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Title: Gold nanotriangles decorated with superparamagnetic iron oxide nanoparticles: a compositional and microstructural study

The combination of iron oxide and gold in a single nanoparticle results in both magnetic and plasmonic properties that can stimulate novel applications in bio-sensing, medical imaging, or therapeutics. Microwave assisted heating allows the fabrication of multi-component, multi-functional nanostructures by promoting selective heating at desired sites. Recently, we reported a microwave-assisted polyol route yielding gold nanotriangles decorated with iron oxide nanoparticles. Here, we present an in-depth microstructural and compositional characterization of the system by using scanning transmission electron microscopy (STEM) and electron energy loss (EELS) spectroscopy. A method to remove the iron oxide nanoparticles from the gold nanocrystals and some insights on crystal nucleation and growth mechanisms are also provided.
Authors:
 [1] ;  [2] ;  [1] ;  [1] ;  [2] ;  [2] ;  [2]
  1. Vanderbilt Univ., Nashville, TN (United States); Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
  2. Inst. de Ciencia de Materials de Barcelona (ICMAP-CSIC), Catalonia (Spain)
Publication Date:
Grant/Contract Number:
AC05-00OR22725
Type:
Accepted Manuscript
Journal Name:
Faraday Discussions
Additional Journal Information:
Journal Volume: 191; Journal ID: ISSN 1359-6640
Publisher:
Royal Society of Chemistry
Research Org:
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Sponsoring Org:
USDOE
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE
OSTI Identifier:
1348341

Hachtel, J. A., Yu, S., Lupini, A. R., Pantelides, S. T., Gich, M., Laromaine, A., and Roig, A.. Gold nanotriangles decorated with superparamagnetic iron oxide nanoparticles: a compositional and microstructural study. United States: N. p., Web. doi:10.1039/C6FD00028B.
Hachtel, J. A., Yu, S., Lupini, A. R., Pantelides, S. T., Gich, M., Laromaine, A., & Roig, A.. Gold nanotriangles decorated with superparamagnetic iron oxide nanoparticles: a compositional and microstructural study. United States. doi:10.1039/C6FD00028B.
Hachtel, J. A., Yu, S., Lupini, A. R., Pantelides, S. T., Gich, M., Laromaine, A., and Roig, A.. 2016. "Gold nanotriangles decorated with superparamagnetic iron oxide nanoparticles: a compositional and microstructural study". United States. doi:10.1039/C6FD00028B. https://www.osti.gov/servlets/purl/1348341.
@article{osti_1348341,
title = {Gold nanotriangles decorated with superparamagnetic iron oxide nanoparticles: a compositional and microstructural study},
author = {Hachtel, J. A. and Yu, S. and Lupini, A. R. and Pantelides, S. T. and Gich, M. and Laromaine, A. and Roig, A.},
abstractNote = {The combination of iron oxide and gold in a single nanoparticle results in both magnetic and plasmonic properties that can stimulate novel applications in bio-sensing, medical imaging, or therapeutics. Microwave assisted heating allows the fabrication of multi-component, multi-functional nanostructures by promoting selective heating at desired sites. Recently, we reported a microwave-assisted polyol route yielding gold nanotriangles decorated with iron oxide nanoparticles. Here, we present an in-depth microstructural and compositional characterization of the system by using scanning transmission electron microscopy (STEM) and electron energy loss (EELS) spectroscopy. A method to remove the iron oxide nanoparticles from the gold nanocrystals and some insights on crystal nucleation and growth mechanisms are also provided.},
doi = {10.1039/C6FD00028B},
journal = {Faraday Discussions},
number = ,
volume = 191,
place = {United States},
year = {2016},
month = {3}
}