Pushing x-ray photon correlation spectroscopy beyond the continuous frame rate limit
Abstract
We demonstrate delayed-frame X-ray Photon Correlation Spectroscopy with 120 microsecond time resolution, limited only by sample scattering rates, with a prototype Pixel-array detector capable of taking two image frames separated by 153 ns or less. Although the overall frame rate is currently limited to about 4 frame pairs per second, we easily measured millisecond correlation functions. In conclusion, this technology, coupled to the use of brighter synchrotrons such as Petra III or the NSLS-II should enable X-ray Photon Correlation Spectroscopy on microsecond time scales on a wider variety of materials.
- Authors:
-
- Argonne National Lab. (ANL), Argonne, IL (United States)
- DePaul Univ., Chicago, IL (United States). Dept. of Physics
- Northern Illinois Univ., DeKalb, IL (United States). Dept. of Electrical Engineering
- Publication Date:
- Research Org.:
- Argonne National Laboratory (ANL), Argonne, IL (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES). Scientific User Facilities Division; USDOE Office of Science - Small Business Innovation Research (SBIR) and Small Business Technology Transfer (STTR) - Small Business Innovative Research Grant Program
- OSTI Identifier:
- 1251156
- Grant/Contract Number:
- AC02-06CH11357; SC0004235
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Optics Express
- Additional Journal Information:
- Journal Volume: 24; Journal Issue: 1; Journal ID: ISSN 1094-4087
- Publisher:
- Optical Society of America (OSA)
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS
Citation Formats
Dufresne, Eric M., Narayanan, Suresh, Sandy, Alec R., Kline, David M., Zhang, Qingteng, Landahl, Eric C., and Ross, Steve. Pushing x-ray photon correlation spectroscopy beyond the continuous frame rate limit. United States: N. p., 2016.
Web. doi:10.1364/OE.24.000355.
Dufresne, Eric M., Narayanan, Suresh, Sandy, Alec R., Kline, David M., Zhang, Qingteng, Landahl, Eric C., & Ross, Steve. Pushing x-ray photon correlation spectroscopy beyond the continuous frame rate limit. United States. https://doi.org/10.1364/OE.24.000355
Dufresne, Eric M., Narayanan, Suresh, Sandy, Alec R., Kline, David M., Zhang, Qingteng, Landahl, Eric C., and Ross, Steve. Wed .
"Pushing x-ray photon correlation spectroscopy beyond the continuous frame rate limit". United States. https://doi.org/10.1364/OE.24.000355. https://www.osti.gov/servlets/purl/1251156.
@article{osti_1251156,
title = {Pushing x-ray photon correlation spectroscopy beyond the continuous frame rate limit},
author = {Dufresne, Eric M. and Narayanan, Suresh and Sandy, Alec R. and Kline, David M. and Zhang, Qingteng and Landahl, Eric C. and Ross, Steve},
abstractNote = {We demonstrate delayed-frame X-ray Photon Correlation Spectroscopy with 120 microsecond time resolution, limited only by sample scattering rates, with a prototype Pixel-array detector capable of taking two image frames separated by 153 ns or less. Although the overall frame rate is currently limited to about 4 frame pairs per second, we easily measured millisecond correlation functions. In conclusion, this technology, coupled to the use of brighter synchrotrons such as Petra III or the NSLS-II should enable X-ray Photon Correlation Spectroscopy on microsecond time scales on a wider variety of materials.},
doi = {10.1364/OE.24.000355},
journal = {Optics Express},
number = 1,
volume = 24,
place = {United States},
year = {Wed Jan 06 00:00:00 EST 2016},
month = {Wed Jan 06 00:00:00 EST 2016}
}
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Works referencing / citing this record:
Spatial and temporal pre-alignment of an X-ray split-and-delay unit by laser light interferometry
journal, April 2019
- Roseker, W.; Lee, S.; Walther, M.
- Review of Scientific Instruments, Vol. 90, Issue 4
Submillisecond X-ray photon correlation spectroscopy from a pixel array detector with fast dual gating and no readout dead-time
journal, April 2016
- Zhang, Qingteng; Dufresne, Eric M.; Grybos, Pawel
- Journal of Synchrotron Radiation, Vol. 23, Issue 3
Spatial and temporal pre-alignment of an X-ray split-and-delay unit by laser light interferometry
text, January 2019
- Roseker, Wojciech; Lee, S.; Walther, Michael
- Deutsches Elektronen-Synchrotron, DESY, Hamburg