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Title: Bulk combinatorial synthesis and high throughput characterization for rapid assessment of magnetic materials: Application of laser engineered net shaping (LENS)

A bulk combinatorial approach for synthesizing alloy libraries using laser engineered net shaping (LENS; i.e., 3D printing) was utilized to rapidly assess material systems for magnetic applications. The LENS system feeds powders in different ratios into a melt pool created by a laser to synthesize samples with bulk (millimeters) dimensions. By analyzing these libraries with autosampler differential scanning calorimeter/thermal gravimetric analysis and vibrating sample magnetometry, we are able to rapidly characterize the thermodynamic and magnetic properties of the libraries. Furthermore, the Fe-Co binary alloy was used as a model system and the results were compared with data in the literature.
Authors:
 [1] ;  [1] ;  [1] ;  [1] ;  [1]
  1. Ames Lab., Ames, IA (United States)
Publication Date:
Report Number(s):
IS-J-9056
Journal ID: ISSN 1047-4838; PII: 1918
Grant/Contract Number:
AC02-07CH11358
Type:
Accepted Manuscript
Journal Name:
JOM. Journal of the Minerals, Metals & Materials Society
Additional Journal Information:
Journal Volume: 68; Journal Issue: 7; Journal ID: ISSN 1047-4838
Publisher:
Springer
Research Org:
Ames Laboratory (AMES), Ames, IA (United States)
Sponsoring Org:
USDOE
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE
OSTI Identifier:
1337695

Geng, J., Nlebedim, I. C., Besser, M. F., Simsek, E., and Ott, R. T.. Bulk combinatorial synthesis and high throughput characterization for rapid assessment of magnetic materials: Application of laser engineered net shaping (LENS). United States: N. p., Web. doi:10.1007/s11837-016-1918-x.
Geng, J., Nlebedim, I. C., Besser, M. F., Simsek, E., & Ott, R. T.. Bulk combinatorial synthesis and high throughput characterization for rapid assessment of magnetic materials: Application of laser engineered net shaping (LENS). United States. doi:10.1007/s11837-016-1918-x.
Geng, J., Nlebedim, I. C., Besser, M. F., Simsek, E., and Ott, R. T.. 2016. "Bulk combinatorial synthesis and high throughput characterization for rapid assessment of magnetic materials: Application of laser engineered net shaping (LENS)". United States. doi:10.1007/s11837-016-1918-x. https://www.osti.gov/servlets/purl/1337695.
@article{osti_1337695,
title = {Bulk combinatorial synthesis and high throughput characterization for rapid assessment of magnetic materials: Application of laser engineered net shaping (LENS)},
author = {Geng, J. and Nlebedim, I. C. and Besser, M. F. and Simsek, E. and Ott, R. T.},
abstractNote = {A bulk combinatorial approach for synthesizing alloy libraries using laser engineered net shaping (LENS; i.e., 3D printing) was utilized to rapidly assess material systems for magnetic applications. The LENS system feeds powders in different ratios into a melt pool created by a laser to synthesize samples with bulk (millimeters) dimensions. By analyzing these libraries with autosampler differential scanning calorimeter/thermal gravimetric analysis and vibrating sample magnetometry, we are able to rapidly characterize the thermodynamic and magnetic properties of the libraries. Furthermore, the Fe-Co binary alloy was used as a model system and the results were compared with data in the literature.},
doi = {10.1007/s11837-016-1918-x},
journal = {JOM. Journal of the Minerals, Metals & Materials Society},
number = 7,
volume = 68,
place = {United States},
year = {2016},
month = {4}
}