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Title: Using stepped anvils to make even insulation layers in laser-heated diamond-anvil cell samples

Here, we describe a method to make even insulation layers for high-pressure laser-heated diamond-anvil cell samples using stepped anvils. Moreover, the method works for both single-sided and double-sided laser heating using solid or fluid insulation. The stepped anvils are used as matched pairs or paired with a flat culet anvil to make gasket insulation layers and not actually used at high pressures; thus, their longevity is ensured. We also compare the radial temperature gradients and Soret diffusion of iron between self-insulating samples and samples produced with stepped anvils and find that less pronounced Soret diffusion occurs in samples with even insulation layers produced by stepped anvils.
Authors:
 [1] ;  [1] ;  [1] ;  [2] ;  [2] ;  [1]
  1. Yale Univ., New Haven, CT (United States). Dept. of Geology and Geophysics
  2. Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)
Publication Date:
Report Number(s):
LLNL-JRNL-695619
Journal ID: ISSN 0034-6748; RSINAK
Grant/Contract Number:
AC52-07NA27344; AC02-98CH10886
Type:
Accepted Manuscript
Journal Name:
Review of Scientific Instruments
Additional Journal Information:
Journal Volume: 86; Journal Issue: 9; Journal ID: ISSN 0034-6748
Publisher:
American Institute of Physics (AIP)
Research Org:
Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)
Sponsoring Org:
USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22)
Country of Publication:
United States
Language:
English
Subject:
75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY
OSTI Identifier:
1336986

Du, Zhixue, Gu, Tingting, Dobrosavljevic, Vasilije, Weir, Samuel T., Falabella, Steve, and Lee, Kanani K. M.. Using stepped anvils to make even insulation layers in laser-heated diamond-anvil cell samples. United States: N. p., Web. doi:10.1063/1.4929667.
Du, Zhixue, Gu, Tingting, Dobrosavljevic, Vasilije, Weir, Samuel T., Falabella, Steve, & Lee, Kanani K. M.. Using stepped anvils to make even insulation layers in laser-heated diamond-anvil cell samples. United States. doi:10.1063/1.4929667.
Du, Zhixue, Gu, Tingting, Dobrosavljevic, Vasilije, Weir, Samuel T., Falabella, Steve, and Lee, Kanani K. M.. 2015. "Using stepped anvils to make even insulation layers in laser-heated diamond-anvil cell samples". United States. doi:10.1063/1.4929667. https://www.osti.gov/servlets/purl/1336986.
@article{osti_1336986,
title = {Using stepped anvils to make even insulation layers in laser-heated diamond-anvil cell samples},
author = {Du, Zhixue and Gu, Tingting and Dobrosavljevic, Vasilije and Weir, Samuel T. and Falabella, Steve and Lee, Kanani K. M.},
abstractNote = {Here, we describe a method to make even insulation layers for high-pressure laser-heated diamond-anvil cell samples using stepped anvils. Moreover, the method works for both single-sided and double-sided laser heating using solid or fluid insulation. The stepped anvils are used as matched pairs or paired with a flat culet anvil to make gasket insulation layers and not actually used at high pressures; thus, their longevity is ensured. We also compare the radial temperature gradients and Soret diffusion of iron between self-insulating samples and samples produced with stepped anvils and find that less pronounced Soret diffusion occurs in samples with even insulation layers produced by stepped anvils.},
doi = {10.1063/1.4929667},
journal = {Review of Scientific Instruments},
number = 9,
volume = 86,
place = {United States},
year = {2015},
month = {9}
}