Variation of transition temperatures and residual resistivity ratio in vapor-grown FeSe

Böhmer, A. E.; Taufour, V.; Straszheim, W. E.; Wolf, T.; Canfield, P. C.

doi:10.1103/PhysRevB.94.024526

Title: Variation of transition temperatures and residual resistivity ratio in vapor-grown FeSe

Abstract

The study of the iron-based superconductor FeSe has blossomed with the availability of high-quality single crystals, obtained through flux/vapor-transport growth techniques below the structural transformation temperature of its tetragonal phase, T≈450°C. Here, we report on the variation of sample morphology and properties due to small modifications in the growth conditions. A considerable variation of the superconducting transition temperature T_c, from 8.8 K to 3 K, which cannot be correlated with the sample composition, is observed. Instead, we point out a clear correlation between T_c and disorder, as measured by the residual resistivity ratio. Notably, the tetragonal-to-orthorhombic structural transition is also found to be quite strongly disorder dependent (T_s≈72–90K) and linearly correlated with T_c.

Authors:

Böhmer, A. E. ^[1]; Taufour, V. ^[1]; Straszheim, W. E. ^[1]; Wolf, T. ^[2]; Canfield, P. C. ^[3]

Ames Lab. and Iowa State Univ., Ames, IA (United States)
Karlsruhe Inst. of Technology (KIT) (Germany). Inst. of Solid State Physics
Ames Lab. and Iowa State Univ., Ames, IA (United States); Iowa State Univ., Ames, IA (United States). Dept. of Physics and Astronomy

Publication Date:: 2016-07-29

Research Org.:: Ames Lab., Ames, IA (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1326844

Alternate Identifier(s):: OSTI ID: 1275981

Report Number(s):: IS-J-9077
Journal ID: ISSN 2469-9950; PRBMDO

Grant/Contract Number:: AC02-07CH11358

Resource Type:: Accepted Manuscript

Journal Name:: Physical Review B

Additional Journal Information:: Journal Volume: 94; Journal Issue: 2; Journal ID: ISSN 2469-9950

Publisher:: American Physical Society (APS)

Country of Publication:: United States

Language:: English

Subject:: 75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY

Citation Formats


                    Böhmer, A. E., Taufour, V., Straszheim, W. E., Wolf, T., and Canfield, P. C. Variation of transition temperatures and residual resistivity ratio in vapor-grown FeSe.  United States: N. p., 2016. 
Web.  doi:10.1103/PhysRevB.94.024526.

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                    Böhmer, A. E., Taufour, V., Straszheim, W. E., Wolf, T., & Canfield, P. C. Variation of transition temperatures and residual resistivity ratio in vapor-grown FeSe.  United States.  https://doi.org/10.1103/PhysRevB.94.024526

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                    Böhmer, A. E., Taufour, V., Straszheim, W. E., Wolf, T., and Canfield, P. C. Fri .  
"Variation of transition temperatures and residual resistivity ratio in vapor-grown FeSe".  United States.  https://doi.org/10.1103/PhysRevB.94.024526.  https://www.osti.gov/servlets/purl/1326844.

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@article{osti_1326844,

  title        = {Variation of transition temperatures and residual resistivity ratio in vapor-grown FeSe},

  author       = {Böhmer, A. E. and Taufour, V. and Straszheim, W. E. and Wolf, T. and Canfield, P. C.},

  abstractNote = {The study of the iron-based superconductor FeSe has blossomed with the availability of high-quality single crystals, obtained through flux/vapor-transport growth techniques below the structural transformation temperature of its tetragonal phase, T≈450°C. Here, we report on the variation of sample morphology and properties due to small modifications in the growth conditions. A considerable variation of the superconducting transition temperature Tc, from 8.8 K to 3 K, which cannot be correlated with the sample composition, is observed. Instead, we point out a clear correlation between Tc and disorder, as measured by the residual resistivity ratio. Notably, the tetragonal-to-orthorhombic structural transition is also found to be quite strongly disorder dependent (Ts≈72–90K) and linearly correlated with Tc.},

  doi          = {10.1103/PhysRevB.94.024526},

  journal      = {Physical Review B},

  number       = 2,

  volume       = 94,

  place        = {United States},

  year         = {2016},

  month        = {7}

}

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Works referencing / citing this record:

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Title: Variation of transition temperatures and residual resistivity ratio in vapor-grown FeSe

Abstract

Citation Formats

Field-induced superconducting phase of FeSe in the BCS-BEC cross-over journal, November 2014

Extreme sensitivity of superconductivity to stoichiometry in Fe 1 + δ Se journal, January 2009

Resistivity and magnetoresistance of FeSe single crystals under helium-gas pressure journal, May 2015

Crystal growth and superconductivity of FeSe x journal, November 2008

Manifestations of multiple-carrier charge transport in the magnetostructurally ordered phase of BaFe 2 As 2 journal, November 2011

The fese (ironselenium) system journal, June 1991

Superconductivity in the PbO-type structure -FeSe journal, September 2008

Single crystal growth and characterization of tetragonal FeSe1−x superconductors journal, January 2013

Aluminiumchlorid als Transportmittel zum chemischen Transport von Übergangsmetallchalkogeniden journal, July 1974

Structural and physical properties of FeSe crystals fabricated by the chemical vapor transport method journal, December 2010

Substitution Effects on FeSe Superconductor journal, July 2009

Growth and superconductivity of FeSex crystals journal, February 2009

Nonmonotonic pressure evolution of the upper critical field in superconducting FeSe journal, February 2016

Pressure Induced Static Magnetic Order in Superconducting FeSe 1 − x journal, February 2010

The Superstructures of Iron Selenide Fe 7 Se 8 journal, June 1961

Electronic and magnetic phase diagram of β-Fe1.01Se with superconductivity at 36.7 K under pressure journal, June 2009

Lack of coupling between superconductivity and orthorhombic distortion in stoichiometric single-crystalline FeSe journal, May 2013

Tetragonal-to-Orthorhombic Structural Phase Transition at 90 K in the Superconductor Fe 1.01 Se journal, July 2009

Superconductivity at 27K in tetragonal FeSe under high pressure journal, October 2008

Crystal structure of the new FeSe1−x superconductor journal, January 2008

Dome-shaped magnetic order competing with high-temperature superconductivity at high pressures in FeSe journal, July 2016

Unusual band renormalization in the simplest iron-based superconductor FeSe 1 − x journal, June 2014

Synthesis, crystal structure, and chemical stability of the superconductor FeSe 1 − x journal, July 2009

Coexistence of superconductivity and magnetism in FeSe 1 − x under pressure journal, February 2012

Enhanced Superconductivity on the Tetragonal Lattice in FeSe under Hydrostatic Pressure journal, January 2014

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In‐situ Electrochemical X‐ray Diffraction: A Rigorous Method to Navigate within Phase Diagrams Reveals β‐Fe 1+ x Se as Superconductor for All x journal, October 2019

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Unusual effects of Be doping in the iron-based superconductor FeSe journal, October 2018

New materials physics journal, November 2019

Anisotropic grain-boundary effect on electronic transport in superconducting FeSe thin films journal, January 2019

Majority carrier type inversion in the FeSe family and a ‘doped semimetal’ scheme in iron-based superconductors journal, May 2019

Imaging anisotropic vortex dynamics in FeSe journal, July 2019

Robustness of superconducting properties to transition metal substitution and impurity phases in Fe 1 − x V x Se journal, September 2019

Lattice dynamics in FeSe via inelastic x-ray scattering and first-principles calculations journal, January 2020

Origin of the Resistivity Anisotropy in the Nematic Phase of FeSe journal, September 2016

Nematic Energy Scale and the Missing Electron Pocket in FeSe journal, December 2019

Discovery of orbital-selective Cooper pairing in FeSe journal, July 2017

Dome of magnetic order inside the nematic phase of sulfur-substituted FeSe under pressure text, January 2017

Suppression of electronic correlations by chemical pressure from FeSe to FeS text, January 2017

Flux growth in a horizontal configuration: an analogue to vapor transport growth text, January 2017

NMR evidence for static local nematicity and its cooperative interplay with low-energy magnetic fluctuations in FeSe under pressure text, January 2017

Majority carrier type inversion in FeSe family and "doped semimetal" scheme in iron-based superconductors text, January 2018

Unusual Effects of Be doping in the Iron Based Superconductor FeSe text, January 2018

Field-induced superconducting phase of FeSe in the BCS-BEC cross-over
journal, November 2014

Extreme sensitivity of superconductivity to stoichiometry in ${Fe}_{1 + δ} Se$
journal, January 2009

Resistivity and magnetoresistance of FeSe single crystals under helium-gas pressure
journal, May 2015

Crystal growth and superconductivity of FeSe _x
journal, November 2008

Manifestations of multiple-carrier charge transport in the magnetostructurally ordered phase of BaFe $_{2}$ As $_{2}$
journal, November 2011

The fese (ironselenium) system
journal, June 1991

Superconductivity in the PbO-type structure -FeSe
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Single crystal growth and characterization of tetragonal FeSe1−x superconductors
journal, January 2013

Aluminiumchlorid als Transportmittel zum chemischen Transport von Übergangsmetallchalkogeniden
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Structural and physical properties of FeSe crystals fabricated by the chemical vapor transport method
journal, December 2010

Substitution Effects on FeSe Superconductor
journal, July 2009

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Nonmonotonic pressure evolution of the upper critical field in superconducting FeSe
journal, February 2016

Pressure Induced Static Magnetic Order in Superconducting ${FeSe}_{1 - x}$
journal, February 2010

The Superstructures of Iron Selenide Fe ₇ Se ₈
journal, June 1961

Electronic and magnetic phase diagram of β-Fe1.01Se with superconductivity at 36.7 K under pressure
journal, June 2009

Lack of coupling between superconductivity and orthorhombic distortion in stoichiometric single-crystalline FeSe
journal, May 2013

Tetragonal-to-Orthorhombic Structural Phase Transition at 90 K in the Superconductor ${Fe}_{1.01} Se$
journal, July 2009

Superconductivity at 27K in tetragonal FeSe under high pressure
journal, October 2008

Crystal structure of the new FeSe1−x superconductor
journal, January 2008

Dome-shaped magnetic order competing with high-temperature superconductivity at high pressures in FeSe
journal, July 2016

Unusual band renormalization in the simplest iron-based superconductor ${FeSe}_{1 - x}$
journal, June 2014

Synthesis, crystal structure, and chemical stability of the superconductor ${FeSe}_{1 - x}$
journal, July 2009

Coexistence of superconductivity and magnetism in FeSe $_{1 - x}$ under pressure
journal, February 2012

Enhanced Superconductivity on the Tetragonal Lattice in FeSe under Hydrostatic Pressure
journal, January 2014

Superconducting and normal phases of FeSe single crystals at high pressure
journal, May 2009

Synthesis, crystal structure, and magnetism of $β$ -Fe $_{1.00 (2)}$ Se $_{1.00 (3)}$ single crystals
journal, June 2011

Elektrochemische In‐situ‐Röntgenbeugung: Eine präzise Methode zur Navigation in Phasendiagrammen enthüllt β‐Fe _{1+ x} Se als Supraleiter für alle x
journal, September 2019

In‐situ Electrochemical X‐ray Diffraction: A Rigorous Method to Navigate within Phase Diagrams Reveals β‐Fe _{1+ x} Se as Superconductor for All x
journal, October 2019

Strong cooperative coupling of pressure-induced magnetic order and nematicity in FeSe
journal, September 2016

Quenched nematic criticality and two superconducting domes in an iron-based superconductor
journal, October 2019

Nematicity, magnetism and superconductivity in FeSe
journal, December 2017

Unusual effects of Be doping in the iron-based superconductor FeSe
journal, October 2018

New materials physics
journal, November 2019

Anisotropic grain-boundary effect on electronic transport in superconducting FeSe thin films
journal, January 2019

Majority carrier type inversion in the FeSe family and a ‘doped semimetal’ scheme in iron-based superconductors
journal, May 2019

Imaging anisotropic vortex dynamics in FeSe
journal, July 2019

Robustness of superconducting properties to transition metal substitution and impurity phases in ${Fe}_{1 - x} V_{x} Se$
journal, September 2019

Lattice dynamics in FeSe via inelastic x-ray scattering and first-principles calculations
journal, January 2020

Origin of the Resistivity Anisotropy in the Nematic Phase of FeSe
journal, September 2016

Nematic Energy Scale and the Missing Electron Pocket in FeSe
journal, December 2019

Discovery of orbital-selective Cooper pairing in FeSe
journal, July 2017

Dome of magnetic order inside the nematic phase of sulfur-substituted FeSe under pressure
text, January 2017

Suppression of electronic correlations by chemical pressure from FeSe to FeS
text, January 2017

Flux growth in a horizontal configuration: an analogue to vapor transport growth
text, January 2017

NMR evidence for static local nematicity and its cooperative interplay with low-energy magnetic fluctuations in FeSe under pressure
text, January 2017

Majority carrier type inversion in FeSe family and "doped semimetal" scheme in iron-based superconductors
text, January 2018

Unusual Effects of Be doping in the Iron Based Superconductor FeSe
text, January 2018