancement via Population Transfer
journal, May 2009

  • O’Dell, Luke A.; Schurko, Robert W.
  • Journal of the American Chemical Society, Vol. 131, Issue 19
  • DOI: 10.1021/ja901278q

Using hyperbolic secant pulses to assist characterization of chemical shift tensors for half-integer spin quadrupolar nuclei in MAS powder samples
journal, June 2009

  • Nakashima, Thomas T.; Teymoori, Roshanak; Wasylishen, Roderick E.
  • Magnetic Resonance in Chemistry, Vol. 47, Issue 6
  • DOI: 10.1002/mrc.2413

Why do spinning sidebands have the same phase?
journal, April 1989


Fast adiabatic pulses for solid-state NMR of paramagnetic systems
journal, February 2007


Spin-Transfer Pathways in Paramagnetic Lithium Transition-Metal Phosphates from Combined Broadband Isotropic Solid-State MAS NMR Spectroscopy and DFT Calculations
journal, October 2012

  • Clément, Raphaële J.; Pell, Andrew J.; Middlemiss, Derek S.
  • Journal of the American Chemical Society, Vol. 134, Issue 41
  • DOI: 10.1021/ja306876u

Absence of Curie Relaxation in Paramagnetic Solids Yields Long 1 H Coherence Lifetimes
journal, November 2007

  • Kervern, Gwendal; Steuernagel, Stefan; Engelke, Frank
  • Journal of the American Chemical Society, Vol. 129, Issue 46
  • DOI: 10.1021/ja075319z

Optimized Adiabatic Pulses for Wideband Spin Inversion
journal, February 1996

  • Kupce, Ēriks; Freeman, Ray
  • Journal of Magnetic Resonance, Series A, Vol. 118, Issue 2
  • DOI: 10.1006/jmra.1996.0042

Single crystal nuclear magnetic resonance in spinning powders
journal, October 2011

  • Pell, Andrew J.; Pintacuda, Guido; Emsley, Lyndon
  • The Journal of Chemical Physics, Vol. 135, Issue 14
  • DOI: 10.1063/1.3640418

Compensating Pulse Imperfections in Solid-State NMR Spectroscopy: A Key to Better Reproducibility and Performance
journal, August 2015

  • Wittmann, Johannes J.; Takeda, Kazuyuki; Meier, Beat H.
  • Angewandte Chemie International Edition, Vol. 54, Issue 43
  • DOI: 10.1002/anie.201504782

Broadband and adiabatic inversion of a two-level system by phase-modulated pulses
journal, December 1985


Measuring Amide Nitrogen Quadrupolar Coupling by High-Resolution 14 N/ 13 C NMR Correlation under Magic-Angle Spinning
journal, May 2006

  • Gan, Zhehong
  • Journal of the American Chemical Society, Vol. 128, Issue 18
  • DOI: 10.1021/ja0578597

Coherent Averaging Effects in Magnetic Resonance
journal, November 1968


Product operator formalism for the description of NMR pulse experiments
journal, January 1984

  • Sørensen, O. W.; Eich, G. W.; Levitt, M. H.
  • Progress in Nuclear Magnetic Resonance Spectroscopy, Vol. 16
  • DOI: 10.1016/0079-6565(84)80005-9

Crystal-Structure Determination of Powdered Paramagnetic Lanthanide Complexes by Proton NMR Spectroscopy
journal, April 2009

  • Kervern, Gwendal; D'Aléo, Anthony; Toupet, Loïc
  • Angewandte Chemie International Edition, Vol. 48, Issue 17
  • DOI: 10.1002/anie.200805302

Proton-detected 14N MAS NMR using homonuclear decoupled rotary resonance
journal, February 2007


Suppression of artifacts in two-dimensional J spectroscopy
journal, September 1977

  • Bodenhausen, Geoffrey; Freeman, Ray; Turner, David L.
  • Journal of Magnetic Resonance (1969), Vol. 27, Issue 3
  • DOI: 10.1016/0022-2364(77)90016-6

Superadiabaticity in magnetic resonance
journal, November 2008

  • Deschamps, Michaël; Kervern, Gwendal; Massiot, Dominique
  • The Journal of Chemical Physics, Vol. 129, Issue 20
  • DOI: 10.1063/1.3012356

Molecular Schrödinger Equation. VIII. A New Method for the Evaluation of Multidimensional Integrals
journal, December 1967

  • Conroy, Harold
  • The Journal of Chemical Physics, Vol. 47, Issue 12
  • DOI: 10.1063/1.1701795

Broadband inversion for MAS NMR with single-sideband-selective adiabatic pulses
journal, January 2011

  • Pell, Andrew J.; Kervern, Gwendal; Emsley, Lyndon
  • The Journal of Chemical Physics, Vol. 134, Issue 2
  • DOI: 10.1063/1.3521491

The Dipolar Broadening of Magnetic Resonance Lines in Crystals
journal, November 1948