Time-resolved x-ray diffraction and electrical resistance measurements of structural phase transitions in zirconium
Abstract
Here, we have designed a portable pressure controller module to tune compression rates and maximum pressures attainable in a standard gas-membrane diamond anvil cell (DAC). During preliminary experiments, performed on zirconium (Zr) metal sample, pressure jumps of up to 80 GPa were systematically obtained in less than 0.2s (resulting in compression rate of few GPa/s up to more than 400 GPa/s). In-situ x-ray diffraction and electrical resistance measurements were performed simultaneously during this rapid pressure increase to provide the first time resolved data on α → ω → β structural evolution in Zr at high pressures. Direct control of compression rates and peak pressures, which can be held for prolonged time, allows for investigation of structural evolution and kinetics of structural phase transitions of materials under previously unexplored compression rate-pressure conditions that bridge traditional static and shock/dynamic experimental platforms.
- Authors:
-
[1];
[1];
[1];
- Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
- Carnegie Inst. of Washington, Argonne, IL (United States). High Pressure Collaborative Access Team (HPCAT)
- Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany)
- Univ. of Alabama, Birmingham, AL (United States)
- Publication Date:
- Research Org.:
- Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS); Univ. of Alabama, Birmingham, AL (United States)
- Sponsoring Org.:
- USDOE National Nuclear Security Administration (NNSA); USDOE Office of Science (SC), Basic Energy Sciences (BES); German Federal Ministry of Education and Research (BMBF); National Science Foundation (NSF)
- OSTI Identifier:
- 1764194
- Alternate Identifier(s):
- OSTI ID: 1251164
- Report Number(s):
- LA-UR-13-28748
Journal ID: ISSN 1742-6596
- Grant/Contract Number:
- 89233218CNA000001; NA0002014; AC52-06NA25396; NA0001974; FG02-99ER45775; AC02-06CH11357; 05KS7RF1
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Journal of Physics. Conference Series (Online)
- Additional Journal Information:
- Journal Name: Journal of Physics. Conference Series (Online); Journal Volume: 500; Journal Issue: 3; Journal ID: ISSN 1742-6596
- Publisher:
- Institute of Physics (IOP)
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; phase transformations; transitional metals; time-resolved x-ray diffraction; high pressure; diamond anvil cell; dynamic compression
Citation Formats
Velisavljevic, Nenad, Sinogeikin, Stanislav, Saavedra, Ramon A., Chellappa, Raja S., Rothkirch, Andre, Dattelbaum, Dana M., Konopkova, Zuzana, Liermann, Hans-Peter, Bishop, Matthew M., Tsoi, Georgiy M., and Vohra, Yogesh K. Time-resolved x-ray diffraction and electrical resistance measurements of structural phase transitions in zirconium. United States: N. p., 2014.
Web. doi:10.1088/1742-6596/500/3/032020.
Velisavljevic, Nenad, Sinogeikin, Stanislav, Saavedra, Ramon A., Chellappa, Raja S., Rothkirch, Andre, Dattelbaum, Dana M., Konopkova, Zuzana, Liermann, Hans-Peter, Bishop, Matthew M., Tsoi, Georgiy M., & Vohra, Yogesh K. Time-resolved x-ray diffraction and electrical resistance measurements of structural phase transitions in zirconium. United States. https://doi.org/10.1088/1742-6596/500/3/032020
Velisavljevic, Nenad, Sinogeikin, Stanislav, Saavedra, Ramon A., Chellappa, Raja S., Rothkirch, Andre, Dattelbaum, Dana M., Konopkova, Zuzana, Liermann, Hans-Peter, Bishop, Matthew M., Tsoi, Georgiy M., and Vohra, Yogesh K. Wed .
"Time-resolved x-ray diffraction and electrical resistance measurements of structural phase transitions in zirconium". United States. https://doi.org/10.1088/1742-6596/500/3/032020. https://www.osti.gov/servlets/purl/1764194.
@article{osti_1764194,
title = {Time-resolved x-ray diffraction and electrical resistance measurements of structural phase transitions in zirconium},
author = {Velisavljevic, Nenad and Sinogeikin, Stanislav and Saavedra, Ramon A. and Chellappa, Raja S. and Rothkirch, Andre and Dattelbaum, Dana M. and Konopkova, Zuzana and Liermann, Hans-Peter and Bishop, Matthew M. and Tsoi, Georgiy M. and Vohra, Yogesh K.},
abstractNote = {Here, we have designed a portable pressure controller module to tune compression rates and maximum pressures attainable in a standard gas-membrane diamond anvil cell (DAC). During preliminary experiments, performed on zirconium (Zr) metal sample, pressure jumps of up to 80 GPa were systematically obtained in less than 0.2s (resulting in compression rate of few GPa/s up to more than 400 GPa/s). In-situ x-ray diffraction and electrical resistance measurements were performed simultaneously during this rapid pressure increase to provide the first time resolved data on α → ω → β structural evolution in Zr at high pressures. Direct control of compression rates and peak pressures, which can be held for prolonged time, allows for investigation of structural evolution and kinetics of structural phase transitions of materials under previously unexplored compression rate-pressure conditions that bridge traditional static and shock/dynamic experimental platforms.},
doi = {10.1088/1742-6596/500/3/032020},
journal = {Journal of Physics. Conference Series (Online)},
number = 3,
volume = 500,
place = {United States},
year = {Wed May 07 00:00:00 EDT 2014},
month = {Wed May 07 00:00:00 EDT 2014}
}
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Works referencing / citing this record:
Developments in time-resolved high pressure x-ray diffraction using rapid compression and decompression
journal, July 2015
- Smith, Jesse S.; Sinogeikin, Stanislav V.; Lin, Chuanlong
- Review of Scientific Instruments, Vol. 86, Issue 7
Online remote control systems for static and dynamic compression and decompression using diamond anvil cells
journal, July 2015
- Sinogeikin, Stanislav V.; Smith, Jesse S.; Rod, Eric
- Review of Scientific Instruments, Vol. 86, Issue 7
Room-temperature compression and equation of state of body-centered cubic zirconium
journal, December 2019
- Pigott, Jeffrey S.; Velisavljevic, Nenad; Moss, Eric K.
- Journal of Physics: Condensed Matter, Vol. 32, Issue 12
The Extreme Conditions Beamline P02.2 and the Extreme Conditions Science Infrastructure at PETRA III
journal, June 2015
- Liermann, H. -P.; Konôpková, Z.; Morgenroth, W.
- Journal of Synchrotron Radiation, Vol. 22, Issue 4