Velocity measurement by coherent x-ray heterodyning
Abstract
Herein, we present a small-angle coherent x-ray scattering technique used for measuring flow velocities in slow moving materials. The technique is an extension of X-ray Photon Correlation Spectroscopy (XPCS): It involves mixing the scattering from moving tracer particles with a static reference that heterodynes the signal. This acts to elongate temporal effects caused by flow in homodyne measurements, allowing for a more robust measurement of flow properties. Using coherent x-ray heterodyning, velocities ranging from 0.1 to 10 μm/s were measured for a viscous fluid pushed through a rectangular channel. We describe experimental protocols and theory for making these Poiseuille flow profile measurements and also develop the relevant theory for using heterodyne XPCS to measure velocities in uniform and Couette flows.
- Authors:
-
[1];
- McGill Univ., Montreal, QC (Canada). Dept of Physics
- Univ. of Ottawa, ON (Canada). Dept. of Physics
- Publication Date:
- Research Org.:
- Argonne National Laboratory (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES); Natural Sciences and Engineering Research Council of Canada (NSERC)
- OSTI Identifier:
- 1342248
- Alternate Identifier(s):
- OSTI ID: 1361740
- Grant/Contract Number:
- AC02-06CH11357
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Review of Scientific Instruments
- Additional Journal Information:
- Journal Volume: 88; Journal Issue: 1; Journal ID: ISSN 0034-6748
- Publisher:
- American Institute of Physics (AIP)
- Country of Publication:
- United States
- Language:
- ENGLISH
- Subject:
- 46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY
Citation Formats
Lhermitte, Julien R. M., Rogers, Michael C., Manet, Sabine, and Sutton, Mark. Velocity measurement by coherent x-ray heterodyning. United States: N. p., 2017.
Web. doi:10.1063/1.4974099.
Lhermitte, Julien R. M., Rogers, Michael C., Manet, Sabine, & Sutton, Mark. Velocity measurement by coherent x-ray heterodyning. United States. https://doi.org/10.1063/1.4974099
Lhermitte, Julien R. M., Rogers, Michael C., Manet, Sabine, and Sutton, Mark. Mon .
"Velocity measurement by coherent x-ray heterodyning". United States. https://doi.org/10.1063/1.4974099. https://www.osti.gov/servlets/purl/1342248.
@article{osti_1342248,
title = {Velocity measurement by coherent x-ray heterodyning},
author = {Lhermitte, Julien R. M. and Rogers, Michael C. and Manet, Sabine and Sutton, Mark},
abstractNote = {Herein, we present a small-angle coherent x-ray scattering technique used for measuring flow velocities in slow moving materials. The technique is an extension of X-ray Photon Correlation Spectroscopy (XPCS): It involves mixing the scattering from moving tracer particles with a static reference that heterodynes the signal. This acts to elongate temporal effects caused by flow in homodyne measurements, allowing for a more robust measurement of flow properties. Using coherent x-ray heterodyning, velocities ranging from 0.1 to 10 μm/s were measured for a viscous fluid pushed through a rectangular channel. We describe experimental protocols and theory for making these Poiseuille flow profile measurements and also develop the relevant theory for using heterodyne XPCS to measure velocities in uniform and Couette flows.},
doi = {10.1063/1.4974099},
journal = {Review of Scientific Instruments},
number = 1,
volume = 88,
place = {United States},
year = {Mon Jan 30 00:00:00 EST 2017},
month = {Mon Jan 30 00:00:00 EST 2017}
}
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Works referenced in this record:
Microfluidic Chips for Immunoassays
journal, June 2013
- Han, Kwi Nam; Li, Cheng Ai; Seong, Gi Hun
- Annual Review of Analytical Chemistry, Vol. 6, Issue 1
Single-molecule denaturation mapping of DNA in nanofluidic channels
journal, July 2010
- Reisner, W.; Larsen, N. B.; Silahtaroglu, A.
- Proceedings of the National Academy of Sciences, Vol. 107, Issue 30
Human gut-on-a-chip inhabited by microbial flora that experiences intestinal peristalsis-like motions and flow
journal, January 2012
- Kim, Hyun Jung; Huh, Dongeun; Hamilton, Geraldine
- Lab on a Chip, Vol. 12, Issue 12
Microfluid mechanics: progress and opportunities
journal, March 2001
- Giordano, N.; Cheng, J-T
- Journal of Physics: Condensed Matter, Vol. 13, Issue 15
Direct Experimental Evidence of Slip in Hexadecane: Solid Interfaces
journal, July 2000
- Pit, R.; Hervet, H.; Léger, L.
- Physical Review Letters, Vol. 85, Issue 5
Apparent fluid slip at hydrophobic microchannel walls
journal, March 2002
- Tretheway, Derek C.; Meinhart, Carl D.
- Physics of Fluids, Vol. 14, Issue 3
Microfluidics: The No-Slip Boundary Condition
book, January 2007
- Lauga, Eric; Brenner, Michael; Stone, Howard
- Springer Handbook of Experimental Fluid Mechanics
XPCS Investigation of the Dynamics of Filler Particles in Stretched Filled Elastomers
journal, October 2012
- Ehrburger-Dolle, Françoise; Morfin, Isabelle; Bley, Françoise
- Macromolecules, Vol. 45, Issue 21
Experimental clues of soft glassy rheology in strained filled elastomers
journal, February 2014
- Ehrburger-Dolle, Françoise; Morfin, Isabelle; Bley, Françoise
- Journal of Polymer Science Part B: Polymer Physics, Vol. 52, Issue 9
Combined measurement of X-ray photon correlation spectroscopy and diffracted X-ray tracking using pink beam X-rays
journal, July 2013
- Shinohara, Yuya; Watanabe, Akira; Kishimoto, Hiroyuki
- Journal of Synchrotron Radiation, Vol. 20, Issue 5
Slow dynamics of nanocomposite polymer aerogels as revealed by X-ray photocorrelation spectroscopy (XPCS)
journal, January 2014
- Hernández, Rebeca; Nogales, Aurora; Sprung, Michael
- The Journal of Chemical Physics, Vol. 140, Issue 2
Observation of speckle by diffraction with coherent X-rays
journal, August 1991
- Sutton, M.; Mochrie, S. G. J.; Greytak, T.
- Nature, Vol. 352, Issue 6336
A review of X-ray intensity fluctuation spectroscopy
journal, June 2008
- Sutton, Mark
- Comptes Rendus Physique, Vol. 9, Issue 5-6
X-ray photon correlation spectroscopy under flow
journal, May 2008
- Fluerasu, Andrei; Moussaïd, Abdellatif; Falus, Péter
- Journal of Synchrotron Radiation, Vol. 15, Issue 4
X-ray intensity fluctuation spectroscopy by heterodyne detection
journal, October 2006
- Livet, F.; Bley, F.; Ehrburger-Dolle, F.
- Journal of Synchrotron Radiation, Vol. 13, Issue 6
Observation of Heterodyne Mixing in Surface X-Ray Photon Correlation Spectroscopy Experiments
journal, August 2003
- Gutt, C.; Ghaderi, T.; Chamard, V.
- Physical Review Letters, Vol. 91, Issue 7
Direct measurement of the propagation velocity of defects using coherent X-rays
journal, March 2016
- Ulbrandt, Jeffrey G.; Rainville, Meliha G.; Wagenbach, Christa
- Nature Physics, Vol. 12, Issue 8
Dynamics in shear flow studied by X-ray Photon Correlation Spectroscopy
journal, April 2008
- Busch, S.; Jensen, T. H.; Chushkin, Y.
- The European Physical Journal E, Vol. 26, Issue 1-2
Dynamics and rheology under continuous shear flow studied by x-ray photon correlation spectroscopy
journal, March 2010
- Fluerasu, Andrei; Kwasniewski, Pawel; Caronna, Chiara
- New Journal of Physics, Vol. 12, Issue 3
The measurement of velocity gradients in laminar flow by homodyne light-scattering spectroscopy
journal, October 1980
- Fuller, G. G.; Rallison, J. M.; Schmidt, R. L.
- Journal of Fluid Mechanics, Vol. 100, Issue 03
Echoes in x-ray speckles track nanometer-scale plastic events in colloidal gels under shear
journal, December 2014
- Rogers, Michael C.; Chen, Kui; Andrzejewski, Lukasz
- Physical Review E, Vol. 90, Issue 6
Rheo-XPCS
journal, August 2015
- Leheny, Robert L.; Rogers, Michael C.; Chen, Kui
- Current Opinion in Colloid & Interface Science, Vol. 20, Issue 4
Structure of Random Porous Materials: Silica Aerogel
journal, May 1986
- Schaefer, Dale W.; Keefer, Keith D.
- Physical Review Letters, Vol. 56, Issue 20, p. 2199-2202
Area detector based photon correlation in the regime of short data batches: Data reduction for dynamic x-ray scattering
journal, September 2000
- Lumma, D.; Lurio, L. B.; Mochrie, S. G. J.
- Review of Scientific Instruments, Vol. 71, Issue 9
X-Ray Intensity Fluctuation Spectroscopy Studies on Phase-Ordering Systems
journal, February 2005
- Fluerasu, Andrei; Sutton, Mark; Dufresne, Eric M.
- Physical Review Letters, Vol. 94, Issue 5
Aging in a filled polymer: Coherent small angle x-ray and light scattering
journal, December 2000
- Geissler, Erik; Hecht, Anne-Marie; Rochas, Cyrille
- Physical Review E, Vol. 62, Issue 6
Dynamics and rheology under continuous shear flow studied by X-ray photon correlation spectroscopy
text, January 2010
- Fluerasu, Andrei; Kwasniewski, Pawel; Caronna, Chiara
- arXiv
Statistical Properties of Scattered Radiation
book, January 1977
- Pusey, P. N.
- Photon Correlation Spectroscopy and Velocimetry
Works referencing / citing this record:
Coherent X-ray measurement of step-flow propagation during growth on polycrystalline thin film surfaces
journal, June 2019
- Headrick, Randall L.; Ulbrandt, Jeffrey G.; Myint, Peco
- Nature Communications, Vol. 10, Issue 1
A new framework for X-ray photon correlation spectroscopy analysis from polycrystalline materials
journal, December 2018
- Lewis, Ronald M.; Jackson, Grayson L.; Maher, Michael J.
- Review of Scientific Instruments, Vol. 89, Issue 12
Coherent X-ray measurement of step-flow propagation during growth on polycrystalline thin film surfaces
text, January 2018
- Headrick, Randall L.; Ulbrandt, Jeffrey G.; Myint, Peco
- arXiv