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Title: Real-time imaging and local elemental analysis of nanostructures in liquids

A new design of in situ liquid cells is demonstrated, providing the first nanometer resolution elemental mapping of nanostructures in solution. Here, the technique has been applied to investigate dynamic liquid-phase synthesis of core–shell nanostructures and to simultaneously image the compositional distribution for multiple elements within the resulting materials.
Authors:
 [1] ;  [1] ;  [1] ;  [1] ;  [2] ;  [1] ;  [3]
  1. Univ. of Manchester, Manchester (United Kingdom)
  2. BP Corp. Research Center, Naperville, IL (United States)
  3. Univ. of Manchester, Manchester (United Kingdom); Argonne National Lab. (ANL), Argonne, IL (United States)
Publication Date:
Grant/Contract Number:
AC02-06CH11357
Type:
Accepted Manuscript
Journal Name:
ChemComm
Additional Journal Information:
Journal Volume: 50; Journal Issue: 70; Journal ID: ISSN 1359-7345
Publisher:
Royal Society of Chemistry
Research Org:
Argonne National Lab. (ANL), Argonne, IL (United States)
Sponsoring Org:
USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22) Engineering and Physical Sciences Research Council (EPSRC); Department of Defense - Defense Threat Reduction Agency; USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22). Scientific User Facilities Division
Country of Publication:
United States
Language:
English
Subject:
77 NANOSCIENCE AND NANOTECHNOLOGY; 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
OSTI Identifier:
1338962

Lewis, Edward A., Haigh, Sarah J., Slater, Thomas J. A., He, Zheyang, Kulzick, Matthew A., Burke, M. Grace, and Zaluzec, Nestor J.. Real-time imaging and local elemental analysis of nanostructures in liquids. United States: N. p., Web. doi:10.1039/c4cc02743d.
Lewis, Edward A., Haigh, Sarah J., Slater, Thomas J. A., He, Zheyang, Kulzick, Matthew A., Burke, M. Grace, & Zaluzec, Nestor J.. Real-time imaging and local elemental analysis of nanostructures in liquids. United States. doi:10.1039/c4cc02743d.
Lewis, Edward A., Haigh, Sarah J., Slater, Thomas J. A., He, Zheyang, Kulzick, Matthew A., Burke, M. Grace, and Zaluzec, Nestor J.. 2014. "Real-time imaging and local elemental analysis of nanostructures in liquids". United States. doi:10.1039/c4cc02743d. https://www.osti.gov/servlets/purl/1338962.
@article{osti_1338962,
title = {Real-time imaging and local elemental analysis of nanostructures in liquids},
author = {Lewis, Edward A. and Haigh, Sarah J. and Slater, Thomas J. A. and He, Zheyang and Kulzick, Matthew A. and Burke, M. Grace and Zaluzec, Nestor J.},
abstractNote = {A new design of in situ liquid cells is demonstrated, providing the first nanometer resolution elemental mapping of nanostructures in solution. Here, the technique has been applied to investigate dynamic liquid-phase synthesis of core–shell nanostructures and to simultaneously image the compositional distribution for multiple elements within the resulting materials.},
doi = {10.1039/c4cc02743d},
journal = {ChemComm},
number = 70,
volume = 50,
place = {United States},
year = {2014},
month = {5}
}