Depth resolved domain mapping in tetragonal SrTiO3 by micro-Laue diffraction
Abstract
Here, we present depth resolved X-ray micro-Laue diffraction experiments on the low temperature domain structure of SrTiO3. At 80 K, monochromatic X-ray diffraction shows an elongated out-of-plane unit cell axis within a matrix of in-plane oriented tetragonal unit cells. Full deviatoric strain mappings from white beam diffraction show a dominance of two tetragonal domain orientations (x- and z-axes) over a large area of sample surface. This information sets an upper bound on domain wall widths and offers a method for studying 3D domain structure at low temperatures.
- Authors:
-
- Stanford Univ., Stanford, CA (United States)
- Stanford Univ., Stanford, CA (United States); SLAC National Accelerator Lab., Menlo Park, CA (United States)
- Argonne National Lab. (ANL), Argonne, IL (United States)
- Publication Date:
- Research Org.:
- SLAC National Accelerator Lab., Menlo Park, CA (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC)
- OSTI Identifier:
- 1253090
- Alternate Identifier(s):
- OSTI ID: 1250391
- Report Number(s):
- SLAC-PUB-16523
Journal ID: ISSN 0003-6951
- Grant/Contract Number:
- AC02-76SF00515; AC02-06CH11357
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Applied Physics Letters
- Additional Journal Information:
- Journal Volume: 108; Journal Issue: 18; Journal ID: ISSN 0003-6951
- Publisher:
- American Institute of Physics (AIP)
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 43 PARTICLE ACCELERATORS; PHYS; SrTiO3; tetragonal; strain; micro-Laue diffraction
Citation Formats
Merz, T. A., Noad, H., Xu, R., Inoue, H., Liu, W., Hikita, Y., Vailionis, A., Moler, K. A., and Hwang, H. Y. Depth resolved domain mapping in tetragonal SrTiO3 by micro-Laue diffraction. United States: N. p., 2016.
Web. doi:10.1063/1.4948351.
Merz, T. A., Noad, H., Xu, R., Inoue, H., Liu, W., Hikita, Y., Vailionis, A., Moler, K. A., & Hwang, H. Y. Depth resolved domain mapping in tetragonal SrTiO3 by micro-Laue diffraction. United States. https://doi.org/10.1063/1.4948351
Merz, T. A., Noad, H., Xu, R., Inoue, H., Liu, W., Hikita, Y., Vailionis, A., Moler, K. A., and Hwang, H. Y. Mon .
"Depth resolved domain mapping in tetragonal SrTiO3 by micro-Laue diffraction". United States. https://doi.org/10.1063/1.4948351. https://www.osti.gov/servlets/purl/1253090.
@article{osti_1253090,
title = {Depth resolved domain mapping in tetragonal SrTiO3 by micro-Laue diffraction},
author = {Merz, T. A. and Noad, H. and Xu, R. and Inoue, H. and Liu, W. and Hikita, Y. and Vailionis, A. and Moler, K. A. and Hwang, H. Y.},
abstractNote = {Here, we present depth resolved X-ray micro-Laue diffraction experiments on the low temperature domain structure of SrTiO3. At 80 K, monochromatic X-ray diffraction shows an elongated out-of-plane unit cell axis within a matrix of in-plane oriented tetragonal unit cells. Full deviatoric strain mappings from white beam diffraction show a dominance of two tetragonal domain orientations (x- and z-axes) over a large area of sample surface. This information sets an upper bound on domain wall widths and offers a method for studying 3D domain structure at low temperatures.},
doi = {10.1063/1.4948351},
journal = {Applied Physics Letters},
number = 18,
volume = 108,
place = {United States},
year = {Mon May 02 00:00:00 EDT 2016},
month = {Mon May 02 00:00:00 EDT 2016}
}
Free Publicly Available Full Text
Publisher's Version of Record
Other availability
Cited by: 5 works
Citation information provided by
Web of Science
Web of Science
Save to My Library
You must Sign In or Create an Account in order to save documents to your library.
Works referenced in this record:
Local electrostatic imaging of striped domain order in LaAlO3/SrTiO3
journal, November 2013
- Honig, M.; Sulpizio, J. A.; Drori, J.
- Nature Materials, Vol. 12, Issue 12
Birefringence of SrTiO 3 at the ferroelastic phase transition
journal, May 2004
- Geday, M. A.; Glazer, A. M.
- Journal of Physics: Condensed Matter, Vol. 16, Issue 20
Locally enhanced conductivity due to the tetragonal domain structure in LaAlO3/SrTiO3 heterointerfaces
journal, September 2013
- Kalisky, Beena; Spanton, Eric M.; Noad, Hilary
- Nature Materials, Vol. 12, Issue 12
The lattice constant vs. temperature relation around the 105 K transition of a flux-grown SrTiO 3 crystal
journal, September 1985
- Sato, M.; Soejima, Y.; Ohama, N.
- Phase Transitions, Vol. 5, Issue 3
Domain formation in epitaxial Pb(Zr, Ti)O3 thin films
journal, October 2001
- Lee, K. S.; Choi, J. H.; Lee, J. Y.
- Journal of Applied Physics, Vol. 90, Issue 8
Atomistic structure of 90° domain walls in ferroelectric PbTiO 3 thin films
journal, March 1995
- Stemmer, S.; Streiffer, S. K.; Ernst, F.
- Philosophical Magazine A, Vol. 71, Issue 3
Optical Study of Tetragonal Domains in LaAlO3/SrTiO3
journal, August 2014
- Erlich, Z.; Frenkel, Y.; Drori, J.
- Journal of Superconductivity and Novel Magnetism, Vol. 28, Issue 3
Microstructure of Ferroelectric Domains in Observed via X-Ray Microdiffraction
journal, August 2005
- Holt, M.; Hassani, Kh.; Sutton, M.
- Physical Review Letters, Vol. 95, Issue 8
Polychromatic X-ray microdiffraction studies of mesoscale structure and dynamics
journal, February 2005
- Ice, G. E.; Larson, B. C.; Yang, W.
- Journal of Synchrotron Radiation, Vol. 12, Issue 2
Elektromechanische Eigenschaften von Strontiumtitanateinkristallen
journal, January 1963
- Schmidt, G.; Hegenbarth, E.
- physica status solidi (b), Vol. 3, Issue 2
Characteristic Structural Phase Transition in Perovskite-Type Compounds
journal, September 1968
- Müller, K. A.; Berlinger, W.; Waldner, F.
- Physical Review Letters, Vol. 21, Issue 12
Analysis of Stress and Temperature Dependence of Fluorescence in SrTi :
journal, December 1970
- Slonczewski, J. C.
- Physical Review B, Vol. 2, Issue 11
Ferroelectric Domain Walls in BaTiO 3 : Fingerprints in XRPD Diagrams and Quantitative HRTEM Image Analysis
journal, June 1997
- Floquet, N.; Valot, C. M.; Mesnier, M. T.
- Journal de Physique III, Vol. 7, Issue 6
Domain-wall orientations in ferroelastics
journal, December 1975
- Sapriel, J.
- Physical Review B, Vol. 12, Issue 11
Interface Physics in Complex Oxide Heterostructures
journal, March 2011
- Zubko, Pavlo; Gariglio, Stefano; Gabay, Marc
- Annual Review of Condensed Matter Physics, Vol. 2, Issue 1
Monodomain strontium titanate
journal, April 1970
- Müller, K. A.; Berlinger, W.; Capizzi, M.
- Solid State Communications, Vol. 8, Issue 7
Low temperature Laue topography of strontium titanate at SPring-8
journal, January 2003
- Ozaki, T.; Fujimoto, I.; Mizuno, K.
- Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Vol. 199
Birefringence of SrTi Produced by the 105°K Structural Phase Transition
journal, November 1972
- Courtens, Eric
- Physical Review Letters, Vol. 29, Issue 20
Dielectric Properties of Strontium Titanate at Low Temperature
journal, August 1970
- Saifi, M. A.; Cross, L. E.
- Physical Review B, Vol. 2, Issue 3
Dramatic mobility enhancements in doped SrTiO3 thin films by defect management
journal, July 2010
- Kozuka, Y.; Hikita, Y.; Bell, C.
- Applied Physics Letters, Vol. 97, Issue 1
Magnetoresistance of cubic and monodomain tetragonal -type strontium titanate
journal, July 1977
- Kuchar, F.; Frankus, P.
- Physical Review B, Vol. 16, Issue 2
Domain population in SrTiO 3 below the cubic-to-tetragonal phase transition
journal, September 1995
- Koga, T.; Lu, Z.; Munakata, K.
- Phase Transitions, Vol. 54, Issue 2
Emergent phenomena at oxide interfaces
journal, January 2012
- Hwang, H. Y.; Iwasa, Y.; Kawasaki, M.
- Nature Materials, Vol. 11, Issue 2
Lattice constant of strontium titanate at low temperatures
journal, May 1973
- Okazaki, A.; Kawaminami, M.
- Materials Research Bulletin, Vol. 8, Issue 5
Domain Wall Damping and Elastic Softening in : Evidence for Polar Twin Walls
journal, October 2012
- Scott, J. F.; Salje, E. K. H.; Carpenter, M. A.
- Physical Review Letters, Vol. 109, Issue 18
Domains within Domains and Walls within Walls: Evidence for Polar Domains in Cryogenic
journal, December 2013
- Salje, E. K. H.; Aktas, O.; Carpenter, M. A.
- Physical Review Letters, Vol. 111, Issue 24
The temperature dependence of the lattice constant of SrTiO 3 around the 105 K transition
journal, February 1984
- Ohama, N.; Sakashita, H.; Okazaki, A.
- Phase Transitions, Vol. 4, Issue 2
White microbeam X-ray spectro-scattering topography on the domain structure of strontium titanate
journal, August 2005
- Kajiwara, Kentaro; Ozaki, Tōru; Sakaue, Hiroaki
- Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Vol. 238, Issue 1-4
Ferroelectric quantum criticality
journal, March 2014
- Rowley, S. E.; Spalek, L. J.; Smith, R. P.
- Nature Physics, Vol. 10, Issue 5
Domain structure of SrTiO 3 under uniaxial stresses
journal, August 1972
- Chang, T. S.
- Journal of Applied Physics, Vol. 43, Issue 8
White beam X-ray topographic measurement of spontaneous strain in strontium titanate
journal, August 2005
- Ozaki, T.; Kusunose, K.; Sakaue, H.
- Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Vol. 238, Issue 1-4
Three-dimensional X-ray structural microscopy with submicrometre resolution
journal, February 2002
- Larson, B. C.; Yang, Wenge; Ice, G. E.
- Nature, Vol. 415, p. 887-890
Magnetic domain-wall width in thin films measured using Fresnel imaging
journal, October 2001
- Lloyd, S. J.; Mathur, N. D.; Loudon, J. C.
- Physical Review B, Vol. 64, Issue 17
SrTi : An intrinsic quantum paraelectric below 4 K
journal, April 1979
- Müller, K. A.; Burkard, H.
- Physical Review B, Vol. 19, Issue 7
Direct measurement of triaxial strain fields around ferroelectric domains using X-ray microdiffraction
journal, May 2003
- Rogan, Robert C.; Tamura, Nobumichi; Swift, Geoffrey A.
- Nature Materials, Vol. 2, Issue 6
Static Critical Exponents at Structural Phase Transitions
journal, January 1971
- Müller, K. A.; Berlinger, W.
- Physical Review Letters, Vol. 26, Issue 1
Landau-Ginzburg model of interphase boundaries in improper ferroelastic Perovskites of symmetry
journal, March 1990
- Cao, Wenwu; Barsch, Gerhard R.
- Physical Review B, Vol. 41, Issue 7
The structure and formation of nanotwins in BaTiO 3 thin films
journal, April 1998
- Jia, C. L.; Urban, K.; Mertin, M.
- Philosophical Magazine A, Vol. 77, Issue 4
The Race to X-ray Microbeam and Nanobeam Science
journal, December 2011
- Ice, G. E.; Budai, J. D.; Pang, J. W. L.
- Science, Vol. 334, Issue 6060
Separation of the and Phases near the Surface of
journal, January 1982
- Höchli, U. T.; Rohrer, H.
- Physical Review Letters, Vol. 48, Issue 3
Works referencing / citing this record:
Physics of SrTiO 3 -based heterostructures and nanostructures: a review
journal, February 2018
- Pai, Yun-Yi; Tylan-Tyler, Anthony; Irvin, Patrick
- Reports on Progress in Physics, Vol. 81, Issue 3
Physics of SrTiO$_3$-based heterostructures and nanostructures: a review
text, January 2017
- Pai, Yun-Yi; Tylan-Tyler, Anthony; Irvin, Patrick
- arXiv