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Title: Mechanical behavior of post-processed Inconel 718 manufactured through the electron beam melting process

Abstract

Here, the electron beam melting (EBM) process was used to fabricate Inconel 718. The microstructure and tensile properties were characterized in both the as-fabricated and post-processed state transverse (T-orientation) and longitudinal (L-orientation) to the build direction. Post-processing involved both a hot isostatic pressing (HIP) and solution treatment and aging (STA) to homogenize the microstructure. In the as-fabricated state, EBM Inconel 718 exhibits a spatially dependent microstructure that is a function of build height. Spanning the last few layers is a cored dendritic structure comprised of the products (carbides and Laves phase) predicted under equilibrium solidification conditions. With increasing distance from the build's top surface, the cored dendritic structure becomes increasingly homogeneous with complete dissolution of the secondary dendrite arms. Further, temporal phase kinetics are observed to lead to the dissolution of the strengthening γ"γ" and precipitation of networks of fine δ needles that span the grains. Microstructurally, post-processing resulted in dissolution of the δ networks and homogeneous precipitation of γ'"γ'" throughout the height of the build. In the as-fabricated state, the monotonic tensile behavior exhibits a height sensitivity within the T-orientation at both 20 and 650 °C. Along the L-orientation, the tensile behavior exhibits strength values comparable to the referencemore » wrought material in the fully heat-treated state. After post-processing, the yield strength, ultimate strength, and elongation at failure for the EBM Inconel 718 were observed to have beneficially increased compared to the as-fabricated material. Further, as a result of post-processing the spatial variance of the ultimate yield strength and elongation at failure within the transverse direction decreased by 4 and 3× respectively.« less

Authors:
 [1];  [2];  [1];  [1]
  1. Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
  2. Arcam AB, Molndal (Sweden)
Publication Date:
Research Org.:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States). Manufacturing Demonstration Facility (MDF)
Sponsoring Org.:
USDOE Office of Energy Efficiency and Renewable Energy (EERE)
OSTI Identifier:
1335303
Alternate Identifier(s):
OSTI ID: 1417102
Grant/Contract Number:  
AC05-00OR22725
Resource Type:
Accepted Manuscript
Journal Name:
Materials Science and Engineering. A, Structural Materials: Properties, Microstructure and Processing
Additional Journal Information:
Journal Volume: 680; Journal Issue: C; Journal ID: ISSN 0921-5093
Publisher:
Elsevier
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; Ni-base superalloy; electron beam melting; post-processing; hot isostatic pressing; additive manufacturing

Citation Formats

Kirka, Michael M., Medina, Frank, Dehoff, Ryan R., and Okello, Alfred O. Mechanical behavior of post-processed Inconel 718 manufactured through the electron beam melting process. United States: N. p., 2016. Web. doi:10.1016/j.msea.2016.10.069.
Kirka, Michael M., Medina, Frank, Dehoff, Ryan R., & Okello, Alfred O. Mechanical behavior of post-processed Inconel 718 manufactured through the electron beam melting process. United States. https://doi.org/10.1016/j.msea.2016.10.069
Kirka, Michael M., Medina, Frank, Dehoff, Ryan R., and Okello, Alfred O. Fri . "Mechanical behavior of post-processed Inconel 718 manufactured through the electron beam melting process". United States. https://doi.org/10.1016/j.msea.2016.10.069. https://www.osti.gov/servlets/purl/1335303.
@article{osti_1335303,
title = {Mechanical behavior of post-processed Inconel 718 manufactured through the electron beam melting process},
author = {Kirka, Michael M. and Medina, Frank and Dehoff, Ryan R. and Okello, Alfred O.},
abstractNote = {Here, the electron beam melting (EBM) process was used to fabricate Inconel 718. The microstructure and tensile properties were characterized in both the as-fabricated and post-processed state transverse (T-orientation) and longitudinal (L-orientation) to the build direction. Post-processing involved both a hot isostatic pressing (HIP) and solution treatment and aging (STA) to homogenize the microstructure. In the as-fabricated state, EBM Inconel 718 exhibits a spatially dependent microstructure that is a function of build height. Spanning the last few layers is a cored dendritic structure comprised of the products (carbides and Laves phase) predicted under equilibrium solidification conditions. With increasing distance from the build's top surface, the cored dendritic structure becomes increasingly homogeneous with complete dissolution of the secondary dendrite arms. Further, temporal phase kinetics are observed to lead to the dissolution of the strengthening γ"γ" and precipitation of networks of fine δ needles that span the grains. Microstructurally, post-processing resulted in dissolution of the δ networks and homogeneous precipitation of γ'"γ'" throughout the height of the build. In the as-fabricated state, the monotonic tensile behavior exhibits a height sensitivity within the T-orientation at both 20 and 650 °C. Along the L-orientation, the tensile behavior exhibits strength values comparable to the reference wrought material in the fully heat-treated state. After post-processing, the yield strength, ultimate strength, and elongation at failure for the EBM Inconel 718 were observed to have beneficially increased compared to the as-fabricated material. Further, as a result of post-processing the spatial variance of the ultimate yield strength and elongation at failure within the transverse direction decreased by 4 and 3× respectively.},
doi = {10.1016/j.msea.2016.10.069},
journal = {Materials Science and Engineering. A, Structural Materials: Properties, Microstructure and Processing},
number = C,
volume = 680,
place = {United States},
year = {Fri Oct 21 00:00:00 EDT 2016},
month = {Fri Oct 21 00:00:00 EDT 2016}
}

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Works referencing / citing this record:

Additive Manufacturing of Alloy 718 via Electron Beam Melting: Effect of Post-Treatment on the Microstructure and the Mechanical Properties
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Can Appropriate Thermal Post-Treatment Make Defect Content in as-Built Electron Beam Additively Manufactured Alloy 718 Irrelevant?
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Damage Tolerance Evaluation of E-PBF-Manufactured Inconel 718 Strut Geometries by Advanced Characterization Techniques
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Influence of build layout and orientation on microstructural characteristics of electron beam melted Alloy 718
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