Oxygen-induced nano-faceting of Re(112¯1)

Wang, Hao; Chen, Wenhua; Bartynski, Robert A.

doi:10.1016/j.susc.2014.12.015

Title: Oxygen-induced nano-faceting of Re( 11 2 ¯ 1 )

Abstract

We report results from a detailed study of oxygen-induced faceting of Re(112¯1) using low energy electron diffraction (LEED). Depending on conditions for reaction with oxygen, the initially planar Re(112¯1) surface evolves sequentially to form zigzag chains consisting of (011¯0) and (101¯0) facets that coexist with stepped (112¯1) plateaus; three-sided pyramids exposing (011¯0), (101¯0) and (336¯4) facets; a faceted surface with five facets including (011¯0), (101¯0), (112¯2)-(2 × 1), (011¯1)-(2 × 1) and (101¯1)-(2 × 1); and four-sided pyramids exposing {011¯0} and {011¯1}-(2 × 1) facets. We have observed reversible morphological transitions between the faceted surfaces and discovered that each intermediate facet in the evolutionary chain contains microscopic structural elements of the preceding and following facets, which may provide a natural explanation for the microscopic mass transport pathways in the morphological evolution. Lastly, scanning tunneling microscopy (STM) data confirm the morphology of faceted surfaces and give complementary information to LEED results.

Authors:

^[1]; Chen, Wenhua ^[1]; Bartynski, Robert A. ^[1]

Rutgers, The State Univ. of New Jersey, Piscataway, NJ (United States)

Publication Date:: Thu Jan 08 00:00:00 EST 2015

Research Org.:: Rutgers Univ., Piscataway, NJ (United States)

Sponsoring Org.:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

OSTI Identifier:: 1349419

Alternate Identifier(s):: OSTI ID: 1244734

Grant/Contract Number:: FG02-93ER14331

Resource Type:: Accepted Manuscript

Journal Name:: Surface Science

Additional Journal Information:: Journal Volume: 635; Journal Issue: C; Journal ID: ISSN 0039-6028

Publisher:: Elsevier

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE; Rhenium; faceting; mass transport; oxygen; morphology

Citation Formats


                    Wang, Hao, Chen, Wenhua, and Bartynski, Robert A. Oxygen-induced nano-faceting of Re(112¯1).  United States: N. p., 2015. 
Web.  doi:10.1016/j.susc.2014.12.015.

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                    Wang, Hao, Chen, Wenhua, & Bartynski, Robert A. Oxygen-induced nano-faceting of Re(112¯1).  United States.  https://doi.org/10.1016/j.susc.2014.12.015

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                    Wang, Hao, Chen, Wenhua, and Bartynski, Robert A. Thu .  
"Oxygen-induced nano-faceting of Re(112¯1)".  United States.  https://doi.org/10.1016/j.susc.2014.12.015.  https://www.osti.gov/servlets/purl/1349419.

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@article{osti_1349419,

  title        = {Oxygen-induced nano-faceting of Re(112¯1)},

  author       = {Wang, Hao and Chen, Wenhua and Bartynski, Robert A.},

  abstractNote = {We report results from a detailed study of oxygen-induced faceting of Re(112¯1) using low energy electron diffraction (LEED). Depending on conditions for reaction with oxygen, the initially planar Re(112¯1) surface evolves sequentially to form zigzag chains consisting of (011¯0) and (101¯0) facets that coexist with stepped (112¯1) plateaus; three-sided pyramids exposing (011¯0), (101¯0) and (336¯4) facets; a faceted surface with five facets including (011¯0), (101¯0), (112¯2)-(2 × 1), (011¯1)-(2 × 1) and (101¯1)-(2 × 1); and four-sided pyramids exposing {011¯0} and {011¯1}-(2 × 1) facets. We have observed reversible morphological transitions between the faceted surfaces and discovered that each intermediate facet in the evolutionary chain contains microscopic structural elements of the preceding and following facets, which may provide a natural explanation for the microscopic mass transport pathways in the morphological evolution. Lastly, scanning tunneling microscopy (STM) data confirm the morphology of faceted surfaces and give complementary information to LEED results.},

  doi          = {10.1016/j.susc.2014.12.015},

  journal      = {Surface Science},

  number       = C,

  volume       = 635,

  place        = {United States},

  year         = {Thu Jan 08 00:00:00 EST 2015},

  month        = {Thu Jan 08 00:00:00 EST 2015}

}

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Title: Oxygen-induced nano-faceting of Re( 11 2 ¯ 1 )

Abstract

Citation Formats

DC-Resistive-Heating-Induced Step Bunching on Vicinal Si (111) journal, December 1990

Quantitative theory of current-induced step bunching on Si(111) journal, June 1998

Electromigration Induced Step Bunching on Si Surfaces – How Does it Depend on the Temperature and Heating Current Direction? journal, January 1991

An STM study of current-induced step bunching on Si(111) journal, June 1996

Symmetry-Induced Magnetic Anisotropy in Fe Films Grown on Stepped Ag(001) journal, September 1996

Tailoring of the Perpendicular Magnetization Component in Ferromagnetic Films on a Vicinal Substrate journal, November 2008

Atom-Resolved Imaging of Dynamic Shape Changes in Supported Copper Nanocrystals journal, March 2002

Dynamic in situ observation of rapid size and shape change of supported Pd nanoparticles during CO/NO cycling journal, May 2007

Shape Changes of Supported Rh Nanoparticles During Oxidation and Reduction Cycles journal, September 2008

Rhodium Nanoparticle Shape Dependence in the Reduction of NO by CO journal, September 2009

Surface facetting induced by adsorbates journal, November 2003

Nanoscale surface chemistry over faceted substrates: structure, reactivity and nanotemplates journal, January 2008

Adsorbate-induced reconstruction of surfaces: An atomistic alternative to microscopic faceting? journal, August 1994

Oxidation of CO by NO on planar and faceted Ir(210) journal, June 2012

Structure Sensitivity in the Oxidation of CO on Ir Surfaces journal, March 2006

Decomposition of Ammonia and Hydrogen on Ir Surfaces: Structure Sensitivity and Nanometer-Scale Size Effects journal, April 2005

Theoretical and experimental studies of hydrogen adsorption and desorption on Ir surfaces journal, January 2013

Nanofaceted C/Re(112̅1): Fabrication, Structure, and Template for Synthesizing Nanostructured Model Pt Electrocatalyst for Hydrogen Evolution Reaction journal, January 2012

Theoretical Study of Carbon Adsorption on Re Surfaces: Morphological Instability journal, August 2014

Oxygen chemisorption on Cu(19 19 1) studied by spot profile analysis low-energy electron diffraction journal, December 2007

Thermal Faceting of Clean and Oxygen-Covered Ir Nanocrystals journal, January 2011

Faceting and defaceting phase transitions of Pd ∕ W ( 111 ) journal, March 2007

Observation of vertex-rounding transition for a crystal in equilibrium: Oxygen-covered tungsten journal, March 2005

Break-Up of Stepped Platinum Catalyst Surfaces by High CO Coverage journal, February 2010

Growth of thin alumina films on a vicinal NiAl surface journal, October 2007

Facet Stability in Oxygen-Induced Nanofaceting of Re(123̅1) journal, November 2007

Morphological evolution in oxygen-induced faceting of Re ( 12 3 ¯ 1 ) journal, November 2006

Atomic and Molecular Adsorption on Re(0001) journal, October 2013

Reaction of rhenium and carbon at high pressures and temperatures journal, January 2008

Rhenium-containing catalysts in reactions of organic compounds journal, February 1998

The ammonia synthesis over rhenium single-crystal catalysts: Kinetics, structure sensitivity, and effect of potassium and oxygen journal, April 1986

A Highly Active Well-Defined Rhenium Heterogeneous Catalyst for Olefin Metathesis Prepared via Surface Organometallic Chemistry journal, March 2001

Rhenium-Catalyzed Growth Carbon Nanotubes journal, June 2007

Thiophene hydrodesulfurization over transition metal surfaces: Structure insensitive over molybdenum and structure sensitive over rhenium journal, April 1988

Structure and stress of Re(112̄1); chiral terraces at a racemic surface journal, January 2013

Adsorption and Decomposition of Acetylene on Planar and Faceted Ir(210) journal, June 2003

Some Theorems on the Free Energies of Crystal Surfaces journal, April 1951

Structure of rhenium surfaces in an oxygen environment journal, January 2011

First-principles studies on adsorbate-induced faceting of Re ( 11 2 ¯ 1 ) journal, April 2009

DC-Resistive-Heating-Induced Step Bunching on Vicinal Si (111)
journal, December 1990

Quantitative theory of current-induced step bunching on Si(111)
journal, June 1998

Electromigration Induced Step Bunching on Si Surfaces – How Does it Depend on the Temperature and Heating Current Direction?
journal, January 1991

An STM study of current-induced step bunching on Si(111)
journal, June 1996

Symmetry-Induced Magnetic Anisotropy in Fe Films Grown on Stepped Ag(001)
journal, September 1996

Tailoring of the Perpendicular Magnetization Component in Ferromagnetic Films on a Vicinal Substrate
journal, November 2008

Atom-Resolved Imaging of Dynamic Shape Changes in Supported Copper Nanocrystals
journal, March 2002

Dynamic in situ observation of rapid size and shape change of supported Pd nanoparticles during CO/NO cycling
journal, May 2007

Shape Changes of Supported Rh Nanoparticles During Oxidation and Reduction Cycles
journal, September 2008

Rhodium Nanoparticle Shape Dependence in the Reduction of NO by CO
journal, September 2009

Surface facetting induced by adsorbates
journal, November 2003

Nanoscale surface chemistry over faceted substrates: structure, reactivity and nanotemplates
journal, January 2008

Adsorbate-induced reconstruction of surfaces: An atomistic alternative to microscopic faceting?
journal, August 1994

Oxidation of CO by NO on planar and faceted Ir(210)
journal, June 2012

Structure Sensitivity in the Oxidation of CO on Ir Surfaces
journal, March 2006

Decomposition of Ammonia and Hydrogen on Ir Surfaces: Structure Sensitivity and Nanometer-Scale Size Effects
journal, April 2005

Theoretical and experimental studies of hydrogen adsorption and desorption on Ir surfaces
journal, January 2013

Nanofaceted C/Re(112̅1): Fabrication, Structure, and Template for Synthesizing Nanostructured Model Pt Electrocatalyst for Hydrogen Evolution Reaction
journal, January 2012

Theoretical Study of Carbon Adsorption on Re Surfaces: Morphological Instability
journal, August 2014

Oxygen chemisorption on Cu(19 19 1) studied by spot profile analysis low-energy electron diffraction
journal, December 2007

Thermal Faceting of Clean and Oxygen-Covered Ir Nanocrystals
journal, January 2011

Faceting and defaceting phase transitions of $Pd ∕ W (111)$
journal, March 2007

Observation of vertex-rounding transition for a crystal in equilibrium: Oxygen-covered tungsten
journal, March 2005

Break-Up of Stepped Platinum Catalyst Surfaces by High CO Coverage
journal, February 2010

Growth of thin alumina films on a vicinal NiAl surface
journal, October 2007

Facet Stability in Oxygen-Induced Nanofaceting of Re(123̅1)
journal, November 2007

Morphological evolution in oxygen-induced faceting of $Re (12 \bar{3} 1)$
journal, November 2006

Atomic and Molecular Adsorption on Re(0001)
journal, October 2013

Reaction of rhenium and carbon at high pressures and temperatures
journal, January 2008

Rhenium-containing catalysts in reactions of organic compounds
journal, February 1998

The ammonia synthesis over rhenium single-crystal catalysts: Kinetics, structure sensitivity, and effect of potassium and oxygen
journal, April 1986

A Highly Active Well-Defined Rhenium Heterogeneous Catalyst for Olefin Metathesis Prepared via Surface Organometallic Chemistry
journal, March 2001

Rhenium-Catalyzed Growth Carbon Nanotubes
journal, June 2007

Thiophene hydrodesulfurization over transition metal surfaces: Structure insensitive over molybdenum and structure sensitive over rhenium
journal, April 1988

Structure and stress of Re(112̄1); chiral terraces at a racemic surface
journal, January 2013

Adsorption and Decomposition of Acetylene on Planar and Faceted Ir(210)
journal, June 2003

Some Theorems on the Free Energies of Crystal Surfaces
journal, April 1951

Structure of rhenium surfaces in an oxygen environment
journal, January 2011

First-principles studies on adsorbate-induced faceting of $Re (11 \bar{2} 1)$
journal, April 2009