NMR study of nematic spin fluctuations in a detwinned single crystal of underdoped Ba(Fe1₋xCox)2As2

Kissikov, T.; Dioguardi, A. P.; Timmons, E. I.; Tanatar, M. A.; Prozorov, R.; Bud'ko, S. L.; Canfield, P. C.; Fernandes, R. M.; Curro, N. J.

doi:10.1103/PhysRevB.94.165123

Title: NMR study of nematic spin fluctuations in a detwinned single crystal of underdoped $Ba {({Fe}_{1 ₋ x} {Co}_{x})}_{2} {As}_{2}$

Abstract

We report the experimental details of how mechanical detwinning can be implemented in tandem with high sensitivity nuclear magnetic resonance measurements and use this setup to measure the inplane anisotropy of the spin-lattice relaxation rate in underdoped Ba(Fe_1-xCo_x)₂As₂ with x = 0:048. The anisotropy reaches a maximum of 30% at TN, and the recovery data reveal that the glassy behavior of the spin fluctuations present in the twinned state persist in the fully detwinned crystal. A theoretical model is presented to describe the spin-lattice relaxation rate in terms of anisotropic nematic spin fluctuations.

Authors:

Kissikov, T. ^[1]; Dioguardi, A. P. ^[2]; Timmons, E. I. ^[3]; Tanatar, M. A. ^[3]; Prozorov, R. ^[3]; Bud'ko, S. L. ^[3]; Canfield, P. C. ^[3]; Fernandes, R. M. ^[4]; Curro, N. J. ^[1]

Univ. of California, Davis, CA (United States)
Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
Ames Lab. and Iowa State Univ., Ames, IA (United States)
Univ. of Minnesota, Minneapolis, MN (United States)

Publication Date:: Tue Oct 11 00:00:00 EDT 2016

Research Org.:: Ames Lab., Ames, IA (United States); Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1335028

Alternate Identifier(s):: OSTI ID: 1328634; OSTI ID: 1357140

Report Number(s):: IS-J-9132; LA-UR-17-22942
Journal ID: ISSN 2469-9950; PRBMDO

Grant/Contract Number:: DMR-1506961; PHY-1066293; SC0012336; AC02-07CH11358; AC52-06NA25396

Resource Type:: Accepted Manuscript

Journal Name:: Physical Review B

Additional Journal Information:: Journal Volume: 94; Journal Issue: 16; Journal ID: ISSN 2469-9950

Publisher:: American Physical Society (APS)

Country of Publication:: United States

Language:: English

Subject:: 72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS; 75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY; Material Science

Citation Formats


                    Kissikov, T., Dioguardi, A. P., Timmons, E. I., Tanatar, M. A., Prozorov, R., Bud'ko, S. L., Canfield, P. C., Fernandes, R. M., and Curro, N. J. NMR study of nematic spin fluctuations in a detwinned single crystal of underdoped Ba(Fe1₋xCox)2As2.  United States: N. p., 2016. 
Web.  doi:10.1103/PhysRevB.94.165123.

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                    Kissikov, T., Dioguardi, A. P., Timmons, E. I., Tanatar, M. A., Prozorov, R., Bud'ko, S. L., Canfield, P. C., Fernandes, R. M., & Curro, N. J. NMR study of nematic spin fluctuations in a detwinned single crystal of underdoped Ba(Fe1₋xCox)2As2.  United States.  https://doi.org/10.1103/PhysRevB.94.165123

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                    Kissikov, T., Dioguardi, A. P., Timmons, E. I., Tanatar, M. A., Prozorov, R., Bud'ko, S. L., Canfield, P. C., Fernandes, R. M., and Curro, N. J. Tue .  
"NMR study of nematic spin fluctuations in a detwinned single crystal of underdoped Ba(Fe1₋xCox)2As2".  United States.  https://doi.org/10.1103/PhysRevB.94.165123.  https://www.osti.gov/servlets/purl/1335028.

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@article{osti_1335028,

  title        = {NMR study of nematic spin fluctuations in a detwinned single crystal of underdoped Ba(Fe1₋xCox)2As2},

  author       = {Kissikov, T. and Dioguardi, A. P. and Timmons, E. I. and Tanatar, M. A. and Prozorov, R. and Bud'ko, S. L. and Canfield, P. C. and Fernandes, R. M. and Curro, N. J.},

  abstractNote = {We report the experimental details of how mechanical detwinning can be implemented in tandem with high sensitivity nuclear magnetic resonance measurements and use this setup to measure the inplane anisotropy of the spin-lattice relaxation rate in underdoped Ba(Fe1-xCox)2As2 with x = 0:048. The anisotropy reaches a maximum of 30% at TN, and the recovery data reveal that the glassy behavior of the spin fluctuations present in the twinned state persist in the fully detwinned crystal. A theoretical model is presented to describe the spin-lattice relaxation rate in terms of anisotropic nematic spin fluctuations.},

  doi          = {10.1103/PhysRevB.94.165123},

  journal      = {Physical Review B},

  number       = 16,

  volume       = 94,

  place        = {United States},

  year         = {Tue Oct 11 00:00:00 EDT 2016},

  month        = {Tue Oct 11 00:00:00 EDT 2016}

}

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Works referencing / citing this record:

Uniaxial strain control of spin-polarization in multicomponent nematic order of BaFe2As2
journal, March 2018

Kissikov, T.; Sarkar, R.; Lawson, M.
Nature Communications, Vol. 9, Issue 1
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Nuclear magnetic resonance probe head design for precision strain control
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Kissikov, T.; Sarkar, R.; Bush, B. T.
Review of Scientific Instruments, Vol. 88, Issue 10
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Divergence of the quadrupole-strain susceptibility of the electronic nematic system YbRu ₂ Ge ₂
journal, March 2019

Rosenberg, Elliott W.; Chu, Jiun-Haw; Ruff, Jacob P. C.
Proceedings of the National Academy of Sciences, Vol. 116, Issue 15
DOI: 10.1073/pnas.1818910116

Nematic fluctuations in iron arsenides NaFeAs and LiFeAs probed by ${}^{75}{As}$ NMR
journal, March 2018

Toyoda, Masayuki; Kobayashi, Yoshiaki; Itoh, Masayuki
Physical Review B, Vol. 97, Issue 9
DOI: 10.1103/physrevb.97.094515

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Title: NMR study of nematic spin fluctuations in a detwinned single crystal of underdoped Ba ( Fe 1 ₋ x Co x ) 2 As 2

Abstract

Citation Formats

Symmetry-breaking orbital anisotropy observed for detwinned Ba(Fe1-xCox)2As2 above the spin density wave transition journal, April 2011

Incommensurate Spin-Density Wave Order in Electron-Doped BaFe 2 As 2 Superconductors journal, June 2011

Angle-resolved NMR: Quantitative theory of 75 As T 1 relaxation rate in BaFe 2 As 2 journal, November 2011

Pairing Mechanism in Fe-Based Superconductors journal, March 2012

Nematic spin correlations in the tetragonal state of uniaxial-strained BaFe2-xNixAs2 journal, July 2014

Coexistence of Cluster Spin Glass and Superconductivity in Ba ( Fe 1 − x Co x ) 2 As 2 for 0.060 ≤ x ≤ 0.071 journal, November 2013

Manifestations of nematic degrees of freedom in the magnetic, elastic, and superconducting properties of the iron pnictides journal, July 2012

Local magnetic inhomogeneities in Ba ( Fe 1 − x Ni x ) 2 As 2 as seen via A 75 s NMR journal, October 2010

Magnetic order close to superconductivity in the iron-based layered LaO1-xF x FeAs systems journal, May 2008

Direct observation of spin–orbit coupling in iron-based superconductors journal, December 2015

Divergent Nematic Susceptibility in an Iron Arsenide Superconductor journal, August 2012

Atomic coexistence of superconductivity and incommensurate magnetic order in the pnictide Ba ( Fe 1 − x Co x ) 2 As 2 journal, October 2009

Origin of the Resistive Anisotropy in the Electronic Nematic Phase of BaFe 2 As 2 Revealed by Optical Spectroscopy journal, September 2015

Nematic Fermi Fluids in Condensed Matter Physics journal, August 2010

Normal-state spin dynamics and temperature-dependent spin-resonance energy in optimally doped BaFe1.85Co0.15As2 journal, December 2009

Spin reorientation driven by the interplay between spin-orbit coupling and Hund's rule coupling in iron pnictides journal, December 2015

Normal-state spin dynamics in the iron-pnictide superconductors BaFe 2 (As 1 − x P x ) 2 and Ba(Fe 1 − x Co x ) 2 As 2 probed with NMR measurements journal, May 2013

Antiferromagnetic order and spin dynamics in iron-based superconductors journal, August 2015

Commensurate antiferromagnetic ordering in Ba ( Fe 1 − x Co x ) 2 As 2 determined by x-ray resonant magnetic scattering at the Fe K edge journal, November 2010

Contrasting Spin Dynamics between Underdoped and Overdoped Ba ( Fe 1 − x Co x ) 2 As 2 journal, January 2010

Incommensurate spin density wave in Co-doped BaFe 2 As 2 journal, March 2010

C 59 o and A 75 s NMR investigation of lightly doped Ba ( Fe 1 − x Co x ) 2 As 2 ( x = 0.02 , 0.04 ) journal, April 2009

Identical spin fluctuations in Cu- and Co-doped BaFe 2 As 2 independent of electron doping journal, September 2014

Enhancement of Superconductivity near a Nematic Quantum Critical Point journal, March 2015

Critical behavior of the spin density wave transition in underdoped Ba(Fe 1 − x Co x ) 2 As 2 ( x ≤ 0.05 ): As 75 NMR investigation journal, June 2014

NMR evidence for inhomogeneous glassy behavior driven by nematic fluctuations in iron arsenide superconductors journal, October 2015

Space group symmetry, spin-orbit coupling, and the low-energy effective Hamiltonian for iron-based superconductors journal, October 2013

Pairing interaction near a nematic quantum critical point of a three-band CuO 2 model journal, November 2014

Magnetic excitations in underdoped Ba(Fe 1 − x Co x ) 2 As 2 with x = 0.047 journal, July 2012

Stretched exponential relaxation arising from a continuous sum of exponential decays journal, November 2006

Antiferromagnetism of SrFe 2 As 2 Studied by Single-Crystal 75 As-NMR journal, June 2009

FeAs-Based Superconductivity: A Case Study of the Effects of Transition Metal Doping on BaFe 2 As 2 journal, August 2010

Evidence of local disorder in the overdoped regime of Ba(Fe 1 − x Co x ) 2 As 2 journal, July 2011

Spatial inhomogeneities in iron pnictide superconductors: The formation of charge stripes journal, July 2010

Neutron-Scattering Measurements of Spin Excitations in LaFeAsO and Ba ( Fe 0.953 Co 0.047 ) 2 As 2 : Evidence for a Sharp Enhancement of Spin Fluctuations by Nematic Order journal, February 2015

Direct imaging of the structural domains in the iron pnictides A Fe 2 As 2 ( A = Ca , Sr , Ba ) journal, May 2009

Antiferromagnetic spin fluctuation and superconductivity journal, July 2003

What drives nematic order in iron-based superconductors? journal, January 2014

Evolution of antiferromagnetic susceptibility under uniaxial pressure in Ba( Fe 1 − x Co x ) 2 As 2 journal, June 2014

In-Plane Resistivity Anisotropy in an Underdoped Iron Arsenide Superconductor journal, August 2010

Unconventional Superconductivity and Antiferromagnetic Quantum Critical Behavior in the Isovalent-Doped BaFe 2 ( As 1 − x P x ) 2 journal, September 2010

Preemptive nematic order, pseudogap, and orbital order in the iron pnictides journal, January 2012

The puzzle of high temperature superconductivity in layered iron pnictides and chalcogenides journal, October 2010

Commensurate Itinerant Antiferromagnetism in BaFe2As2: 75As-NMR Studies on a Self-Flux Grown Single Crystal text, January 2008

FeAs-based superconductivity: a case study of the effects of transition metal doping on BaFe2As2 text, January 2010

Preemptive nematic order, pseudogap, and orbital order in the iron pnictides text, January 2011

Effect of tensile stress on the in-plane resistivity anisotropy in BaFe2As2 text, January 2011

Manifestations of nematic degrees of freedom in the magnetic, elastic, and superconducting properties of the iron pnictides text, January 2012

Magnetic excitations in underdoped Ba(Fe1-xCox)2As2 with x=0.047 text, January 2012

Space group symmetry, spin-orbit coupling and the low energy effective Hamiltonian for iron based superconductors text, January 2013

Normal state spin dynamics in the iron-pnictide superconductors BaFe2(As1-xPx)2 and Ba(Fe1-xCox)2As2 probed with NMR measurements text, January 2013

Direct observation of spin-orbit coupling in iron-based superconductors text, January 2014

Neutron-scattering measurements of the spin excitations in LaFeAsO and Ba(Fe$_{0.953}$Co$_{0.047}$)$_{2}$As$_{2}$: Evidence for a sharp enhancement of spin fluctuations by nematic order text, January 2014

NMR evidence for inhomogeneous glassy behavior driven by nematic fluctuations in iron arsenide superconductors text, January 2015

Antiferromagnetic order and spin dynamics in iron-based superconductors text, January 2015

Uniaxial strain control of spin-polarization in multicomponent nematic order of BaFe2As2 journal, March 2018

Nuclear magnetic resonance probe head design for precision strain control journal, October 2017

Divergence of the quadrupole-strain susceptibility of the electronic nematic system YbRu 2 Ge 2 journal, March 2019

Nematic fluctuations in iron arsenides NaFeAs and LiFeAs probed by As 75 NMR journal, March 2018

Title: NMR study of nematic spin fluctuations in a detwinned single crystal of underdoped $Ba {({Fe}_{1 ₋ x} {Co}_{x})}_{2} {As}_{2}$

Symmetry-breaking orbital anisotropy observed for detwinned Ba(Fe1-xCox)2As2 above the spin density wave transition
journal, April 2011

Incommensurate Spin-Density Wave Order in Electron-Doped ${BaFe}_{2} {As}_{2}$ Superconductors
journal, June 2011

Angle-resolved NMR: Quantitative theory of $^{75}$ As $T_{1}$ relaxation rate in BaFe $_{2}$ As $_{2}$
journal, November 2011

Pairing Mechanism in Fe-Based Superconductors
journal, March 2012

Nematic spin correlations in the tetragonal state of uniaxial-strained BaFe2-xNixAs2
journal, July 2014

Coexistence of Cluster Spin Glass and Superconductivity in $Ba ({Fe}_{1 - x} {Co}_{x})_{2} {As}_{2}$ for $0.060 \leq x \leq 0.071$
journal, November 2013

Manifestations of nematic degrees of freedom in the magnetic, elastic, and superconducting properties of the iron pnictides
journal, July 2012

Local magnetic inhomogeneities in $Ba {({Fe}_{1 - x} {Ni}_{x})}_{2} {As}_{2}$ as seen via ${}^{75}A s$ NMR
journal, October 2010

Magnetic order close to superconductivity in the iron-based layered LaO1-xF x FeAs systems
journal, May 2008

Direct observation of spin–orbit coupling in iron-based superconductors
journal, December 2015

Divergent Nematic Susceptibility in an Iron Arsenide Superconductor
journal, August 2012

Atomic coexistence of superconductivity and incommensurate magnetic order in the pnictide $Ba {({Fe}_{1 - x} {Co}_{x})}_{2} {As}_{2}$
journal, October 2009

Origin of the Resistive Anisotropy in the Electronic Nematic Phase of ${BaFe}_{2} {As}_{2}$ Revealed by Optical Spectroscopy
journal, September 2015

Nematic Fermi Fluids in Condensed Matter Physics
journal, August 2010

Normal-state spin dynamics and temperature-dependent spin-resonance energy in optimally doped BaFe1.85Co0.15As2
journal, December 2009

Spin reorientation driven by the interplay between spin-orbit coupling and Hund's rule coupling in iron pnictides
journal, December 2015

Normal-state spin dynamics in the iron-pnictide superconductors BaFe $_{2}$ (As $_{1 - x}$ P $_{x}$ ) $_{2}$ and Ba(Fe $_{1 - x}$ Co $_{x}$ ) $_{2}$ As $_{2}$ probed with NMR measurements
journal, May 2013

Antiferromagnetic order and spin dynamics in iron-based superconductors
journal, August 2015

Commensurate antiferromagnetic ordering in $Ba {({Fe}_{1 - x} {Co}_{x})}_{2} {As}_{2}$ determined by x-ray resonant magnetic scattering at the $Fe K$ edge
journal, November 2010

Contrasting Spin Dynamics between Underdoped and Overdoped $Ba ({Fe}_{1 - x} {Co}_{x})_{2} {As}_{2}$
journal, January 2010

Incommensurate spin density wave in Co-doped BaFe ₂ As ₂
journal, March 2010

${}^{59}C o$ and ${}^{75}A s$ NMR investigation of lightly doped $Ba {({Fe}_{1 - x} {Co}_{x})}_{2} {As}_{2}$ $(x = 0.02, 0.04)$
journal, April 2009

Identical spin fluctuations in Cu- and Co-doped ${BaFe}_{2} {As}_{2}$ independent of electron doping
journal, September 2014

Enhancement of Superconductivity near a Nematic Quantum Critical Point
journal, March 2015

Critical behavior of the spin density wave transition in underdoped ${Ba(Fe}_{1 - x} {Co}_{x})_{2} {As}_{2}$ ( $x \leq 0.05$ ): ${}^{75}{As}$ NMR investigation
journal, June 2014

NMR evidence for inhomogeneous glassy behavior driven by nematic fluctuations in iron arsenide superconductors
journal, October 2015

Space group symmetry, spin-orbit coupling, and the low-energy effective Hamiltonian for iron-based superconductors
journal, October 2013

Pairing interaction near a nematic quantum critical point of a three-band ${CuO}_{2}$ model
journal, November 2014

Magnetic excitations in underdoped Ba(Fe $_{1 - x}$ Co $_{x}$ ) $_{2}$ As $_{2}$ with $x = 0.047$
journal, July 2012

Stretched exponential relaxation arising from a continuous sum of exponential decays
journal, November 2006

Antiferromagnetism of SrFe ₂ As ₂ Studied by Single-Crystal ⁷⁵ As-NMR
journal, June 2009

FeAs-Based Superconductivity: A Case Study of the Effects of Transition Metal Doping on BaFe ₂ As ₂
journal, August 2010

Evidence of local disorder in the overdoped regime of Ba(Fe $_{1 - x}$ Co $_{x}$ ) $_{2}$ As $_{2}$
journal, July 2011

Spatial inhomogeneities in iron pnictide superconductors: The formation of charge stripes
journal, July 2010

Neutron-Scattering Measurements of Spin Excitations in LaFeAsO and $Ba ({Fe}_{0.953} {Co}_{0.047})_{2} {As}_{2}$ : Evidence for a Sharp Enhancement of Spin Fluctuations by Nematic Order
journal, February 2015

Direct imaging of the structural domains in the iron pnictides $A {Fe}_{2} {As}_{2}$ $(A = Ca, Sr, Ba)$
journal, May 2009

Antiferromagnetic spin fluctuation and superconductivity
journal, July 2003

What drives nematic order in iron-based superconductors?
journal, January 2014

Evolution of antiferromagnetic susceptibility under uniaxial pressure in Ba( ${Fe}_{1 - x} {Co}_{x}$ ) $_{2} {As}_{2}$
journal, June 2014

In-Plane Resistivity Anisotropy in an Underdoped Iron Arsenide Superconductor
journal, August 2010

Unconventional Superconductivity and Antiferromagnetic Quantum Critical Behavior in the Isovalent-Doped ${BaFe}_{2} ({As}_{1 - x} P_{x})_{2}$
journal, September 2010

Preemptive nematic order, pseudogap, and orbital order in the iron pnictides
journal, January 2012

The puzzle of high temperature superconductivity in layered iron pnictides and chalcogenides
journal, October 2010

Commensurate Itinerant Antiferromagnetism in BaFe2As2: 75As-NMR Studies on a Self-Flux Grown Single Crystal
text, January 2008

FeAs-based superconductivity: a case study of the effects of transition metal doping on BaFe2As2
text, January 2010

Preemptive nematic order, pseudogap, and orbital order in the iron pnictides
text, January 2011

Effect of tensile stress on the in-plane resistivity anisotropy in BaFe2As2
text, January 2011

Manifestations of nematic degrees of freedom in the magnetic, elastic, and superconducting properties of the iron pnictides
text, January 2012

Magnetic excitations in underdoped Ba(Fe1-xCox)2As2 with x=0.047
text, January 2012

Space group symmetry, spin-orbit coupling and the low energy effective Hamiltonian for iron based superconductors
text, January 2013

Normal state spin dynamics in the iron-pnictide superconductors BaFe2(As1-xPx)2 and Ba(Fe1-xCox)2As2 probed with NMR measurements
text, January 2013

Direct observation of spin-orbit coupling in iron-based superconductors
text, January 2014

Neutron-scattering measurements of the spin excitations in LaFeAsO and Ba(Fe$_{0.953}$Co$_{0.047}$)$_{2}$As$_{2}$: Evidence for a sharp enhancement of spin fluctuations by nematic order
text, January 2014

NMR evidence for inhomogeneous glassy behavior driven by nematic fluctuations in iron arsenide superconductors
text, January 2015

Antiferromagnetic order and spin dynamics in iron-based superconductors
text, January 2015

Uniaxial strain control of spin-polarization in multicomponent nematic order of BaFe2As2
journal, March 2018

Nuclear magnetic resonance probe head design for precision strain control
journal, October 2017

Divergence of the quadrupole-strain susceptibility of the electronic nematic system YbRu ₂ Ge ₂
journal, March 2019

Nematic fluctuations in iron arsenides NaFeAs and LiFeAs probed by ${}^{75}{As}$ NMR
journal, March 2018