DOE PAGES title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Control of Reaction Kinetics During Friction Stir Processing

Abstract

Friction stir processing (FSP) was used to successfully embed galfenol particles into aluminum (AA 1100 Al) matrix uniformly. But, intermetallic layer of Al3Fe was formed around the galfenol particles. We estimated the activation energy for Al3Fe formation during FSP, and attempts were made to minimize the Al3Fe layer thickness. By changing the processing conditions, FSP successfully eliminated the intermetallic layer. Therefore, FSP, in addition to microstructural control, can successfully fabricate intermetallic-free embedded regions by controlling the reaction kinetics.

Authors:
 [1];  [1];  [1];  [2];  [3]
  1. Univ. of North Texas, Denton, TX (United States). Dept. of Materials Science and Engineering
  2. Pacific Northwest National Lab. (PNNL), Richland, WA (United States). Energy and Environment Directorate
  3. Pacific Northwest National Lab. (PNNL), Richland, WA (United States). Applied Materials and Performance
Publication Date:
Research Org.:
Pacific Northwest National Lab. (PNNL), Richland, WA (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1345532
Report Number(s):
PNNL-SA-118475
Journal ID: ISSN 1073-5623; PII: 4013
Grant/Contract Number:  
AC0576RL01830
Resource Type:
Accepted Manuscript
Journal Name:
Metallurgical and Materials Transactions. A, Physical Metallurgy and Materials Science
Additional Journal Information:
Journal Volume: 2017; Journal ID: ISSN 1073-5623
Publisher:
ASM International
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE

Citation Formats

Das, Shamiparna, Martinez, Nelson Y., Mishra, Rajiv S., Grant, Glenn J., and Jana, Saumyadeep. Control of Reaction Kinetics During Friction Stir Processing. United States: N. p., 2017. Web. doi:10.1007/s11661-017-4013-1.
Das, Shamiparna, Martinez, Nelson Y., Mishra, Rajiv S., Grant, Glenn J., & Jana, Saumyadeep. Control of Reaction Kinetics During Friction Stir Processing. United States. https://doi.org/10.1007/s11661-017-4013-1
Das, Shamiparna, Martinez, Nelson Y., Mishra, Rajiv S., Grant, Glenn J., and Jana, Saumyadeep. Fri . "Control of Reaction Kinetics During Friction Stir Processing". United States. https://doi.org/10.1007/s11661-017-4013-1. https://www.osti.gov/servlets/purl/1345532.
@article{osti_1345532,
title = {Control of Reaction Kinetics During Friction Stir Processing},
author = {Das, Shamiparna and Martinez, Nelson Y. and Mishra, Rajiv S. and Grant, Glenn J. and Jana, Saumyadeep},
abstractNote = {Friction stir processing (FSP) was used to successfully embed galfenol particles into aluminum (AA 1100 Al) matrix uniformly. But, intermetallic layer of Al3Fe was formed around the galfenol particles. We estimated the activation energy for Al3Fe formation during FSP, and attempts were made to minimize the Al3Fe layer thickness. By changing the processing conditions, FSP successfully eliminated the intermetallic layer. Therefore, FSP, in addition to microstructural control, can successfully fabricate intermetallic-free embedded regions by controlling the reaction kinetics.},
doi = {10.1007/s11661-017-4013-1},
journal = {Metallurgical and Materials Transactions. A, Physical Metallurgy and Materials Science},
number = ,
volume = 2017,
place = {United States},
year = {Fri Feb 17 00:00:00 EST 2017},
month = {Fri Feb 17 00:00:00 EST 2017}
}

Journal Article:
Free Publicly Available Full Text
Publisher's Version of Record

Citation Metrics:
Cited by: 1 work
Citation information provided by
Web of Science

Save / Share:

Works referenced in this record:

Friction stir processing: a novel technique for fabrication of surface composite
journal, January 2003


Texture and weak grain size dependence in friction stir processed Mg–Al–Zn alloy
journal, October 2006


Fatigue crack growth behavior of friction stir processed aluminum alloy
journal, August 2008


Effect of friction stir processing on the microstructure of cast A356 aluminum
journal, October 2006

  • Ma, Z. Y.; Sharma, S. R.; Mishra, R. S.
  • Materials Science and Engineering: A, Vol. 433, Issue 1-2
  • DOI: 10.1016/j.msea.2006.06.099

The effect of process parameters on microstructural characteristics of AZ91/SiO2 composite fabricated by FSP
journal, January 2013


Effect of texture on the mechanical behavior of ultrafine grained magnesium alloy
journal, March 2011


A novel technique for development of A356/Al2O3 surface nanocomposite by friction stir processing
journal, October 2011


Magnetic Properties of Friction Stir Processed Composite
journal, March 2016


Continuous dynamic recrystallization during friction stir welding of high strength aluminum alloys
journal, September 2000


MWCNTs/AZ31 surface composites fabricated by friction stir processing
journal, March 2006


High strain rate superplasticity in a commercial 2024 Al alloy via friction stir processing
journal, October 2003


Al–Al3Ti nanocomposites produced in situ by friction stir processing
journal, November 2006


Friction stir welding and processing
journal, August 2005


Microstructure and mechanical properties of Al–Fe in situ nanocomposite produced by friction stir processing
journal, September 2008


Fullerene/A5083 composites fabricated by material flow during friction stir processing
journal, October 2007


Prediction of phase formation sequence and phase stability in binary metal‐aluminum thin‐film systems using the effective heat of formation rule
journal, October 1991

  • Pretorius, R.; Vredenberg, A. M.; Saris, F. W.
  • Journal of Applied Physics, Vol. 70, Issue 7
  • DOI: 10.1063/1.349211

Phase sequence of silicide formation at metal-silicon interfaces
journal, January 1990


Effect of friction stir processing with SiC particles on microstructure and hardness of AZ31
journal, October 2006


High strain rate superplasticity in a friction stir processed 7075 Al alloy
journal, December 1999


Al–Ni intermetallic composites produced in situ by friction stir processing
journal, August 2010


Effect of welding speed on microstructural and mechanical properties of friction stir welded Inconel 600
journal, December 2009


Microstructures and mechanical properties of Al/Al2O3 surface nano-composite layer produced by friction stir processing
journal, January 2009

  • Shafiei-Zarghani, A.; Kashani-Bozorg, S. F.; Zarei-Hanzaki, A.
  • Materials Science and Engineering: A, Vol. 500, Issue 1-2
  • DOI: 10.1016/j.msea.2008.09.064