In-situ high-pressure x-ray diffraction study of zinc ferrite nanoparticles

Ferrari, S.; Kumar, R. S.; Grinblat, F.; Aphesteguy, J. C.; Saccone, F. D.; Errandonea, D.

doi:10.1016/j.solidstatesciences.2016.04.006

Title: In-situ high-pressure x-ray diffraction study of zinc ferrite nanoparticles

Abstract

We have studied the high-pressure structural behavior of zinc ferrite (ZnFe₂O₄) nanoparticles by powder X-ray diffraction measurements up to 47 GPa. We found that the cubic spinel structure of ZnFe₂O₄ remains up to 33 GPa and a phase transition is induced beyond this pressure. The high-pressure phase is indexed to an orthorhombic CaMn₂O₄-type structure. Upon decompression the low- and high-pressure phases coexist. The compressibility of both structures was also investigated. We have observed that the lattice parameters of the high-pressure phase behave anisotropically upon compression. Further, we predict possible phase transition around 55 GPa. For comparison, we also studied the compression behavior of magnetite (Fe₃O₄) nanoparticles by X-ray diffraction up to 23 GPa. Spinel-type ZnFe₂O₄ and Fe₃O₄ nanoparticles have a bulk modulus of 172 (20) GPa and 152 (9) GPa, respectively. Lastly, this indicates that in both cases the nanoparticles do not undergo a Hall-Petch strengthening.

Authors:

Ferrari, S. ^[1]; Kumar, R. S. ^[2];

^[1]; Aphesteguy, J. C. ^[1]; Saccone, F. D. ^[3]; Errandonea, D. ^[4]

Instituto de Tecnologia y Ciencias de la Ingenieria "Ing. Hilario Fernandez Long" (UBA-CONICET), Buenos Aires (Argentina)
Univ. of Nevada, Las Vegas, NV (United States)
Facultad de Ingenieria (UBA), Buenos Aires (Argentina)
Univ. de Valencia, Valencia (Spain)

Publication Date:: Sat Apr 23 00:00:00 EDT 2016

Research Org.:: Univ. of Nevada, Las Vegas, NV (United States)

Sponsoring Org.:: USDOE National Nuclear Security Administration (NNSA); USDOE Office of Science (SC), Basic Energy Sciences (BES)

OSTI Identifier:: 1332349

Alternate Identifier(s):: OSTI ID: 1357835

Grant/Contract Number:: NA0001982; NA0001974; FG02-99ER45775; AC02-06CH11357

Resource Type:: Accepted Manuscript

Journal Name:: Solid State Sciences

Additional Journal Information:: Journal Volume: 56; Journal Issue: C; Journal ID: ISSN 1293-2558

Publisher:: Elsevier

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE; 75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY; crystal structure; nanostructure; oxides; phase transitions; X-ray diffraction

Citation Formats


                    Ferrari, S., Kumar, R. S., Grinblat, F., Aphesteguy, J. C., Saccone, F. D., and Errandonea, D. In-situ high-pressure x-ray diffraction study of zinc ferrite nanoparticles.  United States: N. p., 2016. 
Web.  doi:10.1016/j.solidstatesciences.2016.04.006.

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                    Ferrari, S., Kumar, R. S., Grinblat, F., Aphesteguy, J. C., Saccone, F. D., & Errandonea, D. In-situ high-pressure x-ray diffraction study of zinc ferrite nanoparticles.  United States.  https://doi.org/10.1016/j.solidstatesciences.2016.04.006

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                    Ferrari, S., Kumar, R. S., Grinblat, F., Aphesteguy, J. C., Saccone, F. D., and Errandonea, D. Sat .  
"In-situ high-pressure x-ray diffraction study of zinc ferrite nanoparticles".  United States.  https://doi.org/10.1016/j.solidstatesciences.2016.04.006.  https://www.osti.gov/servlets/purl/1332349.

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@article{osti_1332349,

  title        = {In-situ high-pressure x-ray diffraction study of zinc ferrite nanoparticles},

  author       = {Ferrari, S. and Kumar, R. S. and Grinblat, F. and Aphesteguy, J. C. and Saccone, F. D. and Errandonea, D.},

  abstractNote = {We have studied the high-pressure structural behavior of zinc ferrite (ZnFe2O4) nanoparticles by powder X-ray diffraction measurements up to 47 GPa. We found that the cubic spinel structure of ZnFe2O4 remains up to 33 GPa and a phase transition is induced beyond this pressure. The high-pressure phase is indexed to an orthorhombic CaMn2O4-type structure. Upon decompression the low- and high-pressure phases coexist. The compressibility of both structures was also investigated. We have observed that the lattice parameters of the high-pressure phase behave anisotropically upon compression. Further, we predict possible phase transition around 55 GPa. For comparison, we also studied the compression behavior of magnetite (Fe3O4) nanoparticles by X-ray diffraction up to 23 GPa. Spinel-type ZnFe2O4 and Fe3O4 nanoparticles have a bulk modulus of 172 (20) GPa and 152 (9) GPa, respectively. Lastly, this indicates that in both cases the nanoparticles do not undergo a Hall-Petch strengthening.},

  doi          = {10.1016/j.solidstatesciences.2016.04.006},

  journal      = {Solid State Sciences},

  number       = C,

  volume       = 56,

  place        = {United States},

  year         = {Sat Apr 23 00:00:00 EDT 2016},

  month        = {Sat Apr 23 00:00:00 EDT 2016}

}

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Works referencing / citing this record:

Pressure-induced structural and spin transitions of Fe3S4
journal, April 2017

Huang, Shengxuan; Kang, Duan; Wu, Xiang
Scientific Reports, Vol. 7, Issue 1
DOI: 10.1038/srep46334

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Title: In-situ high-pressure x-ray diffraction study of zinc ferrite nanoparticles

Abstract

Citation Formats

Lattice Parameters and Stability of the Spinel Compounds in Relation to the Ionic Radii and Electronegativities of Constituting Chemical Elements journal, May 2014

Superparamagnetism in ZnFe 2 O 4 Induced by High Pressure Squeezing journal, June 1964

Phase transition of synthetic zinc ferrite spinel (ZnFe 2 O 4 ) at high pressure, from synchrotron X-ray powder diffraction journal, November 2000

On the compressibility of ferrite spinels: a high-pressure X-ray diffraction study of M Fe 2 O 4 ( M =Mg, Co, Zn) journal, December 2009

Elasticity of franklinite and trends for transition-metal oxide spinels journal, March 2013

Elastic Constants for Zinc Ferrite from the Infrared Spectrum journal, August 1973

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VESTA 3 for three-dimensional visualization of crystal, volumetric and morphology data journal, October 2011

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Compressibility and Structural Stability of Nanocrystalline TiO 2 Anatase Synthesized from Freeze-Dried Precursors journal, October 2014

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Structural and Magnetic Properties of Zn-Doped Magnetite Nanoparticles Obtained by Wet Chemical Method journal, June 2015

Two-dimensional detector software: From real detector to idealised image or two-theta scan journal, January 1996

Rietveld texture analysis from diffraction images journal, November 2007

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Equation of state and thermodynamic parameters of NaCl to 300 kbar in the high-temperature domain journal, January 1986

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Comment on “High-pressure x-ray diffraction study of YBO 3 /Eu 3+ , GdBO 3 , and EuBO 3 : Pressure-induced amorphization in GdBO 3 ” [J. Appl. Phys. 115 , 043507 (2014)] journal, June 2014

Complex high-pressure polymorphism of barium tungstate journal, August 2012

High-pressure structural behaviour of HoVO 4 : combined XRD experiments and ab initio calculations journal, June 2014

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New model for the magnetic structure of the marokite-type oxide CaMn2O4 journal, April 2003

Kompressibilitätsmessungen an festen Körpern journal, January 1921

Equation of state of magnetite and its high-pressure modification: Thermodynamics of the Fe-O system at high pressure journal, March 2000

In situ structure determination of the high-pressure phase of Fe 3 O 4 journal, February 1999

Isothermal compression of magnetite to 320 KB journal, March 1974

Compressibility of Nanocrystalline TiO 2 Anatase journal, September 2012

High-pressure study of the behavior of mineral barite by x-ray diffraction journal, August 2011

Pressure-induced transition in titanium metal a systematic study of the effects of uniaxial stress journal, January 2005

Pressure-induced structural and spin transitions of Fe3S4 journal, April 2017

Lattice Parameters and Stability of the Spinel Compounds in Relation to the Ionic Radii and Electronegativities of Constituting Chemical Elements
journal, May 2014

Superparamagnetism in ZnFe ₂ O ₄ Induced by High Pressure Squeezing
journal, June 1964

Phase transition of synthetic zinc ferrite spinel (ZnFe 2 O 4 ) at high pressure, from synchrotron X-ray powder diffraction
journal, November 2000

On the compressibility of ferrite spinels: a high-pressure X-ray diffraction study of M Fe ₂ O ₄ ( M =Mg, Co, Zn)
journal, December 2009

Elasticity of franklinite and trends for transition-metal oxide spinels
journal, March 2013

Elastic Constants for Zinc Ferrite from the Infrared Spectrum
journal, August 1973

Single crystal elastic constants of zinc ferrite (ZnFe2O4)
journal, July 1990

VESTA 3 for three-dimensional visualization of crystal, volumetric and morphology data
journal, October 2011

Cobalt ferrite nanoparticles under high pressure
journal, August 2015

Nanomaterials under high-pressure
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Compressibility and Structural Stability of Nanocrystalline TiO ₂ Anatase Synthesized from Freeze-Dried Precursors
journal, October 2014

What is behind the inverse Hall–Petch effect in nanocrystalline materials?
journal, June 2007

Structural and Magnetic Properties of Zn-Doped Magnetite Nanoparticles Obtained by Wet Chemical Method
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Two-dimensional detector software: From real detector to idealised image or two-theta scan
journal, January 1996

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Equation of state of $α$ -Al $_{2}$ O $_{3}$
journal, August 2013

High pressure–high temperature equations of state of neon and diamond
journal, March 2008

High-pressure x-ray diffraction and ab initio study of ${Ni}_{2} {Mo}_{3} N$ , ${Pd}_{2} {Mo}_{3} N$ , ${Pt}_{2} {Mo}_{3} N$ , ${Co}_{3} {Mo}_{3} N$ , and ${Fe}_{3} {Mo}_{3} N$ : Two families of ultra-incompressible bimetallic interstitial nitrides
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Post-spinel transformations and equation of state in ${ZnGa}_{2} O_{4}$ : Determination at high pressure by in situ x-ray diffraction
journal, January 2009

Equation of state and thermodynamic parameters of NaCl to 300 kbar in the high-temperature domain
journal, January 1986

Hydrostatic limits of 11 pressure transmitting media
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Comment on “High-pressure x-ray diffraction study of YBO ₃ /Eu ³⁺ , GdBO ₃ , and EuBO ₃ : Pressure-induced amorphization in GdBO ₃ ” [J. Appl. Phys. 115 , 043507 (2014)]
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Complex high-pressure polymorphism of barium tungstate
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High-pressure structural behaviour of HoVO ₄ : combined XRD experiments and ab initio calculations
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New model for the magnetic structure of the marokite-type oxide CaMn2O4
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Kompressibilitätsmessungen an festen Körpern
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Equation of state of magnetite and its high-pressure modification: Thermodynamics of the Fe-O system at high pressure
journal, March 2000

In situ structure determination of the high-pressure phase of Fe ₃ O ₄
journal, February 1999

Isothermal compression of magnetite to 320 KB
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Compressibility of Nanocrystalline TiO ₂ Anatase
journal, September 2012

High-pressure study of the behavior of mineral barite by x-ray diffraction
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Pressure-induced transition in titanium metal a systematic study of the effects of uniaxial stress
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