Stability of nanosized oxides in ferrite under extremely high dose self ion irradiations
Abstract
We produced a nanostructured ferritic alloy (NFA), 14YWT, in the form of thin walled tubing. The stability of the nano-oxides (NOs) was determined under 3.5 MeV Fe+2 irradiations up to a dose of ~585 dpa at 450 °C. Transmission electron microscopy (TEM) and atom probe tomography (APT) show that severe ion irradiation results in a ~25% reduction in size between the unirradiated and irradiated case at 270 dpa while no further reduction within the experimental error was seen at higher doses. Conversely, number density increased by ~30% after irradiation. Moreover, this ‘inverse coarsening’ can be rationalized by the competition between radiation driven ballistic dissolution and diffusional NO reformation. There were no significant changes in the composition of the matrix or NOs observed after irradiation. Modeling the experimental results also indicated a dissolution of the particles.
- Authors:
-
- Univ. of California, Santa Barbara, CA (United States)
- Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
- Univ. of New Mexico, Albuquerque, NM (United States)
- Texas A & M Univ., College Station, TX (United States)
- Case Western Reserve Univ., Cleveland, OH (United States)
- Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
- Publication Date:
- Research Org.:
- Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
- Sponsoring Org.:
- USDOE Office of Nuclear Energy (NE); USDOE Office of Science (SC), Fusion Energy Sciences (FES)
- OSTI Identifier:
- 1351787
- Alternate Identifier(s):
- OSTI ID: 1340917; OSTI ID: 1419385
- Report Number(s):
- LA-UR-16-22034
Journal ID: ISSN 0022-3115; AF5810000; NEAF225; TRN: US1701012
- Grant/Contract Number:
- AC05-00OR22725; AC52-06NA25396; NE0008297
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Journal of Nuclear Materials
- Additional Journal Information:
- Journal Volume: 486; Journal Issue: C; Journal ID: ISSN 0022-3115
- Publisher:
- Elsevier
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS; 36 MATERIALS SCIENCE
Citation Formats
Almirall, Nathan, Odette, George R., Maloy, S. A., Anderoglu, Osman, Shao, Lin, Gigax, Jonathan G., Price, Lloyd, Chen, D., Chen, Tianyi, Garner, Frank A., Wu, Yuan, Wells, Peter, Lewandowski, John J., Hoelzer, David T., and Aydogan, Eda. Stability of nanosized oxides in ferrite under extremely high dose self ion irradiations. United States: N. p., 2017.
Web. doi:10.1016/j.jnucmat.2017.01.015.
Almirall, Nathan, Odette, George R., Maloy, S. A., Anderoglu, Osman, Shao, Lin, Gigax, Jonathan G., Price, Lloyd, Chen, D., Chen, Tianyi, Garner, Frank A., Wu, Yuan, Wells, Peter, Lewandowski, John J., Hoelzer, David T., & Aydogan, Eda. Stability of nanosized oxides in ferrite under extremely high dose self ion irradiations. United States. https://doi.org/10.1016/j.jnucmat.2017.01.015
Almirall, Nathan, Odette, George R., Maloy, S. A., Anderoglu, Osman, Shao, Lin, Gigax, Jonathan G., Price, Lloyd, Chen, D., Chen, Tianyi, Garner, Frank A., Wu, Yuan, Wells, Peter, Lewandowski, John J., Hoelzer, David T., and Aydogan, Eda. Tue .
"Stability of nanosized oxides in ferrite under extremely high dose self ion irradiations". United States. https://doi.org/10.1016/j.jnucmat.2017.01.015. https://www.osti.gov/servlets/purl/1351787.
@article{osti_1351787,
title = {Stability of nanosized oxides in ferrite under extremely high dose self ion irradiations},
author = {Almirall, Nathan and Odette, George R. and Maloy, S. A. and Anderoglu, Osman and Shao, Lin and Gigax, Jonathan G. and Price, Lloyd and Chen, D. and Chen, Tianyi and Garner, Frank A. and Wu, Yuan and Wells, Peter and Lewandowski, John J. and Hoelzer, David T. and Aydogan, Eda},
abstractNote = {We produced a nanostructured ferritic alloy (NFA), 14YWT, in the form of thin walled tubing. The stability of the nano-oxides (NOs) was determined under 3.5 MeV Fe+2 irradiations up to a dose of ~585 dpa at 450 °C. Transmission electron microscopy (TEM) and atom probe tomography (APT) show that severe ion irradiation results in a ~25% reduction in size between the unirradiated and irradiated case at 270 dpa while no further reduction within the experimental error was seen at higher doses. Conversely, number density increased by ~30% after irradiation. Moreover, this ‘inverse coarsening’ can be rationalized by the competition between radiation driven ballistic dissolution and diffusional NO reformation. There were no significant changes in the composition of the matrix or NOs observed after irradiation. Modeling the experimental results also indicated a dissolution of the particles.},
doi = {10.1016/j.jnucmat.2017.01.015},
journal = {Journal of Nuclear Materials},
number = C,
volume = 486,
place = {United States},
year = {Tue Jan 10 00:00:00 EST 2017},
month = {Tue Jan 10 00:00:00 EST 2017}
}
Web of Science
Works referenced in this record:
Cladding and duct materials for advanced nuclear recycle reactors
journal, January 2008
- Allen, T. R.; Busby, J. T.; Klueh, R. L.
- JOM, Vol. 60, Issue 1
Recent Developments in Irradiation-Resistant Steels
journal, August 2008
- Odette, G. R.; Alinger, M. J.; Wirth, B. D.
- Annual Review of Materials Research, Vol. 38, Issue 1, p. 471-503
Irradiation-tolerant nanostructured ferritic alloys: Transforming helium from a liability to an asset
journal, September 2010
- Odette, G. R.; Hoelzer, D. T.
- JOM, Vol. 62, Issue 9
Recent Progress in Developing and Qualifying Nanostructured Ferritic Alloys for Advanced Fission and Fusion Applications
journal, November 2014
- Odette, G. R.
- JOM, Vol. 66, Issue 12
Transmission electron microscopy characterization of the nanofeatures in nanostructured ferritic alloy MA957
journal, May 2012
- Wu, Y.; Haney, E. M.; Cunningham, N. J.
- Acta Materialia, Vol. 60, Issue 8
Glancing angle XRD analysis of particle stability under self-ion irradiation in oxide dispersion strengthened alloys
journal, January 2016
- London, A. J.; Panigrahi, B. K.; Tang, C. C.
- Scripta Materialia, Vol. 110
A new method for the quantitative analysis of the scale and composition of nanosized oxide in 9Cr-ODS steel
journal, October 2009
- Ohnuma, M.; Suzuki, J.; Ohtsuka, S.
- Acta Materialia, Vol. 57, Issue 18
Phase stability of oxide dispersion-strengthened ferritic steels in neutron irradiation
journal, December 2002
- Yamashita, S.; Oka, K.; Ohnuki, S.
- Journal of Nuclear Materials, Vol. 307-311
Microstructural development of a heavily neutron-irradiated ODS ferritic steel (MA957) at elevated temperature
journal, August 2007
- Yamashita, S.; Akasaka, N.; Ukai, S.
- Journal of Nuclear Materials, Vol. 367-370
Structural and chemical matrix evolution following neutron irradiation in a MA957 oxide dispersion strengthened material
journal, March 2013
- Ribis, J.
- Journal of Nuclear Materials, Vol. 434, Issue 1-3
Orientation relationships and interface structure of α′-Cr nanoclusters embedded in α-Fe matrix after α–α′ demixing in neutron irradiated Oxide Dispersion Strengthened material
journal, May 2012
- Ribis, J.; Lozano-Perez, S.
- Materials Letters, Vol. 74
Nano-cluster stability following neutron irradiation in MA957 oxide dispersion strengthened material
journal, January 2014
- Ribis, J.; Lozano-Perez, S.
- Journal of Nuclear Materials, Vol. 444, Issue 1-3
Atom probe tomography analysis of high dose MA957 at selected irradiation temperatures
journal, April 2015
- Bailey, Nathan A.; Stergar, Erich; Toloczko, Mychailo
- Journal of Nuclear Materials, Vol. 459
Microstructural changes of neutron irradiated ODS ferritic and martensitic steels
journal, August 2004
- Akasaka, N.; Yamashita, S.; Yoshitake, T.
- Journal of Nuclear Materials, Vol. 329-333
Stability of nanometer-sized oxide clusters in mechanically-alloyed steel under ion-induced displacement cascade damage conditions
journal, February 2007
- Pareige, P.; Miller, M. K.; Stoller, R. E.
- Journal of Nuclear Materials, Vol. 360, Issue 2
High Burnup Fuel Cladding Materials R&D for Advanced Nuclear Systems: Nano-sized oxide dispersion strengthening steels
journal, March 2007
- Kimura, Akihiko; Cho, Han-Sik; Toda, Naoki
- Journal of Nuclear Science and Technology, Vol. 44, Issue 3
Stability of Y–Ti complex oxides in Fe–16Cr–0.1Ti ODS ferritic steel before and after heavy-ion irradiation
journal, April 2009
- Kishimoto, H.; Kasada, R.; Hashitomi, O.
- Journal of Nuclear Materials, Vol. 386-388
Heavy-ion irradiation effects on the morphology of complex oxide particles in oxide dispersion strengthened ferritic steels
journal, August 2007
- Kishimoto, H.; Yutani, K.; Kasada, R.
- Journal of Nuclear Materials, Vol. 367-370
Radiation response of a 9 chromium oxide dispersion strengthened steel to heavy ion irradiation
journal, March 2008
- Allen, T. R.; Gan, J.; Cole, J. I.
- Journal of Nuclear Materials, Vol. 375, Issue 1
Response of nanostructured ferritic alloys to high-dose heavy ion irradiation
journal, February 2014
- Parish, Chad M.; White, Ryan M.; LeBeau, James M.
- Journal of Nuclear Materials, Vol. 445, Issue 1-3
Radiation stability of nanoclusters in nano-structured oxide dispersion strengthened (ODS) steels
journal, March 2013
- Certain, A.; Kuchibhatla, S.; Shutthanandan, V.
- Journal of Nuclear Materials, Vol. 434, Issue 1-3
Stability of nanoclusters in 14YWT oxide dispersion strengthened steel under heavy ion-irradiation by atom probe tomography
journal, December 2014
- He, Jianchao; Wan, Farong; Sridharan, Kumar
- Journal of Nuclear Materials, Vol. 455, Issue 1-3
Effect of nano-oxide particle size on radiation resistance of iron–chromium alloys
journal, February 2016
- Xu, Weizong; Li, Lulu; Valdez, James A.
- Journal of Nuclear Materials, Vol. 469
Nano-oxide particle stability of 9–12Cr grain morphology modified ODS steels under neutron irradiation
journal, August 2004
- Yamashita, S.; Akasaka, N.; Ohnuki, S.
- Journal of Nuclear Materials, Vol. 329-333
The crystal structure, orientation relationships and interfaces of the nanoscale oxides in nanostructured ferritic alloys
journal, June 2016
- Wu, Yuan; Ciston, Jim; Kräemer, Stephan
- Acta Materialia, Vol. 111
Effect of tube processing methods on the texture and grain boundary characteristics of 14YWT nanostructured ferritic alloys
journal, April 2016
- Aydogan, E.; Pal, S.; Anderoglu, O.
- Materials Science and Engineering: A, Vol. 661
Effect of irradiation mode on the microstructure of self-ion irradiated ferritic-martensitic alloys
journal, October 2015
- Getto, E.; Jiao, Z.; Monterrosa, A. M.
- Journal of Nuclear Materials, Vol. 465
The influence of ion beam rastering on the swelling of self-ion irradiated pure iron at 450 °C
journal, October 2015
- Gigax, Jonathan G.; Aydogan, Eda; Chen, Tianyi
- Journal of Nuclear Materials, Vol. 465
Interfacial strained structure and orientation relationships of the nanosized oxide particles deduced from elasticity-driven morphology in oxide dispersion strengthened materials
journal, January 2012
- Ribis, J.; de Carlan, Y.
- Acta Materialia, Vol. 60, Issue 1
Radiation-induced Ostwald ripening in oxide dispersion strengthened ferritic steels irradiated at high ion dose
journal, October 2014
- Lescoat, M. -L.; Ribis, J.; Chen, Y.
- Acta Materialia, Vol. 78
A procedure for quantification of precipitate microstructures from three-dimensional atom probe data
journal, May 2003
- Vaumousse, D.; Cerezo, A.; Warren, P. J.
- Ultramicroscopy, Vol. 95
On the remarkable thermal stability of nanostructured ferritic alloys
journal, September 2014
- Cunningham, N.; Wu, Y.; Klingensmith, D.
- Materials Science and Engineering: A, Vol. 613
Nanoscale characterisation of ODS–Eurofer 97 steel: An atom-probe tomography study
journal, May 2010
- Williams, Ceri A.; Marquis, Emmanuelle A.; Cerezo, Alfred
- Journal of Nuclear Materials, Vol. 400, Issue 1
On the Field Evaporation Behavior of Dielectric Materials in Three-Dimensional Atom Probe: A Numeric Simulation
journal, October 2010
- Oberdorfer, Christian; Schmitz, Guido
- Microscopy and Microanalysis, Vol. 17, Issue 1
Core/shell structures of oxygen-rich nanofeatures in oxide-dispersion strengthened Fe–Cr alloys
journal, November 2008
- Marquis, Emmanuelle A.
- Applied Physics Letters, Vol. 93, Issue 18, Article No. 181904
Quantification of oxide particle composition in model oxide dispersion strengthened steel alloys
journal, December 2015
- London, A. J.; Lozano-Perez, S.; Moody, M. P.
- Ultramicroscopy, Vol. 159
New insights into the chemical structure of Y2Ti2O7−δ nanoparticles in oxide dispersion-strengthened steels designed for sodium fast reactors by electron energy-loss spectroscopy
journal, January 2015
- Badjeck, V.; Walls, M. G.; Chaffron, L.
- Journal of Nuclear Materials, Vol. 456
Microstructural changes and void swelling of a 12Cr ODS ferritic-martensitic alloy after high-dpa self-ion irradiation
journal, December 2015
- Chen, Tianyi; Aydogan, Eda; Gigax, Jonathan G.
- Journal of Nuclear Materials, Vol. 467
Synchrotron study on load partitioning between ferrite/martensite and nanoparticles of a 9Cr ODS steel
journal, December 2014
- Mo, Kun; Zhou, Zhangjian; Miao, Yinbin
- Journal of Nuclear Materials, Vol. 455, Issue 1-3
In situ synchrotron tensile investigations on the phase responses within an oxide dispersion-strengthened (ODS) 304 steel
journal, February 2015
- Miao, Yinbin; Mo, Kun; Zhou, Zhangjian
- Materials Science and Engineering: A, Vol. 625
The stability of precipitates in an irradiation environment
journal, September 1972
- Nelson, R. S.; Hudson, J. A.; Mazey, D. J.
- Journal of Nuclear Materials, Vol. 44, Issue 3
Temperature dependent dispersoid stability in ion-irradiated ferritic-martensitic dual-phase oxide-dispersion-strengthened alloy: Coherent interfaces vs. incoherent interfaces
journal, September 2016
- Chen, Tianyi; Gigax, Jonathan G.; Price, Lloyd
- Acta Materialia, Vol. 116
Theory of diffusion-limited precipitation
journal, September 1958
- Ham, Frank S.
- Journal of Physics and Chemistry of Solids, Vol. 6, Issue 4
Point defect survival and clustering fractions obtained from molecular dynamics simulations of high energy cascades
journal, October 1996
- Stoller, Roger E.
- Journal of Nuclear Materials, Vol. 233-237
Cu-precipitation kinetics in from atomistic simulations: Vacancy-trapping effects and Cu-cluster mobility
journal, December 2007
- Soisson, Frédéric; Fu, Chu-Chun
- Physical Review B, Vol. 76, Issue 21
Formation of Y2O3 nanoclusters in nano-structured ferritic alloys: Modeling of precipitation kinetics and yield strength
journal, July 2010
- Hin, Céline; Wirth, Brian D.
- Journal of Nuclear Materials, Vol. 402, Issue 1
Thermodynamic and kinetic modeling of oxide precipitation in nanostructured ferritic alloys
journal, June 2015
- Barnard, L.; Cunningham, N.; Odette, G. R.
- Acta Materialia, Vol. 91
Recoil resolution and particle stability under irradiation
journal, January 1981
- Frost, H. J.; Russell, K. C.
- Journal of Nuclear Materials, Vol. 104
Phase stability in thermally-aged CASS CF8 under heavy ion irradiation
journal, July 2015
- Li, Meimei; Miller, Michael K.; Chen, Wei-Ying
- Journal of Nuclear Materials, Vol. 462
Stability of MX-type strengthening nanoprecipitates in ferritic steels under thermal aging, stress and ion irradiation
journal, June 2014
- Tan, L.; Byun, T. S.; Katoh, Y.
- Acta Materialia, Vol. 71
Works referencing / citing this record:
Effect of High-Density Nanoparticles on Recrystallization and Texture Evolution in Ferritic Alloys
journal, March 2019
- Aydogan, Eda; Rietema, Connor; Carvajal-Nunez, Ursula
- Crystals, Vol. 9, Issue 3
α′ formation kinetics and radiation induced segregation in neutron irradiated 14YWT nanostructured ferritic alloys
journal, June 2019
- Aydogan, E.; Martinez, E.; March, K.
- Scientific Reports, Vol. 9, Issue 1
Influence of Al Addition Strategy on the Microstructure of a Low‐Cr Oxide Dispersion‐Strengthened Ferritic Steel
journal, December 2019
- Xu, Shuai; Zhou, Zhangjian; Long, Fei
- Advanced Engineering Materials, Vol. 22, Issue 4
An in situ study on Kr ion–irradiated crystalline Cu/amorphous-CuNb nanolaminates
journal, March 2019
- Fan, Zhe; Fan, Cuncai; Li, Jin
- Journal of Materials Research, Vol. 34, Issue 13