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Title: Polarized light microscopy study on the reentrant phase transition in a (Ba 1–xK x)Fe 2As 2 single crystal with x = 0.24

In this study, a sequence of structural/magnetic transitions on cooling is reported in the literature for hole-doped iron-based superconductor (Ba 1–xK x)Fe 2As 2 with x = 0.24. By using polarized light microscopy, we directly observe the formation of orthorhombic domains in (Ba 1–xK x)Fe 2As 2 (x = 0.24) single crystal below a temperature of simultaneous structural/magnetic transition T N ~ 80 K. The structural domains vanish below ~30 K, but reappear below T = 15 K. Our results are consistent with reentrance transformation sequence from high-temperature tetragonal (HTT) to low temperature orthorhombic (LTO1) structure at T N ~ 80 K, LTO1 to low temperature tetragonal (LTT) structure at T c ~ 25 K, and LTT to low temperature orthorhombic (LTO2) structure at T ~ 15 K.
Authors:
 [1] ;  [2] ;  [2] ;  [2]
  1. Ames Lab., Ames, IA (United States)
  2. Ames Lab. and Iowa State Univ., Ames, IA (United States)
Publication Date:
Report Number(s):
IS-J-9184
Journal ID: ISSN 2073-4352; CRYSBC; PII: cryst6110142
Grant/Contract Number:
AC02-07CH11358
Type:
Accepted Manuscript
Journal Name:
Crystals
Additional Journal Information:
Journal Volume: 6; Journal Issue: 11; Journal ID: ISSN 2073-4352
Publisher:
MDPI
Research Org:
Ames Laboratory (AMES), Ames, IA (United States)
Sponsoring Org:
USDOE
Country of Publication:
United States
Language:
English
Subject:
75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY; reentrant phase transition; polarized optical images; structural domains
OSTI Identifier:
1347413

Liu, Yong, Tanatar, Makariy A., Timmons, Erik, and Lograsso, Thomas A.. Polarized light microscopy study on the reentrant phase transition in a (Ba1–xKx)Fe2As2 single crystal with x = 0.24. United States: N. p., Web. doi:10.3390/cryst6110142.
Liu, Yong, Tanatar, Makariy A., Timmons, Erik, & Lograsso, Thomas A.. Polarized light microscopy study on the reentrant phase transition in a (Ba1–xKx)Fe2As2 single crystal with x = 0.24. United States. doi:10.3390/cryst6110142.
Liu, Yong, Tanatar, Makariy A., Timmons, Erik, and Lograsso, Thomas A.. 2016. "Polarized light microscopy study on the reentrant phase transition in a (Ba1–xKx)Fe2As2 single crystal with x = 0.24". United States. doi:10.3390/cryst6110142. https://www.osti.gov/servlets/purl/1347413.
@article{osti_1347413,
title = {Polarized light microscopy study on the reentrant phase transition in a (Ba1–xKx)Fe2As2 single crystal with x = 0.24},
author = {Liu, Yong and Tanatar, Makariy A. and Timmons, Erik and Lograsso, Thomas A.},
abstractNote = {In this study, a sequence of structural/magnetic transitions on cooling is reported in the literature for hole-doped iron-based superconductor (Ba1–xKx)Fe2As2 with x = 0.24. By using polarized light microscopy, we directly observe the formation of orthorhombic domains in (Ba1–xKx)Fe2As2 (x = 0.24) single crystal below a temperature of simultaneous structural/magnetic transition TN ~ 80 K. The structural domains vanish below ~30 K, but reappear below T = 15 K. Our results are consistent with reentrance transformation sequence from high-temperature tetragonal (HTT) to low temperature orthorhombic (LTO1) structure at TN ~ 80 K, LTO1 to low temperature tetragonal (LTT) structure at Tc ~ 25 K, and LTT to low temperature orthorhombic (LTO2) structure at T ~ 15 K.},
doi = {10.3390/cryst6110142},
journal = {Crystals},
number = 11,
volume = 6,
place = {United States},
year = {2016},
month = {11}
}