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Title: Precipitation kinetics during aging of an alumina-forming austenitic stainless steel

Abstract

The microstructural evolution of DAFA26, an alumina-forming austenitic (AFA) stainless steel, was investigated during aging. The effect of aging at 750 °C and 800 °C on the growth of spherical γ’-Ni3(Al, Ti) particles present in the as-processed state was studied extensively using X-ray diffraction, microhardness testing, scanning electron microscopy, transmission electron microscopy, and atom probe tomography. The γ’ particles had a cube-on-cube orientation relationship with the matrix (i.e. ((010)(010)m//(010)(010)p, [100][100]m//[100][100]p)). The coarsening kinetics of γ’-Ni3Al particles were in agreement with the Lifshitz, Slyozof-Wagner theory. Coarse Laves phase particles were also present in the as-processed state, and during the aging process both smaller Laves phase precipitates and B2-NiAl precipitates formed on both the grain boundaries and in the matrix. As a result, the γ’ precipitates were determined to have the most impact on the room temperature hardness.

Authors:
 [1];  [1];  [1];  [1];  [2];  [1];  [2]
  1. Dartmouth College, Hanover, NH (United States)
  2. Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Publication Date:
Research Org.:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Sponsoring Org.:
USDOE Office of Science (SC)
OSTI Identifier:
1252150
Alternate Identifier(s):
OSTI ID: 1360851
Grant/Contract Number:  
AC05-00OR22725; DEFG2612FE0008857
Resource Type:
Accepted Manuscript
Journal Name:
Materials Science and Engineering. A, Structural Materials: Properties, Microstructure and Processing
Additional Journal Information:
Journal Volume: 667; Journal ID: ISSN 0921-5093
Publisher:
Elsevier
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; austenite; intermetallics; aging; coarsening; grain boundaries; precipitation

Citation Formats

Trotter, Geneva, Hu, Bin, Sun, Annie Y., Harder, Reed, Miller, Michael K., Baker, Ian, and Yao, Lan. Precipitation kinetics during aging of an alumina-forming austenitic stainless steel. United States: N. p., 2016. Web. doi:10.1016/j.msea.2016.04.081.
Trotter, Geneva, Hu, Bin, Sun, Annie Y., Harder, Reed, Miller, Michael K., Baker, Ian, & Yao, Lan. Precipitation kinetics during aging of an alumina-forming austenitic stainless steel. United States. https://doi.org/10.1016/j.msea.2016.04.081
Trotter, Geneva, Hu, Bin, Sun, Annie Y., Harder, Reed, Miller, Michael K., Baker, Ian, and Yao, Lan. Thu . "Precipitation kinetics during aging of an alumina-forming austenitic stainless steel". United States. https://doi.org/10.1016/j.msea.2016.04.081. https://www.osti.gov/servlets/purl/1252150.
@article{osti_1252150,
title = {Precipitation kinetics during aging of an alumina-forming austenitic stainless steel},
author = {Trotter, Geneva and Hu, Bin and Sun, Annie Y. and Harder, Reed and Miller, Michael K. and Baker, Ian and Yao, Lan},
abstractNote = {The microstructural evolution of DAFA26, an alumina-forming austenitic (AFA) stainless steel, was investigated during aging. The effect of aging at 750 °C and 800 °C on the growth of spherical γ’-Ni3(Al, Ti) particles present in the as-processed state was studied extensively using X-ray diffraction, microhardness testing, scanning electron microscopy, transmission electron microscopy, and atom probe tomography. The γ’ particles had a cube-on-cube orientation relationship with the matrix (i.e. ((010)(010)m//(010)(010)p, [100][100]m//[100][100]p)). The coarsening kinetics of γ’-Ni3Al particles were in agreement with the Lifshitz, Slyozof-Wagner theory. Coarse Laves phase particles were also present in the as-processed state, and during the aging process both smaller Laves phase precipitates and B2-NiAl precipitates formed on both the grain boundaries and in the matrix. As a result, the γ’ precipitates were determined to have the most impact on the room temperature hardness.},
doi = {10.1016/j.msea.2016.04.081},
journal = {Materials Science and Engineering. A, Structural Materials: Properties, Microstructure and Processing},
number = ,
volume = 667,
place = {United States},
year = {Thu Apr 28 00:00:00 EDT 2016},
month = {Thu Apr 28 00:00:00 EDT 2016}
}

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Cited by: 26 works
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Works referenced in this record:

Materials for ultra-supercritical coal-fired power plant boilers
journal, November 2006

  • Viswanathan, R.; Coleman, K.; Rao, U.
  • International Journal of Pressure Vessels and Piping, Vol. 83, Issue 11-12
  • DOI: 10.1016/j.ijpvp.2006.08.006

U.S. Program on Materials Technology for Ultra-Supercritical Coal Power Plants
journal, June 2005

  • Viswanathan, R.; Henry, J. F.; Tanzosh, J.
  • Journal of Materials Engineering and Performance, Vol. 14, Issue 3
  • DOI: 10.1361/10599490524039

The development of alumina-forming austenitic stainless steels for high-temperature structural use
journal, July 2008


Creep-Resistant, Al2O3-Forming Austenitic Stainless Steels
journal, April 2007


Alumina-Forming Austenitic Stainless Steels Strengthened by Laves Phase and MC Carbide Precipitates
journal, September 2007

  • Yamamoto, Y.; Brady, M. P.; Lu, Z. P.
  • Metallurgical and Materials Transactions A, Vol. 38, Issue 11
  • DOI: 10.1007/s11661-007-9319-y

On the Loss of Protective Scale Formation in Creep-Resistant, Alumina-Forming Austenitic Stainless Steels at 900°C in Air
journal, September 2008


Effect of Alloying Additions on Phase Equilibria and Creep Resistance of Alumina-Forming Austenitic Stainless Steels
journal, June 2009

  • Yamamoto, Y.; Santella, M. L.; Brady, M. P.
  • Metallurgical and Materials Transactions A, Vol. 40, Issue 8
  • DOI: 10.1007/s11661-009-9886-1

Aging effects on the mechanical properties of alumina-forming austenitic stainless steels
journal, March 2010


Composition, Microstructure, and Water Vapor Effects on Internal/External Oxidation of Alumina-Forming Austenitic Stainless Steels
journal, July 2009


Overview of Strategies for High-Temperature Creep and Oxidation Resistance of Alumina-Forming Austenitic Stainless Steels
journal, July 2010

  • Yamamoto, Y.; Brady, M. P.; Santella, M. L.
  • Metallurgical and Materials Transactions A, Vol. 42, Issue 4
  • DOI: 10.1007/s11661-010-0295-2

Development of L12-ordered Ni3(Al,Ti)-strengthened alumina-forming austenitic stainless steel alloys
journal, December 2013


Accelerated precipitation in the AFA stainless steel Fe–20Cr–30Ni–2Nb–5Al via cold working
journal, October 2014


The Effects of Cold Work on the Microstructure and Mechanical Properties of Intermetallic Strengthened Alumina-Forming Austenitic Stainless Steels
journal, June 2015

  • Hu, B.; Trotter, G.; Baker, Ian
  • Metallurgical and Materials Transactions A, Vol. 46, Issue 8
  • DOI: 10.1007/s11661-015-2981-6

Strategies for fabricating atom probe specimens with a dual beam FIB
journal, March 2005


Unit-cell refinement from powder diffraction scans
journal, December 1981


Formation of annealing twins in f.c.c. crystals
journal, June 1997


Microstructural stability and mechanical properties of a newly developed Ni–Fe-base superalloy
journal, January 2015


Ordering and precipitation of γ′ phase in low supersaturated Ni-Cr-Al model alloy: An atomic scale investigation
journal, September 1997


γ′ coarsening in high volume fraction nickel-base alloys
journal, June 1990


Coarsening behaviour of a Ni-base superalloy under different heat treatment conditions
journal, June 2007

  • Ges, A. M.; Fornaro, O.; Palacio, H. A.
  • Materials Science and Engineering: A, Vol. 458, Issue 1-2
  • DOI: 10.1016/j.msea.2006.12.107

Gamma prime coarsening and age-hardening behaviors in a new nickel base superalloy
journal, April 2004


The kinetics of precipitation from supersaturated solid solutions
journal, April 1961


Works referencing / citing this record:

Effect of the Deformation Amount on the Microstructure and Tensile Properties of 304 Stainless Steel with 2 wt% Al Content by Cold Rolling
journal, January 2020


Precipitates and Particles Coarsening of 9Cr–1.7W–0.4Mo–Co Ferritic Heat-Resistant Steel after Isothermal Aging
journal, July 2017