Effects of heat treatments on microstructure and properties of Ti-6Al-4V ELI alloy fabricated by electron beam melting (EBM)
Abstract
Electron beam melting (EBM) is a metal powder bed fusion additive manufacturing (AM) technology that is used to fabricate three-dimensional near-net-shaped parts directly from computer models. Ti-6Al-4V is the most widely used and studied alloy for this technology and is the focus of this work in its ELI (Extra Low Interstitial) variation. The mechanisms of microstructure formation, evolution, and its subsequent influence on mechanical properties of the alloy in as-fabricated condition have been documented by various researchers. In the present work, the thermal history resulting in the formation of the as-fabricated microstructure was analyzed and studied by a thermal simulation. Subsequently different heat treatments were performed based on three approaches in order to study the effects of heat treatments on the singular and exclusive microstructure formed during the EBM fabrication process. In the first approach, the effect of cooling rate after the solutionizing process was studied. In the second approach, the variation of α lath thickness during annealing treatment and correlation with mechanical properties was established. In the last approach, several solutionizing and aging experiments were conducted.
- Authors:
-
- Worcester Polytechnic Inst., Worcester, MA (United States). Integrative Materials Design Center
- Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Materials Science & Technology Division; Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Manufacturing Demonstration Facility
- Publication Date:
- Research Org.:
- Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States). Manufacturing Demonstration Facility (MDF)
- Sponsoring Org.:
- USDOE Office of Energy Efficiency and Renewable Energy (EERE), Energy Efficiency Office. Advanced Manufacturing Office
- OSTI Identifier:
- 1339366
- Alternate Identifier(s):
- OSTI ID: 1412564
- Grant/Contract Number:
- AC05-00OR22725
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Materials Science and Engineering. A, Structural Materials: Properties, Microstructure and Processing
- Additional Journal Information:
- Journal Volume: 685; Journal Issue: C; Journal ID: ISSN 0921-5093
- Publisher:
- Elsevier
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; Additive manufacturing; Electron beam melting; Ti-6Al-4V; Microstructure evolution; Mechanical characterization; Heat treatment
Citation Formats
Galarraga, Haize, Warren, Robert J., Lados, Diana A., Dehoff, Ryan R., Kirka, Michael M., and Nandwana, Peeyush. Effects of heat treatments on microstructure and properties of Ti-6Al-4V ELI alloy fabricated by electron beam melting (EBM). United States: N. p., 2017.
Web. doi:10.1016/j.msea.2017.01.019.
Galarraga, Haize, Warren, Robert J., Lados, Diana A., Dehoff, Ryan R., Kirka, Michael M., & Nandwana, Peeyush. Effects of heat treatments on microstructure and properties of Ti-6Al-4V ELI alloy fabricated by electron beam melting (EBM). United States. https://doi.org/10.1016/j.msea.2017.01.019
Galarraga, Haize, Warren, Robert J., Lados, Diana A., Dehoff, Ryan R., Kirka, Michael M., and Nandwana, Peeyush. Fri .
"Effects of heat treatments on microstructure and properties of Ti-6Al-4V ELI alloy fabricated by electron beam melting (EBM)". United States. https://doi.org/10.1016/j.msea.2017.01.019. https://www.osti.gov/servlets/purl/1339366.
@article{osti_1339366,
title = {Effects of heat treatments on microstructure and properties of Ti-6Al-4V ELI alloy fabricated by electron beam melting (EBM)},
author = {Galarraga, Haize and Warren, Robert J. and Lados, Diana A. and Dehoff, Ryan R. and Kirka, Michael M. and Nandwana, Peeyush},
abstractNote = {Electron beam melting (EBM) is a metal powder bed fusion additive manufacturing (AM) technology that is used to fabricate three-dimensional near-net-shaped parts directly from computer models. Ti-6Al-4V is the most widely used and studied alloy for this technology and is the focus of this work in its ELI (Extra Low Interstitial) variation. The mechanisms of microstructure formation, evolution, and its subsequent influence on mechanical properties of the alloy in as-fabricated condition have been documented by various researchers. In the present work, the thermal history resulting in the formation of the as-fabricated microstructure was analyzed and studied by a thermal simulation. Subsequently different heat treatments were performed based on three approaches in order to study the effects of heat treatments on the singular and exclusive microstructure formed during the EBM fabrication process. In the first approach, the effect of cooling rate after the solutionizing process was studied. In the second approach, the variation of α lath thickness during annealing treatment and correlation with mechanical properties was established. In the last approach, several solutionizing and aging experiments were conducted.},
doi = {10.1016/j.msea.2017.01.019},
journal = {Materials Science and Engineering. A, Structural Materials: Properties, Microstructure and Processing},
number = C,
volume = 685,
place = {United States},
year = {Fri Jan 06 00:00:00 EST 2017},
month = {Fri Jan 06 00:00:00 EST 2017}
}
Web of Science
Works referenced in this record:
Additive Manufacturing: Making Imagination the Major Limitation
journal, March 2014
- Zhai, Yuwei; Lados, Diana A.; LaGoy, Jane L.
- JOM, Vol. 66, Issue 5
An Overview of Densification, Microstructure and Mechanical Property of Additively Manufactured Ti-6Al-4V — Comparison among Selective Laser Melting, Electron Beam Melting, Laser Metal Deposition and Selective Laser Sintering, and with Conventional Powder
book, April 2015
- Yan, Ming; Yu, Peng
- Sintering Techniques of Materials
Electron Beam Additive Manufacturing of Titanium Components: Properties and Performance
journal, November 2013
- Edwards, P.; O'Conner, A.; Ramulu, M.
- Journal of Manufacturing Science and Engineering, Vol. 135, Issue 6
Microstructure and mechanical properties of Ti‐6Al‐4V produced by electron beam melting of pre‐alloyed powders
journal, May 2009
- Facchini, Luca; Magalini, Emanuele; Robotti, Pierfrancesco
- Rapid Prototyping Journal, Vol. 15, Issue 3
Effects of processing on microstructure and mechanical properties of a titanium alloy (Ti–6Al–4V) fabricated using electron beam melting (EBM), Part 2: Energy input, orientation, and location
journal, June 2013
- Hrabe, Nikolas; Quinn, Timothy
- Materials Science and Engineering: A, Vol. 573
Effects of processing on microstructure and mechanical properties of a titanium alloy (Ti–6Al–4V) fabricated using electron beam melting (EBM), part 1: Distance from build plate and part size
journal, June 2013
- Hrabe, Nikolas; Quinn, Timothy
- Materials Science and Engineering: A, Vol. 573
Microstructures and mechanical properties of electron beam-rapid manufactured Ti–6Al–4V biomedical prototypes compared to wrought Ti–6Al–4V
journal, February 2009
- Murr, L. E.; Esquivel, E. V.; Quinones, S. A.
- Materials Characterization, Vol. 60, Issue 2
Microstructures and Mechanical Properties of Ti6Al4V Parts Fabricated by Selective Laser Melting and Electron Beam Melting
journal, August 2013
- Rafi, H. K.; Karthik, N. V.; Gong, Haijun
- Journal of Materials Engineering and Performance, Vol. 22, Issue 12
Measurement of the interlamellar spacing of pearlite
journal, February 1984
- Vander Voort, G. F.; Roósz, A.
- Metallography, Vol. 17, Issue 1
Evaluation of microstructural development in electron beam melted Ti-6Al-4V
journal, March 2012
- Safdar, A.; Wei, L. -Y.; Snis, A.
- Materials Characterization, Vol. 65
On Process Temperature in Powder-Bed Electron Beam Additive Manufacturing: Model Development and Validation
journal, October 2014
- Cheng, Bo; Price, Steven; Lydon, James
- Journal of Manufacturing Science and Engineering, Vol. 136, Issue 6
Temperature Measurements in Powder-Bed Electron Beam Additive Manufacturing
conference, March 2015
- Price, Steven; Lydon, James; Cooper, Ken
- ASME 2014 International Mechanical Engineering Congress and Exposition, Volume 2A: Advanced Manufacturing
The Origin of Microstructural Diversity, Texture, and Mechanical Properties in Electron Beam Melted Ti-6Al-4V
journal, August 2010
- Al-Bermani, S. S.; Blackmore, M. L.; Zhang, W.
- Metallurgical and Materials Transactions A, Vol. 41, Issue 13
Thermal Modeling of Electron Beam Additive Manufacturing Process: Powder Sintering Effects
conference, July 2013
- Shen, Ninggang; Chou, Kevin
- ASME 2012 International Manufacturing Science and Engineering Conference collocated with the 40th North American Manufacturing Research Conference and in participation with the International Conference on Tribology Materials and Processing
Geometric consideration of support structures in part overhang fabrications by electron beam additive manufacturing
journal, December 2015
- Cheng, Bo; Chou, Kevin
- Computer-Aided Design, Vol. 69
Heat treatment of Ti6Al4V produced by Selective Laser Melting: Microstructure and mechanical properties
journal, November 2012
- Vrancken, Bey; Thijs, Lore; Kruth, Jean-Pierre
- Journal of Alloys and Compounds, Vol. 541
Microstructural modification of Ti–6Al–4V by using an in-situ printed heat sink in Electron Beam Melting® (EBM)
journal, December 2015
- Jamshidinia, M.; Atabaki, M. Mazar; Zahiri, M.
- Journal of Materials Processing Technology, Vol. 226
Works referencing / citing this record:
Identification of Mechanical Properties for Titanium Alloy Ti-6Al-4V Produced Using LENS Technology
journal, March 2019
- Szafrańska, Aleksandra; Antolak-Dudka, Anna; Baranowski, Paweł
- Materials, Vol. 12, Issue 6
Influence of Thermal Treatment on the Microstructure, Mechanical Properties, and Corrosion Resistance of Newly Developed Ti20Nb13Zr Biomedical Alloy in a Simulated Body Environment
journal, February 2019
- Hussein, M. A.; Azeem, M.; Kumar, A. Madhan
- Journal of Materials Engineering and Performance, Vol. 28, Issue 3
Static and Dynamic Loading Behavior of Ti6Al4V Honeycomb Structures Manufactured by Laser Engineered Net Shaping (LENSTM) Technology
journal, April 2019
- Antolak-Dudka, Anna; Płatek, Paweł; Durejko, Tomasz
- Materials, Vol. 12, Issue 8
Effect of heat treatments on microstructure/small-scale properties of additive manufactured Ti-6Al-4V
journal, May 2019
- Muhammad, Muztahid; Pegues, Jonathan W.; Shamsaei, Nima
- The International Journal of Advanced Manufacturing Technology, Vol. 103, Issue 9-12
Microstructure and Mechanical Performance of Ti–6Al–4V Lattice Structures Manufactured via Electron Beam Melting (EBM): A Review
journal, January 2020
- Del Guercio, Giuseppe; Galati, Manuela; Saboori, Abdollah
- Acta Metallurgica Sinica (English Letters), Vol. 33, Issue 2
Thermal Modeling of Temperature Distribution in Metal Additive Manufacturing Considering Effects of Build Layers, Latent Heat, and Temperature-Sensitivity of Material Properties
journal, September 2018
- Mirkoohi, Elham; Ning, Jinqiang; Bocchini, Peter
- Journal of Manufacturing and Materials Processing, Vol. 2, Issue 3
Selective laser melting of Ti alloys and hydroxyapatite for tissue engineering: progress and challenges
journal, May 2019
- Jaber, Hassanen; Kovacs, Tunde
- Materials Research Express, Vol. 6, Issue 8
Effect of Martensitic Transformation on Elastic Modulus Anisotropy of Ti-6Al-4V Alloy
journal, January 2018
- Feng, Zhongxue; Yang, Yingxiang; Xu, Zhichao
- Materials Research, Vol. 21, Issue 4
Post-processing to Modify the α Phase Micro-Texture and β Phase Grain Morphology in Ti-6Al-4V Fabricated by Powder Bed Electron Beam Melting
journal, May 2019
- Nandwana, Peeyush; Lee, Yousub; Ranger, Chasen
- Metallurgical and Materials Transactions A, Vol. 50, Issue 7
Hollow cathode plasma nitriding of medical grade Ti6Al4V: A comprehensive study
journal, June 2020
- Fontoura, Cristian Padilha; Rodrigues, Melissa Machado; Garcia, Charlene Silvestrin Celi
- Journal of Biomaterials Applications
Additive Manufacturing of Titanium Alloys by Electron Beam Melting: A Review
journal, December 2017
- Zhang, Lai-Chang; Liu, Yujing; Li, Shujun
- Advanced Engineering Materials, Vol. 20, Issue 5
Metal Alloys for Fusion-Based Additive Manufacturing
journal, February 2018
- Zhang, Duyao; Sun, Shoujin; Qiu, Dong
- Advanced Engineering Materials, Vol. 20, Issue 5
Laser Metal Deposition of Ti6Al4V—A Brief Review
journal, January 2020
- Zhong, Chongliang; Liu, Jianing; Zhao, Tong
- Applied Sciences, Vol. 10, Issue 3
Effect of Gradient Energy Density on the Microstructure and Mechanical Properties of Ti6Al4V Fabricated by Selective Electron Beam Additive Manufacture
journal, March 2020
- Hsu, Ta-I; Jhong, Yu-Ting; Tsai, Meng-Hsiu
- Materials, Vol. 13, Issue 7
Manufacturing of Titanium Components with 3DPMD
journal, May 2019
- Hoefer, Kevin; Nitsche, Alexander; Haelsig, André
- Metals, Vol. 9, Issue 5
Residual Lattice Strain and Phase Distribution in Ti-6Al-4V Produced by Electron Beam Melting
journal, February 2019
- Maimaitiyili, Tuerdi; Woracek, Robin; Neikter, Magnus
- Materials, Vol. 12, Issue 4
The Hardness of Additively Manufactured Alloys
journal, October 2018
- Zuback, J. S.; DebRoy, T.
- Materials, Vol. 11, Issue 11
Laser Metal Deposition of Ti6Al4V : A Brief Review
text, January 2020
- Zhong, Chongliang; Liu, Jianing; Zhao, Tong
- RWTH Aachen University
The Hardness of Additively Manufactured Alloys
journal, October 2018
- Zuback, J. S.; DebRoy, T.
- Materials, Vol. 11, Issue 11
Identification of Mechanical Properties for Titanium Alloy Ti-6Al-4V Produced Using LENS Technology
journal, March 2019
- Szafrańska, Aleksandra; Antolak-Dudka, Anna; Baranowski, Paweł
- Materials, Vol. 12, Issue 6
Static and Dynamic Loading Behavior of Ti6Al4V Honeycomb Structures Manufactured by Laser Engineered Net Shaping (LENSTM) Technology
journal, April 2019
- Antolak-Dudka, Anna; Płatek, Paweł; Durejko, Tomasz
- Materials, Vol. 12, Issue 8