Highly Crystalline Multimetallic Nanoframes with Three-Dimensional Electrocatalytic Surfaces
Abstract
Control of structure at the atomic level can precisely and effectively tune catalytic properties of materials, enabling enhancement in both activity and durability. We synthesized a highly active and durable class of electrocatalysts by exploiting the structural evolution of platinum-nickel (Pt-Ni) bimetallic nanocrystals. The starting material, crystalline PtNi3 polyhedra, transforms in solution by interior erosion into Pt3Ni nanoframes with surfaces that offer three-dimensional molecular accessibility. The edges of the Pt-rich PtNi3 polyhedra are maintained in the final Pt3Ni nanoframes. Both the interior and exterior catalytic surfaces of this open-framework structure are composed of the nanosegregated Pt-skin structure, which exhibits enhanced oxygen reduction reaction (ORR) activity. The Pt3Ni nanoframe catalysts achieved a factor of 36 enhancement in mass activity and a factor of 22 enhancement in specific activity, respectively, for this reaction (relative to state-of-the-art platinum-carbon catalysts) during prolonged exposure to reaction conditions.
- Authors:
-
- Univ. of California, Berkeley, CA (United States). Dept. of Chemistry; Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States). Materials Science Division; Tsinghua Univ., Beijing (China). Dept. of Chemistry
- Argonne National Lab. (ANL), Argonne, IL (United States). Materials Science Division
- Univ. of California, Berkeley, CA (United States). Dept. of Chemistry; Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States). Materials Science Division
- Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States). Materials Science Division
- Univ. of Wisconsin, Madison, WI (United States). Dept. of Chemical and Biological Engineering
- Division of Materials Science and Technology, Oak Ridge National Laboratory, Oak Ridge, TN 37831, USA.
- Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Materials Science & Technology Division
- Tsinghua Univ., Beijing (China). Dept. of Chemistry
- Univ. of California, Berkeley, CA (United States). Dept. of Chemistry; Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States). Materials Science Division; King Abdulaziz Univ., Jeddah (Saudi Arabia). Dept. of Chemistry; Univ. of California, Berkeley and Lawrence Berkeley National Lab. (LBNL), CA (United States). Kavli Energy NanoSciences Inst.
- Publication Date:
- Research Org.:
- Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States); Argonne National Laboratory (ANL), Argonne, IL (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES). Materials Sciences & Engineering Division; USDOE Office of Energy Efficiency and Renewable Energy (EERE), Transportation Office. Fuel Cell Technologies Office; USDOE Office of Science (SC), Basic Energy Sciences (BES)
- OSTI Identifier:
- 1833358
- Alternate Identifier(s):
- OSTI ID: 1357584
- Grant/Contract Number:
- AC02-06CH11357; AC02-05CH11231; FG02-05ER15731
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Science
- Additional Journal Information:
- Journal Volume: 343; Journal Issue: 6177; Journal ID: ISSN 0036-8075
- Publisher:
- AAAS
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE
Citation Formats
Chen, Chen, Kang, Yijin, Huo, Ziyang, Zhu, Zhongwei, Huang, Wenyu, Xin, Huolin L., Snyder, Joshua D., Li, Dongguo, Herron, Jeffrey A., Mavrikakis, Manos, Chi, Miaofang, More, Karren L., Li, Yadong, Markovic, Nenad M., Somorjai, Gabor A., Yang, Peidong, and Stamenkovic, Vojislav R. Highly Crystalline Multimetallic Nanoframes with Three-Dimensional Electrocatalytic Surfaces. United States: N. p., 2014.
Web. doi:10.1126/science.1249061.
Chen, Chen, Kang, Yijin, Huo, Ziyang, Zhu, Zhongwei, Huang, Wenyu, Xin, Huolin L., Snyder, Joshua D., Li, Dongguo, Herron, Jeffrey A., Mavrikakis, Manos, Chi, Miaofang, More, Karren L., Li, Yadong, Markovic, Nenad M., Somorjai, Gabor A., Yang, Peidong, & Stamenkovic, Vojislav R. Highly Crystalline Multimetallic Nanoframes with Three-Dimensional Electrocatalytic Surfaces. United States. https://doi.org/10.1126/science.1249061
Chen, Chen, Kang, Yijin, Huo, Ziyang, Zhu, Zhongwei, Huang, Wenyu, Xin, Huolin L., Snyder, Joshua D., Li, Dongguo, Herron, Jeffrey A., Mavrikakis, Manos, Chi, Miaofang, More, Karren L., Li, Yadong, Markovic, Nenad M., Somorjai, Gabor A., Yang, Peidong, and Stamenkovic, Vojislav R. Thu .
"Highly Crystalline Multimetallic Nanoframes with Three-Dimensional Electrocatalytic Surfaces". United States. https://doi.org/10.1126/science.1249061. https://www.osti.gov/servlets/purl/1833358.
@article{osti_1833358,
title = {Highly Crystalline Multimetallic Nanoframes with Three-Dimensional Electrocatalytic Surfaces},
author = {Chen, Chen and Kang, Yijin and Huo, Ziyang and Zhu, Zhongwei and Huang, Wenyu and Xin, Huolin L. and Snyder, Joshua D. and Li, Dongguo and Herron, Jeffrey A. and Mavrikakis, Manos and Chi, Miaofang and More, Karren L. and Li, Yadong and Markovic, Nenad M. and Somorjai, Gabor A. and Yang, Peidong and Stamenkovic, Vojislav R.},
abstractNote = {Control of structure at the atomic level can precisely and effectively tune catalytic properties of materials, enabling enhancement in both activity and durability. We synthesized a highly active and durable class of electrocatalysts by exploiting the structural evolution of platinum-nickel (Pt-Ni) bimetallic nanocrystals. The starting material, crystalline PtNi3 polyhedra, transforms in solution by interior erosion into Pt3Ni nanoframes with surfaces that offer three-dimensional molecular accessibility. The edges of the Pt-rich PtNi3 polyhedra are maintained in the final Pt3Ni nanoframes. Both the interior and exterior catalytic surfaces of this open-framework structure are composed of the nanosegregated Pt-skin structure, which exhibits enhanced oxygen reduction reaction (ORR) activity. The Pt3Ni nanoframe catalysts achieved a factor of 36 enhancement in mass activity and a factor of 22 enhancement in specific activity, respectively, for this reaction (relative to state-of-the-art platinum-carbon catalysts) during prolonged exposure to reaction conditions.},
doi = {10.1126/science.1249061},
journal = {Science},
number = 6177,
volume = 343,
place = {United States},
year = {Thu Feb 27 00:00:00 EST 2014},
month = {Thu Feb 27 00:00:00 EST 2014}
}
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Boosting the oxygen evolution reaction performance of CoS 2 microspheres by subtle ionic liquid modification
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- Ji, Siyuan; Li, Tongtong; Gao, Zhi-Da
- Chemical Communications, Vol. 54, Issue 63
Alloy-composition-dependent oxygen reduction reaction activity and electrochemical stability of Pt-based bimetallic systems: a model electrocatalyst study of Pt/Pt x Ni 100−x (111)
journal, January 2018
- Todoroki, Naoto; Kawamura, Ryutaro; Asano, Masato
- Physical Chemistry Chemical Physics, Vol. 20, Issue 17
Hollow nanoparticles as emerging electrocatalysts for renewable energy conversion reactions
journal, January 2018
- Park, Jongsik; Kwon, Taehyun; Kim, Jun
- Chemical Society Reviews, Vol. 47, Issue 22
Synthesis of germanium–platinum nanoparticles as high-performance catalysts for spray-deposited large-area dye-sensitized solar cells (DSSC) and the hydrogen evolution reaction (HER)
journal, January 2018
- Lim, Suh-Ciuan; Hsiao, Ming-Cheng; Lu, Ming-De
- Nanoscale, Vol. 10, Issue 35
RuO x -decorated multimetallic hetero-nanocages as highly efficient electrocatalysts toward the methanol oxidation reaction
journal, January 2018
- Park, Jongsik; Kim, Hee Jin; Oh, Aram
- Nanoscale, Vol. 10, Issue 45
Direct fabrication of bi-metallic PdRu nanorod assemblies for electrochemical ammonia synthesis
journal, January 2019
- Wang, Hongjing; Li, Yinghao; Yang, Dandan
- Nanoscale, Vol. 11, Issue 12
Carved nanoframes of cobalt–iron bimetal phosphide as a bifunctional electrocatalyst for efficient overall water splitting
journal, January 2019
- Lian, Yuebin; Sun, Hao; Wang, Xuebin
- Chemical Science, Vol. 10, Issue 2
Morphology evolution of fcc Ru nanoparticles under hydrogen atmosphere
journal, January 2019
- Liu, Lili; Yu, Mengting; Hou, Bo
- Nanoscale, Vol. 11, Issue 16
Ultrasmall MoP encapsulated in nitrogen-doped carbon hybrid frameworks for highly efficient hydrogen evolution reaction in both acid and alkaline solutions
journal, January 2019
- Huang, Xiaokang; Wang, Xiang; Jiang, Pengbo
- Inorganic Chemistry Frontiers, Vol. 6, Issue 6
Rational design and synthesis of noble-metal nanoframes for catalytic and photonic applications
journal, September 2016
- Wang, Xue; Ruditskiy, Aleksey; Xia, Younan
- National Science Review, Vol. 3, Issue 4
Atomic-level structure engineering of metal oxides for high-rate oxygen intercalation pseudocapacitance
journal, October 2018
- Ling, Tao; Da, Pengfei; Zheng, Xueli
- Science Advances, Vol. 4, Issue 10
Analysis of H 2 /Air Polarization Curves: The Influence of Low Pt Loading and Fabrication Process
journal, January 2018
- Yu, Haoran; Bonville, Leonard; Maric, Radenka
- Journal of The Electrochemical Society, Vol. 165, Issue 5
Editors' Choice—Connecting Fuel Cell Catalyst Nanostructure and Accessibility Using Quantitative Cryo-STEM Tomography
journal, January 2018
- Padgett, Elliot; Andrejevic, Nina; Liu, Zhongyi
- Journal of The Electrochemical Society, Vol. 165, Issue 3
Noble Metal Based Alloy Nanoframes: Syntheses and Applications in Fuel Cells
journal, July 2019
- Nosheen, Farhat; Anwar, Tauseef; Siddique, Ayesha
- Frontiers in Chemistry, Vol. 7
Metal Catalysts for Heterogeneous Catalysis: From Single Atoms to Nanoclusters and Nanoparticles
journal, April 2018
- Liu, Lichen; Corma, Avelino
- Chemical Reviews, Vol. 118, Issue 10
Thermal Properties and Segregation Behavior of Pt Nanowires Modified with Au, Ag, and Pd Atoms: A Classical Molecular Dynamics Study
journal, July 2019
- Gambu, Thobani G.; Terranova, Umberto; Santos-Carballal, David
- The Journal of Physical Chemistry C, Vol. 123, Issue 33
Atomically Resolved Anisotropic Electrochemical Shaping of Nano-electrocatalyst
journal, April 2019
- Ruiz-Zepeda, Francisco; Gatalo, Matija; Pavlišič, Andraž
- Nano Letters, Vol. 19, Issue 8
Tuning the Electrocatalytic Performance of Ionic Liquid Modified Pt Catalysts for the Oxygen Reduction Reaction via Cationic Chain Engineering
journal, July 2018
- Zhang, Gui-Rong; Wolker, Thomas; Sandbeck, Daniel J. S.
- ACS Catalysis, Vol. 8, Issue 9
On-Chip in Situ Monitoring of Competitive Interfacial Anionic Chemisorption as a Descriptor for Oxygen Reduction Kinetics
journal, April 2018
- Ding, Mengning; Zhong, Guangyan; Zhao, Zipeng
- ACS Central Science, Vol. 4, Issue 5
Dealloying of Nitrogen-Introduced Pt–Co Alloy Nanoparticles: Preferential Core–Shell Formation with Enhanced Activity for Oxygen Reduction Reaction
journal, December 2016
- Takahashi, Shuntaro; Takahashi, Naoki; Todoroki, Naoto
- ACS Omega, Vol. 1, Issue 6
Exceptional Oxygen Reduction Reaction Activity and Durability of Platinum–Nickel Nanowires through Synthesis and Post-Treatment Optimization
journal, April 2017
- Alia, Shaun M.; Ngo, Chilan; Shulda, Sarah
- ACS Omega, Vol. 2, Issue 4
Interfacial Structure of PtNi Surface Alloy on Pt(111) Electrode for Oxygen Reduction Reaction
journal, May 2017
- Kumeda, Tomoaki; Otsuka, Naoto; Tajiri, Hiroo
- ACS Omega, Vol. 2, Issue 5
Programming ORR Activity of Ni/NiOx@Pd Electrocatalysts via Controlling Depth of Surface-Decorated Atomic Pt Clusters
journal, August 2018
- Bhalothia, Dinesh; Chou, Jyh-Pin; Yan, Che
- ACS Omega, Vol. 3, Issue 8
Facile Synthesis of PtCu Alloy/Graphene Oxide Hybrids as Improved Electrocatalysts for Alkaline Fuel Cells
journal, August 2018
- Liu, Taiyang; Li, Chaozhong; Yuan, Qiang
- ACS Omega, Vol. 3, Issue 8
In Situ Construction of Small Pt NPs Embedded in 3D Spherical Porous Carbon as an Electrocatalyst for Liquid Fuel Oxidation with High Performance
journal, December 2018
- Ding, Tao; Zhang, Li; Li, Huanran
- ACS Omega, Vol. 3, Issue 12
Inflating hollow nanocrystals through a repeated Kirkendall cavitation process
journal, November 2017
- Tianou, He; Wang, Weicong; Yang, Xiaolong
- Nature Communications, Vol. 8, Issue 1
Activating cobalt(II) oxide nanorods for efficient electrocatalysis by strain engineering
journal, November 2017
- Ling, Tao; Yan, Dong-Yang; Wang, Hui
- Nature Communications, Vol. 8, Issue 1
In situ inward epitaxial growth of bulk macroporous single crystals
journal, December 2017
- Chen, Chenlong; Sun, Shujing; Chou, Mitch M. C.
- Nature Communications, Vol. 8, Issue 1
Nanoscale kinetics of asymmetrical corrosion in core-shell nanoparticles
journal, March 2018
- Shan, Hao; Gao, Wenpei; Xiong, Yalin
- Nature Communications, Vol. 9, Issue 1
Platinum-trimer decorated cobalt-palladium core-shell nanocatalyst with promising performance for oxygen reduction reaction
journal, January 2019
- Dai, Sheng; Chou, Jyh-Pin; Wang, Kuan-Wen
- Nature Communications, Vol. 10, Issue 1
Octahedral gold-silver nanoframes with rich crystalline defects for efficient methanol oxidation manifesting a CO-promoting effect
journal, August 2019
- Xiong, Likun; Sun, Zhongti; Zhang, Xiang
- Nature Communications, Vol. 10, Issue 1
A self-supporting bimetallic Au@Pt core-shell nanoparticle electrocatalyst for the synergistic enhancement of methanol oxidation
journal, July 2017
- Tan, Changhui; Sun, Yinghui; Zheng, Jianzhong
- Scientific Reports, Vol. 7, Issue 1
Recent developments of nano-structured materials as the catalysts for oxygen reduction reaction
journal, April 2018
- Kang, SungYeon; Kim, HuiJung; Chung, Yong-Ho
- Nano Convergence, Vol. 5, Issue 1
Engineering Ru@Pt Core-Shell Catalysts for Enhanced Electrochemical Oxygen Reduction Mass Activity and Stability
journal, January 2018
- Jackson, Ariel; Strickler, Alaina; Higgins, Drew
- Nanomaterials, Vol. 8, Issue 1
Solution-Grown Dendritic Pt-Based Ternary Nanostructures for Enhanced Oxygen Reduction Reaction Functionality
journal, June 2018
- Leteba, Gerard; Mitchell, David; Levecque, Pieter
- Nanomaterials, Vol. 8, Issue 7
Micelle-Assisted Strategy for the Direct Synthesis of Large-Sized Mesoporous Platinum Catalysts by Vapor Infiltration of a Reducing Agent
journal, October 2018
- Li, Yunqi; Liu, Yuwei; Yamauchi, Yusuke
- Nanomaterials, Vol. 8, Issue 10
Nanostructure Optimization of Platinum-Based Nanomaterials for Catalytic Applications
journal, November 2018
- Duan, Sibin; Du, Zhe; Fan, Hongsheng
- Nanomaterials, Vol. 8, Issue 11
Direct Spectroscopy for Probing the Critical Role of Partial Covalency in Oxygen Reduction Reaction for Cobalt-Manganese Spinel Oxides
journal, April 2019
- Long, Xinghui; Yu, Pengfei; Zhang, Nian
- Nanomaterials, Vol. 9, Issue 4