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Title: Submillisecond X-ray photon correlation spectroscopy from a pixel array detector with fast dual gating and no readout dead-time

Abstract

Small-angle scattering X-ray photon correlation spectroscopy (XPCS) studies were performed using a novel photon-counting pixel array detector with dual counters for each pixel. Each counter can be read out independently from the other to ensure there is no readout dead-time between the neighboring frames. A maximum frame rate of 11.8 kHz was achieved. Results on test samples show good agreement with simple diffusion. Lastly, the potential of extending the time resolution of XPCS beyond the limit set by the detector frame rate using dual counters is also discussed.

Authors:
 [1];  [1];  [2];  [2];  [2];  [1];  [3];  [2];  [1]
  1. Argonne National Lab. (ANL), Lemont, IL (United States)
  2. AGH Univ. of Science and Technology, Krakow (Poland)
  3. Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States)
Publication Date:
Research Org.:
Argonne National Lab. (ANL), Argonne, IL (United States); Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States)
Sponsoring Org.:
USDOE Office of Science (SC), High Energy Physics (HEP) (SC-25)
OSTI Identifier:
1326216
Alternate Identifier(s):
OSTI ID: 1333142
Report Number(s):
FERMILAB-PUB-16-530-PPD
Journal ID: ISSN 1600-5775; JSYRES; 128033
Grant/Contract Number:  
AC02-06CH11357; AC02-07CH11359
Resource Type:
Accepted Manuscript
Journal Name:
Journal of Synchrotron Radiation (Online)
Additional Journal Information:
Journal Name: Journal of Synchrotron Radiation (Online); Journal Volume: 23; Journal Issue: 3; Journal ID: ISSN 1600-5775
Publisher:
International Union of Crystallography
Country of Publication:
United States
Language:
English
Subject:
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY; pixel array detector (PAD); high frame rate; small angle x-ray scattering (SAXS); two counters; x-ray photon correlation spectroscopy (XPCS); 43 PARTICLE ACCELERATORS; photon counting; X-ray photon correlation spectroscopy (XPCS); small-angle X-ray scattering (SAXS)

Citation Formats

Zhang, Qingteng, Dufresne, Eric M., Grybos, Pawel, Kmon, Piotr, Maj, Piotr, Narayanan, Suresh, Deptuch, Grzegorz W., Szczygiel, Robert, and Sandy, Alec. Submillisecond X-ray photon correlation spectroscopy from a pixel array detector with fast dual gating and no readout dead-time. United States: N. p., 2016. Web. doi:10.1107/S1600577516005166.
Zhang, Qingteng, Dufresne, Eric M., Grybos, Pawel, Kmon, Piotr, Maj, Piotr, Narayanan, Suresh, Deptuch, Grzegorz W., Szczygiel, Robert, & Sandy, Alec. Submillisecond X-ray photon correlation spectroscopy from a pixel array detector with fast dual gating and no readout dead-time. United States. doi:10.1107/S1600577516005166.
Zhang, Qingteng, Dufresne, Eric M., Grybos, Pawel, Kmon, Piotr, Maj, Piotr, Narayanan, Suresh, Deptuch, Grzegorz W., Szczygiel, Robert, and Sandy, Alec. Tue . "Submillisecond X-ray photon correlation spectroscopy from a pixel array detector with fast dual gating and no readout dead-time". United States. doi:10.1107/S1600577516005166. https://www.osti.gov/servlets/purl/1326216.
@article{osti_1326216,
title = {Submillisecond X-ray photon correlation spectroscopy from a pixel array detector with fast dual gating and no readout dead-time},
author = {Zhang, Qingteng and Dufresne, Eric M. and Grybos, Pawel and Kmon, Piotr and Maj, Piotr and Narayanan, Suresh and Deptuch, Grzegorz W. and Szczygiel, Robert and Sandy, Alec},
abstractNote = {Small-angle scattering X-ray photon correlation spectroscopy (XPCS) studies were performed using a novel photon-counting pixel array detector with dual counters for each pixel. Each counter can be read out independently from the other to ensure there is no readout dead-time between the neighboring frames. A maximum frame rate of 11.8 kHz was achieved. Results on test samples show good agreement with simple diffusion. Lastly, the potential of extending the time resolution of XPCS beyond the limit set by the detector frame rate using dual counters is also discussed.},
doi = {10.1107/S1600577516005166},
journal = {Journal of Synchrotron Radiation (Online)},
number = 3,
volume = 23,
place = {United States},
year = {2016},
month = {4}
}

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